Effect of CNT-COOH Addition on the Compressive Strength, Chloride Resistance, and Microstructure of Cement Mortar

This work evaluated the effect of multiwalled carboxyl carbon nanotube (CNT-COOH), upon cement mortar. In order to obtain a homogeneous suspension, the CNT-COOH was dispersed in distilled water, and it then underwent an ultrasonication treatment. Samples of cement mortar were prepared with varying t...

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Main Authors: Xiaofan Wang, Yao Shi, Xueyang Pei, Lipeng Cui, Hua Zhu
Format: Article
Language:English
Published: Wiley 2022-01-01
Series:Advances in Materials Science and Engineering
Online Access:http://dx.doi.org/10.1155/2022/3345279
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author Xiaofan Wang
Yao Shi
Xueyang Pei
Lipeng Cui
Hua Zhu
author_facet Xiaofan Wang
Yao Shi
Xueyang Pei
Lipeng Cui
Hua Zhu
author_sort Xiaofan Wang
collection DOAJ
description This work evaluated the effect of multiwalled carboxyl carbon nanotube (CNT-COOH), upon cement mortar. In order to obtain a homogeneous suspension, the CNT-COOH was dispersed in distilled water, and it then underwent an ultrasonication treatment. Samples of cement mortar were prepared with varying the additions of this suspension at 0.01%, 0.05%, and 0.10% by weight of the cement. These samples were tested in compression and for chloride migration in terms of diffusion coefficient. An increase in the CNT-COOH content led to an increase in the compressive strength. While there was an increase in the chloride diffusion coefficient up to 0.05% weight fraction, higher dosage led to a drop in the chloride diffusion coefficient with a further increase in the compressive strength. Using mercury intrusion porosimetry (MIP), it is shown that at a weight fraction of 0.10%, CNT-COOH effects a pore-size refinement by eliminating macropores (≥50 nm) and a 34% reduction in porosity. The (scanning electron microscopy) SEM and (X-ray diffraction) XRD analyses confirm that CNT-COOH leads to mature hydration products, nucleation effect, and a refined microstructure.
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spelling doaj-art-7de204e869d04dad948e95e083e9d2c12025-02-03T01:32:34ZengWileyAdvances in Materials Science and Engineering1687-84422022-01-01202210.1155/2022/3345279Effect of CNT-COOH Addition on the Compressive Strength, Chloride Resistance, and Microstructure of Cement MortarXiaofan Wang0Yao Shi1Xueyang Pei2Lipeng Cui3Hua Zhu4College of Civil EngineeringCCCC Second Harbour Engineering Company Design & Research Institute Co. LtdCollege of Civil EngineeringThe First Project of the China Railway Construction Group LimitedCollege of Civil EngineeringThis work evaluated the effect of multiwalled carboxyl carbon nanotube (CNT-COOH), upon cement mortar. In order to obtain a homogeneous suspension, the CNT-COOH was dispersed in distilled water, and it then underwent an ultrasonication treatment. Samples of cement mortar were prepared with varying the additions of this suspension at 0.01%, 0.05%, and 0.10% by weight of the cement. These samples were tested in compression and for chloride migration in terms of diffusion coefficient. An increase in the CNT-COOH content led to an increase in the compressive strength. While there was an increase in the chloride diffusion coefficient up to 0.05% weight fraction, higher dosage led to a drop in the chloride diffusion coefficient with a further increase in the compressive strength. Using mercury intrusion porosimetry (MIP), it is shown that at a weight fraction of 0.10%, CNT-COOH effects a pore-size refinement by eliminating macropores (≥50 nm) and a 34% reduction in porosity. The (scanning electron microscopy) SEM and (X-ray diffraction) XRD analyses confirm that CNT-COOH leads to mature hydration products, nucleation effect, and a refined microstructure.http://dx.doi.org/10.1155/2022/3345279
spellingShingle Xiaofan Wang
Yao Shi
Xueyang Pei
Lipeng Cui
Hua Zhu
Effect of CNT-COOH Addition on the Compressive Strength, Chloride Resistance, and Microstructure of Cement Mortar
Advances in Materials Science and Engineering
title Effect of CNT-COOH Addition on the Compressive Strength, Chloride Resistance, and Microstructure of Cement Mortar
title_full Effect of CNT-COOH Addition on the Compressive Strength, Chloride Resistance, and Microstructure of Cement Mortar
title_fullStr Effect of CNT-COOH Addition on the Compressive Strength, Chloride Resistance, and Microstructure of Cement Mortar
title_full_unstemmed Effect of CNT-COOH Addition on the Compressive Strength, Chloride Resistance, and Microstructure of Cement Mortar
title_short Effect of CNT-COOH Addition on the Compressive Strength, Chloride Resistance, and Microstructure of Cement Mortar
title_sort effect of cnt cooh addition on the compressive strength chloride resistance and microstructure of cement mortar
url http://dx.doi.org/10.1155/2022/3345279
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AT lipengcui effectofcntcoohadditiononthecompressivestrengthchlorideresistanceandmicrostructureofcementmortar
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