Microwave Promoted Regeneration of Carbonyl Compounds from Oximes Using N, N-Dichloro Poly(Styrene-co-divinylbenzene)Sulphonamide Resin

An efficient, economically viable and operationally simple method was developed for deoximation of oximes (of ketones and aldehydes) to their corresponding carbonyl compounds using polymer beads of N, N-dichloro poly(styrene-co-divinylbenzene)sulphonamide resin. Polymeric reagent offered speedy conv...

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Main Authors: A.G. Beldar, Mamta Sharma
Format: Article
Language:English
Published: Wiley 2011-01-01
Series:E-Journal of Chemistry
Online Access:http://dx.doi.org/10.1155/2011/590923
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author A.G. Beldar
Mamta Sharma
author_facet A.G. Beldar
Mamta Sharma
author_sort A.G. Beldar
collection DOAJ
description An efficient, economically viable and operationally simple method was developed for deoximation of oximes (of ketones and aldehydes) to their corresponding carbonyl compounds using polymer beads of N, N-dichloro poly(styrene-co-divinylbenzene)sulphonamide resin. Polymeric reagent offered speedy conversion and substantial yields of products under mild condition and is recyclable. Deoximation was monitored by the use of 13C NMR.
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institution Kabale University
issn 0973-4945
2090-9810
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publishDate 2011-01-01
publisher Wiley
record_format Article
series E-Journal of Chemistry
spelling doaj-art-9b3b163c5277444d847a941c8cb46d062025-02-03T06:06:09ZengWileyE-Journal of Chemistry0973-49452090-98102011-01-018128829210.1155/2011/590923Microwave Promoted Regeneration of Carbonyl Compounds from Oximes Using N, N-Dichloro Poly(Styrene-co-divinylbenzene)Sulphonamide ResinA.G. Beldar0Mamta Sharma1Synthetic Chemistry Division, Defence R & D Establishment, Jhansi Road, Gwalior-474002, M.P., IndiaSynthetic Chemistry Division, Defence R & D Establishment, Jhansi Road, Gwalior-474002, M.P., IndiaAn efficient, economically viable and operationally simple method was developed for deoximation of oximes (of ketones and aldehydes) to their corresponding carbonyl compounds using polymer beads of N, N-dichloro poly(styrene-co-divinylbenzene)sulphonamide resin. Polymeric reagent offered speedy conversion and substantial yields of products under mild condition and is recyclable. Deoximation was monitored by the use of 13C NMR.http://dx.doi.org/10.1155/2011/590923
spellingShingle A.G. Beldar
Mamta Sharma
Microwave Promoted Regeneration of Carbonyl Compounds from Oximes Using N, N-Dichloro Poly(Styrene-co-divinylbenzene)Sulphonamide Resin
E-Journal of Chemistry
title Microwave Promoted Regeneration of Carbonyl Compounds from Oximes Using N, N-Dichloro Poly(Styrene-co-divinylbenzene)Sulphonamide Resin
title_full Microwave Promoted Regeneration of Carbonyl Compounds from Oximes Using N, N-Dichloro Poly(Styrene-co-divinylbenzene)Sulphonamide Resin
title_fullStr Microwave Promoted Regeneration of Carbonyl Compounds from Oximes Using N, N-Dichloro Poly(Styrene-co-divinylbenzene)Sulphonamide Resin
title_full_unstemmed Microwave Promoted Regeneration of Carbonyl Compounds from Oximes Using N, N-Dichloro Poly(Styrene-co-divinylbenzene)Sulphonamide Resin
title_short Microwave Promoted Regeneration of Carbonyl Compounds from Oximes Using N, N-Dichloro Poly(Styrene-co-divinylbenzene)Sulphonamide Resin
title_sort microwave promoted regeneration of carbonyl compounds from oximes using n n dichloro poly styrene co divinylbenzene sulphonamide resin
url http://dx.doi.org/10.1155/2011/590923
work_keys_str_mv AT agbeldar microwavepromotedregenerationofcarbonylcompoundsfromoximesusingnndichloropolystyrenecodivinylbenzenesulphonamideresin
AT mamtasharma microwavepromotedregenerationofcarbonylcompoundsfromoximesusingnndichloropolystyrenecodivinylbenzenesulphonamideresin