The Thermodynamic and Gelation Properties of Ovalbumin and Lysozyme

Ovalbumin (OVA) and lysozyme (LYZ) are the predominant globular proteins in egg white and play a crucial role in influencing thermal stability and colloidal behavior. In this study, the thermal and conformational stability of OVA and LYZ under various physicochemical conditions including pH (5–9), p...

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Main Authors: Lifeng Wang, Rongcheng Li, Siyi Lv, Yulin Liu, Shuaifu Fang, Jingnan Zang, Mingmin Qing, Yujie Chi
Format: Article
Language:English
Published: MDPI AG 2025-06-01
Series:Gels
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Online Access:https://www.mdpi.com/2310-2861/11/6/470
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author Lifeng Wang
Rongcheng Li
Siyi Lv
Yulin Liu
Shuaifu Fang
Jingnan Zang
Mingmin Qing
Yujie Chi
author_facet Lifeng Wang
Rongcheng Li
Siyi Lv
Yulin Liu
Shuaifu Fang
Jingnan Zang
Mingmin Qing
Yujie Chi
author_sort Lifeng Wang
collection DOAJ
description Ovalbumin (OVA) and lysozyme (LYZ) are the predominant globular proteins in egg white and play a crucial role in influencing thermal stability and colloidal behavior. In this study, the thermal and conformational stability of OVA and LYZ under various physicochemical conditions including pH (5–9), protein concentrations (5, 10, and 20%), heating rates (2.5, 5, and 10 °C/min), sugars (sucrose and glucose), and salts (NaCl, KCl, and CaCl<sub>2</sub>) was systematically investigated using differential scanning calorimetry (DSC), aiming to elucidate their behavior within colloidal and gel-forming systems. The denaturation temperatures (T<sub>d</sub>) of OVA and LYZ in water (5% <i>w</i>/<i>v</i>, 5 °C/min) were 80.22 °C and 77.46 °C, respectively. The T<sub>d</sub> of LYZ and OVA decreased with protein concentration, heating rate, and CaCl<sub>2</sub>. OVA thermal stability was improved with increasing pH, but the stability of LYZ was decreased. Sugars enhanced the thermal stability of OVA and LYZ. In contrast, NaCl and KCl increased OVA stability but reduced LYZ stability. LYZ exhibited nearly 100% reversibility during the second heating cycle in water. Sugars maintained reversibility at approximately 90% for LYZ. However, the presence of salts diminished the reversibility. In contrast, OVA was completely denatured in water and sugar and salt solutions.
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spelling doaj-art-831f4d0c86d74b928ed687031fee772c2025-08-20T03:24:36ZengMDPI AGGels2310-28612025-06-0111647010.3390/gels11060470The Thermodynamic and Gelation Properties of Ovalbumin and LysozymeLifeng Wang0Rongcheng Li1Siyi Lv2Yulin Liu3Shuaifu Fang4Jingnan Zang5Mingmin Qing6Yujie Chi7College of Food Science, Northeast Agricultural University, Harbin 150030, ChinaCollege of Food Science, Northeast Agricultural University, Harbin 150030, ChinaCollege of Food Science, Northeast Agricultural University, Harbin 150030, ChinaCollege of Food Science, Northeast Agricultural University, Harbin 150030, ChinaCollege of Food Science, Northeast Agricultural University, Harbin 150030, ChinaCollege of Food Science, Northeast Agricultural University, Harbin 150030, ChinaCollege of Food Science, Northeast Agricultural University, Harbin 150030, ChinaCollege of Food Science, Northeast Agricultural University, Harbin 150030, ChinaOvalbumin (OVA) and lysozyme (LYZ) are the predominant globular proteins in egg white and play a crucial role in influencing thermal stability and colloidal behavior. In this study, the thermal and conformational stability of OVA and LYZ under various physicochemical conditions including pH (5–9), protein concentrations (5, 10, and 20%), heating rates (2.5, 5, and 10 °C/min), sugars (sucrose and glucose), and salts (NaCl, KCl, and CaCl<sub>2</sub>) was systematically investigated using differential scanning calorimetry (DSC), aiming to elucidate their behavior within colloidal and gel-forming systems. The denaturation temperatures (T<sub>d</sub>) of OVA and LYZ in water (5% <i>w</i>/<i>v</i>, 5 °C/min) were 80.22 °C and 77.46 °C, respectively. The T<sub>d</sub> of LYZ and OVA decreased with protein concentration, heating rate, and CaCl<sub>2</sub>. OVA thermal stability was improved with increasing pH, but the stability of LYZ was decreased. Sugars enhanced the thermal stability of OVA and LYZ. In contrast, NaCl and KCl increased OVA stability but reduced LYZ stability. LYZ exhibited nearly 100% reversibility during the second heating cycle in water. Sugars maintained reversibility at approximately 90% for LYZ. However, the presence of salts diminished the reversibility. In contrast, OVA was completely denatured in water and sugar and salt solutions.https://www.mdpi.com/2310-2861/11/6/470DSCthermal denaturationovalbuminlysozymereversibility
spellingShingle Lifeng Wang
Rongcheng Li
Siyi Lv
Yulin Liu
Shuaifu Fang
Jingnan Zang
Mingmin Qing
Yujie Chi
The Thermodynamic and Gelation Properties of Ovalbumin and Lysozyme
Gels
DSC
thermal denaturation
ovalbumin
lysozyme
reversibility
title The Thermodynamic and Gelation Properties of Ovalbumin and Lysozyme
title_full The Thermodynamic and Gelation Properties of Ovalbumin and Lysozyme
title_fullStr The Thermodynamic and Gelation Properties of Ovalbumin and Lysozyme
title_full_unstemmed The Thermodynamic and Gelation Properties of Ovalbumin and Lysozyme
title_short The Thermodynamic and Gelation Properties of Ovalbumin and Lysozyme
title_sort thermodynamic and gelation properties of ovalbumin and lysozyme
topic DSC
thermal denaturation
ovalbumin
lysozyme
reversibility
url https://www.mdpi.com/2310-2861/11/6/470
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