TEM Study of High-Temperature Precipitation of Delta Phase in Inconel 718 Alloy

Inconel 718 is widely used because of its ability to retain strength at up to 650∘C for long periods of time through coherent metastable 𝛾 Ni3Nb precipitation associated with a smaller volume fraction of 𝛾 Ni3Al precipitates. At very long ageing times at service temperature, 𝛾 decomposes to...

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Main Authors: Moukrane Dehmas, Jacques Lacaze, Aliou Niang, Bernard Viguier
Format: Article
Language:English
Published: Wiley 2011-01-01
Series:Advances in Materials Science and Engineering
Online Access:http://dx.doi.org/10.1155/2011/940634
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author Moukrane Dehmas
Jacques Lacaze
Aliou Niang
Bernard Viguier
author_facet Moukrane Dehmas
Jacques Lacaze
Aliou Niang
Bernard Viguier
author_sort Moukrane Dehmas
collection DOAJ
description Inconel 718 is widely used because of its ability to retain strength at up to 650∘C for long periods of time through coherent metastable 𝛾 Ni3Nb precipitation associated with a smaller volume fraction of 𝛾 Ni3Al precipitates. At very long ageing times at service temperature, 𝛾 decomposes to the stable Ni3Nb 𝛿 phase. This latter phase is also present above the 𝛾 solvus and is used for grain control during forging of alloy 718. While most works available on 𝛿 precipitation have been performed at temperatures below the 𝛾 solvus, it appeared of interest to also investigate the case where 𝛿 phase precipitates directly from the fcc matrix free of 𝛾 precipitates. This was studied by X-ray diffraction and transmission electron microscopy (TEM). TEM observations confirmed the presence of rotation-ordered domains in 𝛿 plates, and some unexpected contrast could be explained by double diffraction due to overlapping phases.
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institution Kabale University
issn 1687-8434
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language English
publishDate 2011-01-01
publisher Wiley
record_format Article
series Advances in Materials Science and Engineering
spelling doaj-art-915af91eacc6402a9f412f8ef5ad78182025-02-03T01:03:32ZengWileyAdvances in Materials Science and Engineering1687-84341687-84422011-01-01201110.1155/2011/940634940634TEM Study of High-Temperature Precipitation of Delta Phase in Inconel 718 AlloyMoukrane Dehmas0Jacques Lacaze1Aliou Niang2Bernard Viguier3IJL-SI2M UMR 7198 CNRS-Nancy Université-UPV Metz, École des Mines de Nancy, Parc de Saurupt, CS 14234, 54042 Nancy Cedex, FranceInstitut Carnot CIRIMAT, Université de Toulouse, INP-ENSIACET, 4 allée Emile Monso, BP 44362, 31030 Toulouse Cedex 4, FranceInstitut Carnot CIRIMAT, Université de Toulouse, INP-ENSIACET, 4 allée Emile Monso, BP 44362, 31030 Toulouse Cedex 4, FranceInstitut Carnot CIRIMAT, Université de Toulouse, INP-ENSIACET, 4 allée Emile Monso, BP 44362, 31030 Toulouse Cedex 4, FranceInconel 718 is widely used because of its ability to retain strength at up to 650∘C for long periods of time through coherent metastable 𝛾 Ni3Nb precipitation associated with a smaller volume fraction of 𝛾 Ni3Al precipitates. At very long ageing times at service temperature, 𝛾 decomposes to the stable Ni3Nb 𝛿 phase. This latter phase is also present above the 𝛾 solvus and is used for grain control during forging of alloy 718. While most works available on 𝛿 precipitation have been performed at temperatures below the 𝛾 solvus, it appeared of interest to also investigate the case where 𝛿 phase precipitates directly from the fcc matrix free of 𝛾 precipitates. This was studied by X-ray diffraction and transmission electron microscopy (TEM). TEM observations confirmed the presence of rotation-ordered domains in 𝛿 plates, and some unexpected contrast could be explained by double diffraction due to overlapping phases.http://dx.doi.org/10.1155/2011/940634
spellingShingle Moukrane Dehmas
Jacques Lacaze
Aliou Niang
Bernard Viguier
TEM Study of High-Temperature Precipitation of Delta Phase in Inconel 718 Alloy
Advances in Materials Science and Engineering
title TEM Study of High-Temperature Precipitation of Delta Phase in Inconel 718 Alloy
title_full TEM Study of High-Temperature Precipitation of Delta Phase in Inconel 718 Alloy
title_fullStr TEM Study of High-Temperature Precipitation of Delta Phase in Inconel 718 Alloy
title_full_unstemmed TEM Study of High-Temperature Precipitation of Delta Phase in Inconel 718 Alloy
title_short TEM Study of High-Temperature Precipitation of Delta Phase in Inconel 718 Alloy
title_sort tem study of high temperature precipitation of delta phase in inconel 718 alloy
url http://dx.doi.org/10.1155/2011/940634
work_keys_str_mv AT moukranedehmas temstudyofhightemperatureprecipitationofdeltaphaseininconel718alloy
AT jacqueslacaze temstudyofhightemperatureprecipitationofdeltaphaseininconel718alloy
AT aliouniang temstudyofhightemperatureprecipitationofdeltaphaseininconel718alloy
AT bernardviguier temstudyofhightemperatureprecipitationofdeltaphaseininconel718alloy