Spectral Characterization and Crystal Structure of 1,2-Bis-(1H-benzimidazol-2-yl)-ethane Dihydrochloride
The crystal structure of 1,2-bis-(1H-benzimidazol-2-yl)-ethane dihydrochloride (1) was determined by X-ray diffraction at room temperature. The structure of 1 was also characterized by mass, elemental analysis, FT-IR, and NMR spectroscopy techniques. The title compound crystallizes in triclinic syst...
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Wiley
2013-01-01
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| Series: | Journal of Chemistry |
| Online Access: | http://dx.doi.org/10.1155/2013/634986 |
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| author | Aydin Tavman Cigdem Sayil |
| author_facet | Aydin Tavman Cigdem Sayil |
| author_sort | Aydin Tavman |
| collection | DOAJ |
| description | The crystal structure of 1,2-bis-(1H-benzimidazol-2-yl)-ethane dihydrochloride (1) was determined by X-ray diffraction at room temperature. The structure of 1 was also characterized by mass, elemental analysis, FT-IR, and NMR spectroscopy techniques. The title compound crystallizes in triclinic system and space group P-1, a=7.1350, b=9.6299(1), c=15.3340(7) Å, α=80.67(2),β=79.66(2),γ=68.395(11)∘, V=958.33(10) Å3, Z=2. Owing to the anti conformations of –CH2– groups, the entire molecule is relatively flat. H1-NMR spectra of 1 show AA′XX′ system characteristics. |
| format | Article |
| id | doaj-art-8e9698aff2dc469e8b4f446193c43c07 |
| institution | Kabale University |
| issn | 2090-9063 2090-9071 |
| language | English |
| publishDate | 2013-01-01 |
| publisher | Wiley |
| record_format | Article |
| series | Journal of Chemistry |
| spelling | doaj-art-8e9698aff2dc469e8b4f446193c43c072025-02-03T05:44:24ZengWileyJournal of Chemistry2090-90632090-90712013-01-01201310.1155/2013/634986634986Spectral Characterization and Crystal Structure of 1,2-Bis-(1H-benzimidazol-2-yl)-ethane DihydrochlorideAydin Tavman0Cigdem Sayil1Department of Chemistry, Faculty of Engineering, Istanbul University, 34320 Istanbul, TurkeyDepartment of Chemistry, Faculty of Engineering, Istanbul University, 34320 Istanbul, TurkeyThe crystal structure of 1,2-bis-(1H-benzimidazol-2-yl)-ethane dihydrochloride (1) was determined by X-ray diffraction at room temperature. The structure of 1 was also characterized by mass, elemental analysis, FT-IR, and NMR spectroscopy techniques. The title compound crystallizes in triclinic system and space group P-1, a=7.1350, b=9.6299(1), c=15.3340(7) Å, α=80.67(2),β=79.66(2),γ=68.395(11)∘, V=958.33(10) Å3, Z=2. Owing to the anti conformations of –CH2– groups, the entire molecule is relatively flat. H1-NMR spectra of 1 show AA′XX′ system characteristics.http://dx.doi.org/10.1155/2013/634986 |
| spellingShingle | Aydin Tavman Cigdem Sayil Spectral Characterization and Crystal Structure of 1,2-Bis-(1H-benzimidazol-2-yl)-ethane Dihydrochloride Journal of Chemistry |
| title | Spectral Characterization and Crystal Structure of 1,2-Bis-(1H-benzimidazol-2-yl)-ethane Dihydrochloride |
| title_full | Spectral Characterization and Crystal Structure of 1,2-Bis-(1H-benzimidazol-2-yl)-ethane Dihydrochloride |
| title_fullStr | Spectral Characterization and Crystal Structure of 1,2-Bis-(1H-benzimidazol-2-yl)-ethane Dihydrochloride |
| title_full_unstemmed | Spectral Characterization and Crystal Structure of 1,2-Bis-(1H-benzimidazol-2-yl)-ethane Dihydrochloride |
| title_short | Spectral Characterization and Crystal Structure of 1,2-Bis-(1H-benzimidazol-2-yl)-ethane Dihydrochloride |
| title_sort | spectral characterization and crystal structure of 1 2 bis 1h benzimidazol 2 yl ethane dihydrochloride |
| url | http://dx.doi.org/10.1155/2013/634986 |
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