Enhanced strength and reduced elastic modulus of biomedical metastable β Ti–Nb alloy via intermediate phase transformation

The high strength of biomedical titanium alloys is primarily attained through precipitation strengthening of the α phase. However, the plasticity and elastic modulus of these alloys are often limited due to their inherent strength–toughness tradeoff and the high-modulus α phase. Metastable β-type Ti...

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Main Authors: Meng Qiang, Xi-rong Yang, Geng-jie Wang, Xiao-yan Liu, Lei Luo, Qun Ren, Jing-zhong Wang
Format: Article
Language:English
Published: Elsevier 2025-03-01
Series:Materials & Design
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Online Access:http://www.sciencedirect.com/science/article/pii/S0264127525000826
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author Meng Qiang
Xi-rong Yang
Geng-jie Wang
Xiao-yan Liu
Lei Luo
Qun Ren
Jing-zhong Wang
author_facet Meng Qiang
Xi-rong Yang
Geng-jie Wang
Xiao-yan Liu
Lei Luo
Qun Ren
Jing-zhong Wang
author_sort Meng Qiang
collection DOAJ
description The high strength of biomedical titanium alloys is primarily attained through precipitation strengthening of the α phase. However, the plasticity and elastic modulus of these alloys are often limited due to their inherent strength–toughness tradeoff and the high-modulus α phase. Metastable β-type Ti–Nb alloys were subjected to equal-channel angular pressing (ECAP) deformation and aging treatment in this study. The lattice defects and high distortion induced by the deformation can provide nucleation sites and drive the precipitation during aging, as well as hinder the dissolution of the low-modulus stress-induced martensitic (SIM) α′′ phase introduced during the deformation, which results in the formation of fine and dispersed nanosized intermediate phases (α + ω + α′′) after short-term aging. As a result, a Ti–Nb alloy with a high strength (∼1021 MPa), low elastic modulus (∼59 GPa), and good elongation (∼12 %) is obtained. Furthermore, the competition between the ω and α phases is observed. The comprehensive mechanical properties of the alloy prepared by ECAP deformation combined with aging treatment in this study surpasses those of many reported titanium alloys prepared by traditional deformation or thermal treatment, which provides a valuable reference for the production of advanced biomedical titanium alloys.
format Article
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institution Kabale University
issn 0264-1275
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publishDate 2025-03-01
publisher Elsevier
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series Materials & Design
spelling doaj-art-7d08ae652a744e4ab7315cc3f96690542025-01-31T05:10:04ZengElsevierMaterials & Design0264-12752025-03-01251113662Enhanced strength and reduced elastic modulus of biomedical metastable β Ti–Nb alloy via intermediate phase transformationMeng Qiang0Xi-rong Yang1Geng-jie Wang2Xiao-yan Liu3Lei Luo4Qun Ren5Jing-zhong Wang6School of Metallurgical Engineering, Xi’an University of Architecture and Technology, Xi’an 710055 ChinaSchool of Metallurgical Engineering, Xi’an University of Architecture and Technology, Xi’an 710055 China; National Experimental Teaching Demonstration Center of Metallurgical Technology, Xi’an 710055 China; Corresponding author at: School of Metallurgical Engineering, Xi’an University of Architecture and Technology, Xi’an 710055, China.State Key Laboratory for Mechanical Behavior of Materials, School of Materials Science and Engineering, Xi’an Jiaotong University, Xi’an 710049 ChinaSchool of Metallurgical Engineering, Xi’an University of Architecture and Technology, Xi’an 710055 ChinaSchool of Metallurgical Engineering, Xi’an University of Architecture and Technology, Xi’an 710055 ChinaSchool of Metallurgical Engineering, Xi’an University of Architecture and Technology, Xi’an 710055 ChinaSchool of Metallurgical Engineering, Xi’an University of Architecture and Technology, Xi’an 710055 ChinaThe high strength of biomedical titanium alloys is primarily attained through precipitation strengthening of the α phase. However, the plasticity and elastic modulus of these alloys are often limited due to their inherent strength–toughness tradeoff and the high-modulus α phase. Metastable β-type Ti–Nb alloys were subjected to equal-channel angular pressing (ECAP) deformation and aging treatment in this study. The lattice defects and high distortion induced by the deformation can provide nucleation sites and drive the precipitation during aging, as well as hinder the dissolution of the low-modulus stress-induced martensitic (SIM) α′′ phase introduced during the deformation, which results in the formation of fine and dispersed nanosized intermediate phases (α + ω + α′′) after short-term aging. As a result, a Ti–Nb alloy with a high strength (∼1021 MPa), low elastic modulus (∼59 GPa), and good elongation (∼12 %) is obtained. Furthermore, the competition between the ω and α phases is observed. The comprehensive mechanical properties of the alloy prepared by ECAP deformation combined with aging treatment in this study surpasses those of many reported titanium alloys prepared by traditional deformation or thermal treatment, which provides a valuable reference for the production of advanced biomedical titanium alloys.http://www.sciencedirect.com/science/article/pii/S0264127525000826Ti–Nb alloyEqual-channel angular pressing deformationStress-induced martensitePrecipitated phaseElastic modulus
spellingShingle Meng Qiang
Xi-rong Yang
Geng-jie Wang
Xiao-yan Liu
Lei Luo
Qun Ren
Jing-zhong Wang
Enhanced strength and reduced elastic modulus of biomedical metastable β Ti–Nb alloy via intermediate phase transformation
Materials & Design
Ti–Nb alloy
Equal-channel angular pressing deformation
Stress-induced martensite
Precipitated phase
Elastic modulus
title Enhanced strength and reduced elastic modulus of biomedical metastable β Ti–Nb alloy via intermediate phase transformation
title_full Enhanced strength and reduced elastic modulus of biomedical metastable β Ti–Nb alloy via intermediate phase transformation
title_fullStr Enhanced strength and reduced elastic modulus of biomedical metastable β Ti–Nb alloy via intermediate phase transformation
title_full_unstemmed Enhanced strength and reduced elastic modulus of biomedical metastable β Ti–Nb alloy via intermediate phase transformation
title_short Enhanced strength and reduced elastic modulus of biomedical metastable β Ti–Nb alloy via intermediate phase transformation
title_sort enhanced strength and reduced elastic modulus of biomedical metastable β ti nb alloy via intermediate phase transformation
topic Ti–Nb alloy
Equal-channel angular pressing deformation
Stress-induced martensite
Precipitated phase
Elastic modulus
url http://www.sciencedirect.com/science/article/pii/S0264127525000826
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