Does Metal Matter: Comparing Photophysical Properties of Bis-Cyclometalated Alkynylphosphonium Au(III) and Pt(II) Complexes

In this work, two series of Au(III) and Pt(II) alkynylphosphonium complexes of composition [M(CNC)(C<sub>2</sub>−L−P(CH<sub>3</sub>)Ph<sub>2</sub>)]<sup>n+</sup> <b>Pt1</b>–<b>Pt3</b> (n = 0) and <b>Au1</b>–<b>...

Full description

Saved in:
Bibliographic Details
Main Authors: Maksim Luginin, Aleksandra Paderina, Anastasia Sizova, Elena Tupikina, Elena Grachova
Format: Article
Language:English
Published: MDPI AG 2025-06-01
Series:Molecules
Subjects:
Online Access:https://www.mdpi.com/1420-3049/30/11/2434
Tags: Add Tag
No Tags, Be the first to tag this record!
Description
Summary:In this work, two series of Au(III) and Pt(II) alkynylphosphonium complexes of composition [M(CNC)(C<sub>2</sub>−L−P(CH<sub>3</sub>)Ph<sub>2</sub>)]<sup>n+</sup> <b>Pt1</b>–<b>Pt3</b> (n = 0) and <b>Au1</b>–<b>Au3</b> (n = 1), (CNC = 2,6-diphenylpyridine; L = phenyl, biphenyl, naphthyl) were synthesized and characterized to discover the similarities and differences in photophysical properties between isoelectronic metallocentres. It is shown that Au(III) and Pt(II) complexes obtained demonstrate different photophysical properties despite isoelectronic metal centres, and some reasons for that are discussed based on experimental data and quantum-chemical calculation results. Complex <b>Pt1</b> also demonstrated the first example of room-temperature solution phosphorescence in the family of [Pt(CNC)(alkynyl)] complexes. It has been found that the crystal packing of <b>Pt1</b> contains a Pt–H interaction, qualified by quantum-chemical calculations as a unique hydrogen bond.
ISSN:1420-3049