Production and Optimization of Bio-Based Silica Nanoparticle from Teff Straw (Eragrostis tef) Using RSM-Based Modeling, Characterization Aspects, and Adsorption Efficacy of Methyl Orange Dye
The brown teff straw was utilized in this study to produce silica using the sol-gel technique. After pretreatment, the raw material of brown teff straw was characterized. The data were analyzed using the central composite design and response surface technique, and four independent parameters, namely...
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Wiley
2022-01-01
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| Series: | Journal of Chemistry |
| Online Access: | http://dx.doi.org/10.1155/2022/9770520 |
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| author | Temesgen Abeto Amibo Surafel Mustefa Beyan Tsegaye Markos Damite |
| author_facet | Temesgen Abeto Amibo Surafel Mustefa Beyan Tsegaye Markos Damite |
| author_sort | Temesgen Abeto Amibo |
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| description | The brown teff straw was utilized in this study to produce silica using the sol-gel technique. After pretreatment, the raw material of brown teff straw was characterized. The data were analyzed using the central composite design and response surface technique, and four independent parameters, namely, temperature, NaOH concentration, rotational speed, and extraction time, were evaluated for process optimization. Before extracting silica with an alkaline solution, the silica content in the ash was determined using an AAS spectrometer. The silica content of teff straw ash is around 92.89%. The ash was treated with NaOH solution in the concentrations range of 1 M to 3 M (0.5 M interval). The extraction time varied at intervals of 55, 70, 85, 100, and 115 minutes. Temperatures were changed using magnetic stirrer equipment in the range of 80°C to 100°C (5°C interval). At 350 rpm, 400 rpm, 450 rpm, 500 rpm, and 550 rpm, the rotating speed was adjusted. The best extraction conditions for amorphous silica were 1.50 M NaOH, 109.99 min, 94.98°C, and a rotating speed of 499.57 rpm, with a maximum yield of 85.85%. XRD and FTIR analyses were used to assess the physicochemical characteristics of the extracted silica. The aqueous solutions of methyl orange were used to test the adsorption efficiency of silica. The percent of removal efficiency for methyl orange was 90.48%. |
| format | Article |
| id | doaj-art-828eccb156b84217be3ad5f62f611301 |
| institution | Kabale University |
| issn | 2090-9071 |
| language | English |
| publishDate | 2022-01-01 |
| publisher | Wiley |
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| series | Journal of Chemistry |
| spelling | doaj-art-828eccb156b84217be3ad5f62f6113012025-02-03T01:25:21ZengWileyJournal of Chemistry2090-90712022-01-01202210.1155/2022/9770520Production and Optimization of Bio-Based Silica Nanoparticle from Teff Straw (Eragrostis tef) Using RSM-Based Modeling, Characterization Aspects, and Adsorption Efficacy of Methyl Orange DyeTemesgen Abeto Amibo0Surafel Mustefa Beyan1Tsegaye Markos Damite2School of Chemical EngineeringSchool of Chemical EngineeringFaculty of Material Science and EngineeringThe brown teff straw was utilized in this study to produce silica using the sol-gel technique. After pretreatment, the raw material of brown teff straw was characterized. The data were analyzed using the central composite design and response surface technique, and four independent parameters, namely, temperature, NaOH concentration, rotational speed, and extraction time, were evaluated for process optimization. Before extracting silica with an alkaline solution, the silica content in the ash was determined using an AAS spectrometer. The silica content of teff straw ash is around 92.89%. The ash was treated with NaOH solution in the concentrations range of 1 M to 3 M (0.5 M interval). The extraction time varied at intervals of 55, 70, 85, 100, and 115 minutes. Temperatures were changed using magnetic stirrer equipment in the range of 80°C to 100°C (5°C interval). At 350 rpm, 400 rpm, 450 rpm, 500 rpm, and 550 rpm, the rotating speed was adjusted. The best extraction conditions for amorphous silica were 1.50 M NaOH, 109.99 min, 94.98°C, and a rotating speed of 499.57 rpm, with a maximum yield of 85.85%. XRD and FTIR analyses were used to assess the physicochemical characteristics of the extracted silica. The aqueous solutions of methyl orange were used to test the adsorption efficiency of silica. The percent of removal efficiency for methyl orange was 90.48%.http://dx.doi.org/10.1155/2022/9770520 |
| spellingShingle | Temesgen Abeto Amibo Surafel Mustefa Beyan Tsegaye Markos Damite Production and Optimization of Bio-Based Silica Nanoparticle from Teff Straw (Eragrostis tef) Using RSM-Based Modeling, Characterization Aspects, and Adsorption Efficacy of Methyl Orange Dye Journal of Chemistry |
| title | Production and Optimization of Bio-Based Silica Nanoparticle from Teff Straw (Eragrostis tef) Using RSM-Based Modeling, Characterization Aspects, and Adsorption Efficacy of Methyl Orange Dye |
| title_full | Production and Optimization of Bio-Based Silica Nanoparticle from Teff Straw (Eragrostis tef) Using RSM-Based Modeling, Characterization Aspects, and Adsorption Efficacy of Methyl Orange Dye |
| title_fullStr | Production and Optimization of Bio-Based Silica Nanoparticle from Teff Straw (Eragrostis tef) Using RSM-Based Modeling, Characterization Aspects, and Adsorption Efficacy of Methyl Orange Dye |
| title_full_unstemmed | Production and Optimization of Bio-Based Silica Nanoparticle from Teff Straw (Eragrostis tef) Using RSM-Based Modeling, Characterization Aspects, and Adsorption Efficacy of Methyl Orange Dye |
| title_short | Production and Optimization of Bio-Based Silica Nanoparticle from Teff Straw (Eragrostis tef) Using RSM-Based Modeling, Characterization Aspects, and Adsorption Efficacy of Methyl Orange Dye |
| title_sort | production and optimization of bio based silica nanoparticle from teff straw eragrostis tef using rsm based modeling characterization aspects and adsorption efficacy of methyl orange dye |
| url | http://dx.doi.org/10.1155/2022/9770520 |
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