Headspace Single-Drop Microextraction Gas Chromatography Mass Spectrometry for the Analysis of Volatile Compounds from Herba Asari
A rapid headspace single-drop microextraction gas chromatography mass spectrometry (SDME-GC-MS) for the analysis of the volatile compounds in Herba Asari was developed in this study. The extraction solvent, extraction temperature and time, sample amount, and particle size were optimized. A mixed sol...
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| Format: | Article |
| Language: | English |
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Wiley
2013-01-01
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| Series: | Journal of Analytical Methods in Chemistry |
| Online Access: | http://dx.doi.org/10.1155/2013/380705 |
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| author | Guan-Jie Wang Li Tian Yu-Ming Fan Mei-Ling Qi |
| author_facet | Guan-Jie Wang Li Tian Yu-Ming Fan Mei-Ling Qi |
| author_sort | Guan-Jie Wang |
| collection | DOAJ |
| description | A rapid headspace single-drop microextraction gas chromatography mass spectrometry (SDME-GC-MS) for the analysis of the volatile compounds in Herba Asari was developed in this study. The extraction solvent, extraction temperature and time, sample amount, and particle size were optimized. A mixed solvent of n-tridecane and butyl acetate (1 : 1) was finally used for the extraction with sample amount of 0.750 g and 100-mesh particle size at 70°C for 15 min. Under the determined conditions, the pound samples of Herba Asari were directly applied for the analysis. The result showed that SDME-GC–MS method was a simple, effective, and inexpensive way to measure the volatile compounds in Herba Asari and could be used for the analysis of volatile compounds in Chinese medicine. |
| format | Article |
| id | doaj-art-838e560ea1b14e54b4b39247c29c7b15 |
| institution | OA Journals |
| issn | 2090-8865 2090-8873 |
| language | English |
| publishDate | 2013-01-01 |
| publisher | Wiley |
| record_format | Article |
| series | Journal of Analytical Methods in Chemistry |
| spelling | doaj-art-838e560ea1b14e54b4b39247c29c7b152025-08-20T02:09:01ZengWileyJournal of Analytical Methods in Chemistry2090-88652090-88732013-01-01201310.1155/2013/380705380705Headspace Single-Drop Microextraction Gas Chromatography Mass Spectrometry for the Analysis of Volatile Compounds from Herba AsariGuan-Jie Wang0Li Tian1Yu-Ming Fan2Mei-Ling Qi3National Institutes for Food and Drug Control, No. 2, Tiantan Xili, Beijing 100050, ChinaNational Institutes for Food and Drug Control, No. 2, Tiantan Xili, Beijing 100050, ChinaNational Institutes for Food and Drug Control, No. 2, Tiantan Xili, Beijing 100050, ChinaBeijing Institute of Technology, No. 5, Zhongguancun South Street, Haidian District, Beijing 100081, ChinaA rapid headspace single-drop microextraction gas chromatography mass spectrometry (SDME-GC-MS) for the analysis of the volatile compounds in Herba Asari was developed in this study. The extraction solvent, extraction temperature and time, sample amount, and particle size were optimized. A mixed solvent of n-tridecane and butyl acetate (1 : 1) was finally used for the extraction with sample amount of 0.750 g and 100-mesh particle size at 70°C for 15 min. Under the determined conditions, the pound samples of Herba Asari were directly applied for the analysis. The result showed that SDME-GC–MS method was a simple, effective, and inexpensive way to measure the volatile compounds in Herba Asari and could be used for the analysis of volatile compounds in Chinese medicine.http://dx.doi.org/10.1155/2013/380705 |
| spellingShingle | Guan-Jie Wang Li Tian Yu-Ming Fan Mei-Ling Qi Headspace Single-Drop Microextraction Gas Chromatography Mass Spectrometry for the Analysis of Volatile Compounds from Herba Asari Journal of Analytical Methods in Chemistry |
| title | Headspace Single-Drop Microextraction Gas Chromatography Mass Spectrometry for the Analysis of Volatile Compounds from Herba Asari |
| title_full | Headspace Single-Drop Microextraction Gas Chromatography Mass Spectrometry for the Analysis of Volatile Compounds from Herba Asari |
| title_fullStr | Headspace Single-Drop Microextraction Gas Chromatography Mass Spectrometry for the Analysis of Volatile Compounds from Herba Asari |
| title_full_unstemmed | Headspace Single-Drop Microextraction Gas Chromatography Mass Spectrometry for the Analysis of Volatile Compounds from Herba Asari |
| title_short | Headspace Single-Drop Microextraction Gas Chromatography Mass Spectrometry for the Analysis of Volatile Compounds from Herba Asari |
| title_sort | headspace single drop microextraction gas chromatography mass spectrometry for the analysis of volatile compounds from herba asari |
| url | http://dx.doi.org/10.1155/2013/380705 |
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