Microwave Promoted Regeneration of Carbonyl Compounds from Oximes Using N, N-Dichloro Poly(Styrene-co-divinylbenzene)Sulphonamide Resin
An efficient, economically viable and operationally simple method was developed for deoximation of oximes (of ketones and aldehydes) to their corresponding carbonyl compounds using polymer beads of N, N-dichloro poly(styrene-co-divinylbenzene)sulphonamide resin. Polymeric reagent offered speedy conv...
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Format: | Article |
Language: | English |
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Wiley
2011-01-01
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Series: | E-Journal of Chemistry |
Online Access: | http://dx.doi.org/10.1155/2011/590923 |
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author | A.G. Beldar Mamta Sharma |
author_facet | A.G. Beldar Mamta Sharma |
author_sort | A.G. Beldar |
collection | DOAJ |
description | An efficient, economically viable and operationally simple method was developed for deoximation of oximes (of ketones and aldehydes) to their corresponding carbonyl compounds using polymer beads of N, N-dichloro poly(styrene-co-divinylbenzene)sulphonamide resin. Polymeric reagent offered speedy conversion and substantial yields of products under mild condition and is recyclable. Deoximation was monitored by the use of 13C NMR. |
format | Article |
id | doaj-art-9b3b163c5277444d847a941c8cb46d06 |
institution | Kabale University |
issn | 0973-4945 2090-9810 |
language | English |
publishDate | 2011-01-01 |
publisher | Wiley |
record_format | Article |
series | E-Journal of Chemistry |
spelling | doaj-art-9b3b163c5277444d847a941c8cb46d062025-02-03T06:06:09ZengWileyE-Journal of Chemistry0973-49452090-98102011-01-018128829210.1155/2011/590923Microwave Promoted Regeneration of Carbonyl Compounds from Oximes Using N, N-Dichloro Poly(Styrene-co-divinylbenzene)Sulphonamide ResinA.G. Beldar0Mamta Sharma1Synthetic Chemistry Division, Defence R & D Establishment, Jhansi Road, Gwalior-474002, M.P., IndiaSynthetic Chemistry Division, Defence R & D Establishment, Jhansi Road, Gwalior-474002, M.P., IndiaAn efficient, economically viable and operationally simple method was developed for deoximation of oximes (of ketones and aldehydes) to their corresponding carbonyl compounds using polymer beads of N, N-dichloro poly(styrene-co-divinylbenzene)sulphonamide resin. Polymeric reagent offered speedy conversion and substantial yields of products under mild condition and is recyclable. Deoximation was monitored by the use of 13C NMR.http://dx.doi.org/10.1155/2011/590923 |
spellingShingle | A.G. Beldar Mamta Sharma Microwave Promoted Regeneration of Carbonyl Compounds from Oximes Using N, N-Dichloro Poly(Styrene-co-divinylbenzene)Sulphonamide Resin E-Journal of Chemistry |
title | Microwave Promoted Regeneration of Carbonyl Compounds from Oximes Using N, N-Dichloro Poly(Styrene-co-divinylbenzene)Sulphonamide Resin |
title_full | Microwave Promoted Regeneration of Carbonyl Compounds from Oximes Using N, N-Dichloro Poly(Styrene-co-divinylbenzene)Sulphonamide Resin |
title_fullStr | Microwave Promoted Regeneration of Carbonyl Compounds from Oximes Using N, N-Dichloro Poly(Styrene-co-divinylbenzene)Sulphonamide Resin |
title_full_unstemmed | Microwave Promoted Regeneration of Carbonyl Compounds from Oximes Using N, N-Dichloro Poly(Styrene-co-divinylbenzene)Sulphonamide Resin |
title_short | Microwave Promoted Regeneration of Carbonyl Compounds from Oximes Using N, N-Dichloro Poly(Styrene-co-divinylbenzene)Sulphonamide Resin |
title_sort | microwave promoted regeneration of carbonyl compounds from oximes using n n dichloro poly styrene co divinylbenzene sulphonamide resin |
url | http://dx.doi.org/10.1155/2011/590923 |
work_keys_str_mv | AT agbeldar microwavepromotedregenerationofcarbonylcompoundsfromoximesusingnndichloropolystyrenecodivinylbenzenesulphonamideresin AT mamtasharma microwavepromotedregenerationofcarbonylcompoundsfromoximesusingnndichloropolystyrenecodivinylbenzenesulphonamideresin |