Improving the accuracy of determining corrosion products in reinforced concrete structures by atomic emission spectrum analysis

To determine the composition of inhomogeneous samples using the method of laser-spark emission spectrometry, calibration dependences are used, which can have significant systematic errors that significantly affect the determination of the quantitative composition of elements. Sample inhomogeneity...

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Main Authors: A. A. Kuznetsov, N. V. Volkova, K. I. Fomichenko, D. M. Korshunov
Format: Article
Language:English
Published: Omsk State Technical University, Federal State Autonoumos Educational Institution of Higher Education 2023-09-01
Series:Омский научный вестник
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Online Access:https://www.omgtu.ru/general_information/media_omgtu/journal_of_omsk_research_journal/files/arhiv/2023/%E2%84%963%20(187)%20(%D0%9E%D0%9D%D0%92)/125-130%20%D0%9A%D1%83%D0%B7%D0%BD%D0%B5%D1%86%D0%BE%D0%B2%20%D0%90.%20%D0%90.,%20%20%D0%92%D0%BE%D0%BB%D0%BA%D0%BE%D0%B2%D0%B0%20%D0%9D.%20%D0%92.,%20%D0%A4%D0%BE%D0%BC%D0%B8%D1%87%D0%B5%D0%BD%D0%BA%D0%BE%20%D0%9A.%20%D0%98.,%20%D0%9A%D0%BE%D1%80%D1%88%D1%83%D0%BD%D0%BE%D0%B2%20%D0%94.%20%D0%9C..pdf
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author A. A. Kuznetsov
N. V. Volkova
K. I. Fomichenko
D. M. Korshunov
author_facet A. A. Kuznetsov
N. V. Volkova
K. I. Fomichenko
D. M. Korshunov
author_sort A. A. Kuznetsov
collection DOAJ
description To determine the composition of inhomogeneous samples using the method of laser-spark emission spectrometry, calibration dependences are used, which can have significant systematic errors that significantly affect the determination of the quantitative composition of elements. Sample inhomogeneity also causes inaccuracies in replicate measurements. To reduce errors, multi-signal calibration and internal standard methods are used, which can significantly improve accuracy when changing experimental conditions and eliminate the need to purchase ex-pensive standard samples.
format Article
id doaj-art-80d06448880a4872b6b6e15487dcf812
institution Kabale University
issn 1813-8225
2541-7541
language English
publishDate 2023-09-01
publisher Omsk State Technical University, Federal State Autonoumos Educational Institution of Higher Education
record_format Article
series Омский научный вестник
spelling doaj-art-80d06448880a4872b6b6e15487dcf8122025-02-03T00:33:33ZengOmsk State Technical University, Federal State Autonoumos Educational Institution of Higher EducationОмский научный вестник1813-82252541-75412023-09-013 (187)12513010.25206/1813-8225-2023-187-125-130Improving the accuracy of determining corrosion products in reinforced concrete structures by atomic emission spectrum analysisA. A. Kuznetsov0https://orcid.org/0000-0002-1815-4679N. V. Volkova1https://orcid.org/0000-0003-4645-9661K. I. Fomichenko2https://orcid.org/0000-0001-5836-2395D. M. Korshunov3https://orcid.org/0000-0002-8500-7193Omsk State Transport UniversityOmsk State Transport UniversityOmsk State Transport UniversityLomonosov Moscow State UniversityTo determine the composition of inhomogeneous samples using the method of laser-spark emission spectrometry, calibration dependences are used, which can have significant systematic errors that significantly affect the determination of the quantitative composition of elements. Sample inhomogeneity also causes inaccuracies in replicate measurements. To reduce errors, multi-signal calibration and internal standard methods are used, which can significantly improve accuracy when changing experimental conditions and eliminate the need to purchase ex-pensive standard samples.https://www.omgtu.ru/general_information/media_omgtu/journal_of_omsk_research_journal/files/arhiv/2023/%E2%84%963%20(187)%20(%D0%9E%D0%9D%D0%92)/125-130%20%D0%9A%D1%83%D0%B7%D0%BD%D0%B5%D1%86%D0%BE%D0%B2%20%D0%90.%20%D0%90.,%20%20%D0%92%D0%BE%D0%BB%D0%BA%D0%BE%D0%B2%D0%B0%20%D0%9D.%20%D0%92.,%20%D0%A4%D0%BE%D0%BC%D0%B8%D1%87%D0%B5%D0%BD%D0%BA%D0%BE%20%D0%9A.%20%D0%98.,%20%D0%9A%D0%BE%D1%80%D1%88%D1%83%D0%BD%D0%BE%D0%B2%20%D0%94.%20%D0%9C..pdfconcretecorrosion productsatomic emission spectral analysislaserinduced breakdown spectroscopycalibration grapherror componentsstable calibration function
spellingShingle A. A. Kuznetsov
N. V. Volkova
K. I. Fomichenko
D. M. Korshunov
Improving the accuracy of determining corrosion products in reinforced concrete structures by atomic emission spectrum analysis
Омский научный вестник
concrete
corrosion products
atomic emission spectral analysis
laserinduced breakdown spectroscopy
calibration graph
error components
stable calibration function
title Improving the accuracy of determining corrosion products in reinforced concrete structures by atomic emission spectrum analysis
title_full Improving the accuracy of determining corrosion products in reinforced concrete structures by atomic emission spectrum analysis
title_fullStr Improving the accuracy of determining corrosion products in reinforced concrete structures by atomic emission spectrum analysis
title_full_unstemmed Improving the accuracy of determining corrosion products in reinforced concrete structures by atomic emission spectrum analysis
title_short Improving the accuracy of determining corrosion products in reinforced concrete structures by atomic emission spectrum analysis
title_sort improving the accuracy of determining corrosion products in reinforced concrete structures by atomic emission spectrum analysis
topic concrete
corrosion products
atomic emission spectral analysis
laserinduced breakdown spectroscopy
calibration graph
error components
stable calibration function
url https://www.omgtu.ru/general_information/media_omgtu/journal_of_omsk_research_journal/files/arhiv/2023/%E2%84%963%20(187)%20(%D0%9E%D0%9D%D0%92)/125-130%20%D0%9A%D1%83%D0%B7%D0%BD%D0%B5%D1%86%D0%BE%D0%B2%20%D0%90.%20%D0%90.,%20%20%D0%92%D0%BE%D0%BB%D0%BA%D0%BE%D0%B2%D0%B0%20%D0%9D.%20%D0%92.,%20%D0%A4%D0%BE%D0%BC%D0%B8%D1%87%D0%B5%D0%BD%D0%BA%D0%BE%20%D0%9A.%20%D0%98.,%20%D0%9A%D0%BE%D1%80%D1%88%D1%83%D0%BD%D0%BE%D0%B2%20%D0%94.%20%D0%9C..pdf
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