A novel technique to synthesis of tenorite (CuO) nanoparticles from low concentration CuSO4 solution
In this study CuO nanoparticles were prepared via direct thermal decomposition method using basic copper sulphates as wet chemically synthesized precursor which was calcined in air at 750°C for 2h. Samples were characterized by thermogravimetric (TG-DSC), X-ray diffraction (XRD), energy dispersi...
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| Format: | Article |
| Language: | English |
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University of Belgrade, Technical Faculty, Bor
2011-01-01
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| Series: | Journal of Mining and Metallurgy. Section B: Metallurgy |
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| Online Access: | http://www.doiserbia.nb.rs/img/doi/1450-5339/2011/1450-53391101073D.pdf |
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| author | Darezereshki E. Bakhtiari F. |
| author_facet | Darezereshki E. Bakhtiari F. |
| author_sort | Darezereshki E. |
| collection | DOAJ |
| description | In this study CuO nanoparticles were prepared via direct thermal decomposition method using basic copper sulphates as wet chemically synthesized precursor which was calcined in air at 750°C for 2h. Samples were characterized by thermogravimetric (TG-DSC), X-ray diffraction (XRD), energy dispersive spectroscopy (EDS), infrared spectrum (IR), scanning electron microscopy (SEM), and transmission electron microscopy (TEM). The XRD, EDS, and IR results indicated that the synthesized CuO particles were pure. The SEM and TEM results showed that the CuO nanoparticles were of approximate spherical shape, and 170±5 nm in size. Using this method, Cuo nanoparticles could be produced without using organic solvent, expensive raw materials, and complicated equipment. |
| format | Article |
| id | doaj-art-83d01fd0b28b49ceb7c9fbbb4ed73cac |
| institution | Kabale University |
| issn | 1450-5339 |
| language | English |
| publishDate | 2011-01-01 |
| publisher | University of Belgrade, Technical Faculty, Bor |
| record_format | Article |
| series | Journal of Mining and Metallurgy. Section B: Metallurgy |
| spelling | doaj-art-83d01fd0b28b49ceb7c9fbbb4ed73cac2025-02-02T11:58:04ZengUniversity of Belgrade, Technical Faculty, BorJournal of Mining and Metallurgy. Section B: Metallurgy1450-53392011-01-01471737810.2298/JMMB1101073DA novel technique to synthesis of tenorite (CuO) nanoparticles from low concentration CuSO4 solutionDarezereshki E.Bakhtiari F.In this study CuO nanoparticles were prepared via direct thermal decomposition method using basic copper sulphates as wet chemically synthesized precursor which was calcined in air at 750°C for 2h. Samples were characterized by thermogravimetric (TG-DSC), X-ray diffraction (XRD), energy dispersive spectroscopy (EDS), infrared spectrum (IR), scanning electron microscopy (SEM), and transmission electron microscopy (TEM). The XRD, EDS, and IR results indicated that the synthesized CuO particles were pure. The SEM and TEM results showed that the CuO nanoparticles were of approximate spherical shape, and 170±5 nm in size. Using this method, Cuo nanoparticles could be produced without using organic solvent, expensive raw materials, and complicated equipment.http://www.doiserbia.nb.rs/img/doi/1450-5339/2011/1450-53391101073D.pdfCuOnanoparticlessynthesisthermal decomposition |
| spellingShingle | Darezereshki E. Bakhtiari F. A novel technique to synthesis of tenorite (CuO) nanoparticles from low concentration CuSO4 solution Journal of Mining and Metallurgy. Section B: Metallurgy CuO nanoparticles synthesis thermal decomposition |
| title | A novel technique to synthesis of tenorite (CuO) nanoparticles from low concentration CuSO4 solution |
| title_full | A novel technique to synthesis of tenorite (CuO) nanoparticles from low concentration CuSO4 solution |
| title_fullStr | A novel technique to synthesis of tenorite (CuO) nanoparticles from low concentration CuSO4 solution |
| title_full_unstemmed | A novel technique to synthesis of tenorite (CuO) nanoparticles from low concentration CuSO4 solution |
| title_short | A novel technique to synthesis of tenorite (CuO) nanoparticles from low concentration CuSO4 solution |
| title_sort | novel technique to synthesis of tenorite cuo nanoparticles from low concentration cuso4 solution |
| topic | CuO nanoparticles synthesis thermal decomposition |
| url | http://www.doiserbia.nb.rs/img/doi/1450-5339/2011/1450-53391101073D.pdf |
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