Application of two-step diffusion couple technique in high-throughput screening of optimal composition and aging temperatures for alloys design: A demonstration in binary Ni-Al system

In this paper, four binary Ni-13.4 at.% Al/Ni-17.7 at.% Al diffusion couples were first prepared and subjected to homogenization at 1573 K for 10,800 s, from which a continuous concentration profile formed. The three diffusion couples were then cooled down for aging at respective temperatures, i.e.,...

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Main Authors: Shang Y.-J., Cao D.-J., Li Q., Yang K., Deng C.-M., Zhang L.-J.
Format: Article
Language:English
Published: University of Belgrade, Technical Faculty, Bor 2021-01-01
Series:Journal of Mining and Metallurgy. Section B: Metallurgy
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Online Access:http://www.doiserbia.nb.rs/img/doi/1450-5339/2021/1450-53392100011S.pdf
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author Shang Y.-J.
Cao D.-J.
Li Q.
Yang K.
Deng C.-M.
Zhang L.-J.
author_facet Shang Y.-J.
Cao D.-J.
Li Q.
Yang K.
Deng C.-M.
Zhang L.-J.
author_sort Shang Y.-J.
collection DOAJ
description In this paper, four binary Ni-13.4 at.% Al/Ni-17.7 at.% Al diffusion couples were first prepared and subjected to homogenization at 1573 K for 10,800 s, from which a continuous concentration profile formed. The three diffusion couples were then cooled down for aging at respective temperatures, i.e., 1173, 1123, and 1073 K, for 14400 s. The effect of composition and aging temperature on the aging microstructure was studied in detail by means of different experimental techniques and statistical analysis. The volume fraction, grain size, and shape factor of γʹ precipitates in the three diffusion couples were plotted as a function of alloy composition and annealing temperatures. Together with the previously proposed evaluation function in which the phase fraction, grain size, and shape factor of γʹ precipitates were chosen as the evaluation indicators, the optimal alloy composition and aging temperature for binary Ni-Al alloys with the best mechanical properties were evaluated, and finally validated by the measured hardness values. The successful demonstration of alloy design in the present binary Ni-Al alloys indicated that the two-step diffusion couple, together with the evaluation function for mechanic properties, should be of generality for high-throughput screening of optimal alloy composition and heat treatment process in different alloys.
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institution Kabale University
issn 1450-5339
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language English
publishDate 2021-01-01
publisher University of Belgrade, Technical Faculty, Bor
record_format Article
series Journal of Mining and Metallurgy. Section B: Metallurgy
spelling doaj-art-8a5e63abe4c24b94928a2db7d05465d52025-02-03T02:39:51ZengUniversity of Belgrade, Technical Faculty, BorJournal of Mining and Metallurgy. Section B: Metallurgy1450-53392217-71752021-01-0157217518410.2298/JMMB191223011S1450-53392100011SApplication of two-step diffusion couple technique in high-throughput screening of optimal composition and aging temperatures for alloys design: A demonstration in binary Ni-Al systemShang Y.-J.0Cao D.-J.1Li Q.2Yang K.3Deng C.-M.4Zhang L.-J.5State Key Laboratory of Powder Metallurgy, Central South University, Changsha, Hunan, ChinaState Key Laboratory of Powder Metallurgy, Central South University, Changsha, Hunan, ChinaState Key Laboratory of Powder Metallurgy, Central South University, Changsha, Hunan, ChinaaInstitute of New Materials, Guangdong Academy of Sciences, National Engineering Laboratory for Modern Materials Surface Engineering Technology, The key Lab of Guangdong for Modern Surface Engineering Technology, Guangzhou, ChinaaInstitute of New Materials, Guangdong Academy of Sciences, National Engineering Laboratory for Modern Materials Surface Engineering Technology, The key Lab of Guangdong for Modern Surface Engineering Technology, Guangzhou, ChinaInstitute of New Materials, Guangdong Academy of Sciences, National Engineering Laboratory for Modern Materials Surface Engineering Technology, The key Lab of Guangdong for Modern Surface Engineering Technology, Guangzhou , China + State Key Laboratory of Powder Metallurgy, Central South University, Changsha, Hunan, ChinaIn this paper, four binary Ni-13.4 at.% Al/Ni-17.7 at.% Al diffusion couples were first prepared and subjected to homogenization at 1573 K for 10,800 s, from which a continuous concentration profile formed. The three diffusion couples were then cooled down for aging at respective temperatures, i.e., 1173, 1123, and 1073 K, for 14400 s. The effect of composition and aging temperature on the aging microstructure was studied in detail by means of different experimental techniques and statistical analysis. The volume fraction, grain size, and shape factor of γʹ precipitates in the three diffusion couples were plotted as a function of alloy composition and annealing temperatures. Together with the previously proposed evaluation function in which the phase fraction, grain size, and shape factor of γʹ precipitates were chosen as the evaluation indicators, the optimal alloy composition and aging temperature for binary Ni-Al alloys with the best mechanical properties were evaluated, and finally validated by the measured hardness values. The successful demonstration of alloy design in the present binary Ni-Al alloys indicated that the two-step diffusion couple, together with the evaluation function for mechanic properties, should be of generality for high-throughput screening of optimal alloy composition and heat treatment process in different alloys.http://www.doiserbia.nb.rs/img/doi/1450-5339/2021/1450-53392100011S.pdftwo-step diffusion coupleni-al alloysmicrostructurehardnessalloys design
spellingShingle Shang Y.-J.
Cao D.-J.
Li Q.
Yang K.
Deng C.-M.
Zhang L.-J.
Application of two-step diffusion couple technique in high-throughput screening of optimal composition and aging temperatures for alloys design: A demonstration in binary Ni-Al system
Journal of Mining and Metallurgy. Section B: Metallurgy
two-step diffusion couple
ni-al alloys
microstructure
hardness
alloys design
title Application of two-step diffusion couple technique in high-throughput screening of optimal composition and aging temperatures for alloys design: A demonstration in binary Ni-Al system
title_full Application of two-step diffusion couple technique in high-throughput screening of optimal composition and aging temperatures for alloys design: A demonstration in binary Ni-Al system
title_fullStr Application of two-step diffusion couple technique in high-throughput screening of optimal composition and aging temperatures for alloys design: A demonstration in binary Ni-Al system
title_full_unstemmed Application of two-step diffusion couple technique in high-throughput screening of optimal composition and aging temperatures for alloys design: A demonstration in binary Ni-Al system
title_short Application of two-step diffusion couple technique in high-throughput screening of optimal composition and aging temperatures for alloys design: A demonstration in binary Ni-Al system
title_sort application of two step diffusion couple technique in high throughput screening of optimal composition and aging temperatures for alloys design a demonstration in binary ni al system
topic two-step diffusion couple
ni-al alloys
microstructure
hardness
alloys design
url http://www.doiserbia.nb.rs/img/doi/1450-5339/2021/1450-53392100011S.pdf
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