Nanocrystalline Al Composites from Powder Milled under Ammonia Gas Flow

The production of high hardness and thermally stable nanocrystalline aluminium composites is described. Al powder was milled at room temperature in an ammonia flow for a period of less than 5 h. NH3 dissociation during milling provokes the absorption, at a high rate, of nitrogen into aluminium, hard...

Full description

Saved in:
Bibliographic Details
Main Authors: J. Cintas, E. S. Caballero, J. M. Montes, F. G. Cuevas, C. Arevalo
Format: Article
Language:English
Published: Wiley 2014-01-01
Series:Advances in Materials Science and Engineering
Online Access:http://dx.doi.org/10.1155/2014/617241
Tags: Add Tag
No Tags, Be the first to tag this record!
_version_ 1832567178558177280
author J. Cintas
E. S. Caballero
J. M. Montes
F. G. Cuevas
C. Arevalo
author_facet J. Cintas
E. S. Caballero
J. M. Montes
F. G. Cuevas
C. Arevalo
author_sort J. Cintas
collection DOAJ
description The production of high hardness and thermally stable nanocrystalline aluminium composites is described. Al powder was milled at room temperature in an ammonia flow for a period of less than 5 h. NH3 dissociation during milling provokes the absorption, at a high rate, of nitrogen into aluminium, hardening it by forming a solid solution. Controlled amounts of AlN and Al5O6N are formed during the subsequent sintering of milled powders for consolidation. The pinning action of these abundant dispersoids highly restrains aluminium grain growth during heating. The mean size of the Al grains remains below 45 nm and even after the milled powder is sintered at 650°C for 1 h.
format Article
id doaj-art-7ded347dc11f425f8e41a30b128a1c15
institution Kabale University
issn 1687-8434
1687-8442
language English
publishDate 2014-01-01
publisher Wiley
record_format Article
series Advances in Materials Science and Engineering
spelling doaj-art-7ded347dc11f425f8e41a30b128a1c152025-02-03T01:02:10ZengWileyAdvances in Materials Science and Engineering1687-84341687-84422014-01-01201410.1155/2014/617241617241Nanocrystalline Al Composites from Powder Milled under Ammonia Gas FlowJ. Cintas0E. S. Caballero1J. M. Montes2F. G. Cuevas3C. Arevalo4Metallurgy and Materials Engineering Group, Escuela Técnica Superior de Ingeniería, University of Seville, Camino de los Descubrimientos s/n, 41092 Sevilla, SpainMetallurgy and Materials Engineering Group, Escuela Técnica Superior de Ingeniería, University of Seville, Camino de los Descubrimientos s/n, 41092 Sevilla, SpainMetallurgy and Materials Engineering Group, Escuela Técnica Superior de Ingeniería, University of Seville, Camino de los Descubrimientos s/n, 41092 Sevilla, SpainDepartment of Chemistry and Materials Science, Escuela Técnica Superior de Ingeniería, University of Huelva, Campus La Rábida, Carretera Palos s/n, Palos de la Frontera, 21819 Huelva, SpainMetallurgy and Materials Engineering Group, Escuela Técnica Superior de Ingeniería, University of Seville, Camino de los Descubrimientos s/n, 41092 Sevilla, SpainThe production of high hardness and thermally stable nanocrystalline aluminium composites is described. Al powder was milled at room temperature in an ammonia flow for a period of less than 5 h. NH3 dissociation during milling provokes the absorption, at a high rate, of nitrogen into aluminium, hardening it by forming a solid solution. Controlled amounts of AlN and Al5O6N are formed during the subsequent sintering of milled powders for consolidation. The pinning action of these abundant dispersoids highly restrains aluminium grain growth during heating. The mean size of the Al grains remains below 45 nm and even after the milled powder is sintered at 650°C for 1 h.http://dx.doi.org/10.1155/2014/617241
spellingShingle J. Cintas
E. S. Caballero
J. M. Montes
F. G. Cuevas
C. Arevalo
Nanocrystalline Al Composites from Powder Milled under Ammonia Gas Flow
Advances in Materials Science and Engineering
title Nanocrystalline Al Composites from Powder Milled under Ammonia Gas Flow
title_full Nanocrystalline Al Composites from Powder Milled under Ammonia Gas Flow
title_fullStr Nanocrystalline Al Composites from Powder Milled under Ammonia Gas Flow
title_full_unstemmed Nanocrystalline Al Composites from Powder Milled under Ammonia Gas Flow
title_short Nanocrystalline Al Composites from Powder Milled under Ammonia Gas Flow
title_sort nanocrystalline al composites from powder milled under ammonia gas flow
url http://dx.doi.org/10.1155/2014/617241
work_keys_str_mv AT jcintas nanocrystallinealcompositesfrompowdermilledunderammoniagasflow
AT escaballero nanocrystallinealcompositesfrompowdermilledunderammoniagasflow
AT jmmontes nanocrystallinealcompositesfrompowdermilledunderammoniagasflow
AT fgcuevas nanocrystallinealcompositesfrompowdermilledunderammoniagasflow
AT carevalo nanocrystallinealcompositesfrompowdermilledunderammoniagasflow