Combustion Synthesis of Fe-Incorporated SnO2 Nanoparticles Using Organometallic Precursor Combination
Synthesis of nanomaterials within flames has been demonstrated as a highly scalable and versatile approach for obtaining a variety of nanoparticles with respect to their chemistry, composition, size, morphology, and dimensionality. Its applicability can be amplified by exploring new material systems...
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| Main Authors: | , , , |
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| Format: | Article |
| Language: | English |
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Wiley
2012-01-01
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| Series: | Advances in Materials Science and Engineering |
| Online Access: | http://dx.doi.org/10.1155/2012/685754 |
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| _version_ | 1832546538612588544 |
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| author | Thomas K. Barkley Jenna E. Vastano James R. Applegate Smitesh D. Bakrania |
| author_facet | Thomas K. Barkley Jenna E. Vastano James R. Applegate Smitesh D. Bakrania |
| author_sort | Thomas K. Barkley |
| collection | DOAJ |
| description | Synthesis of nanomaterials within flames has been demonstrated as a highly scalable and versatile approach for obtaining a variety of nanoparticles with respect to their chemistry, composition, size, morphology, and dimensionality. Its applicability can be amplified by exploring new material systems and providing further control over the particle characteristics. This study focused on iron-incorporated SnO2 nanoparticles generated using an inverse coflow diffusion flame burner that supported a near-stoichiometric methane-air combustion. A liquid organometallic precursor solution of Sn(CH3)4 and Fe(CO)5 was used to produce 11–14 nm nanocrystalline particles. Synthesized particles were analyzed using TEM, XRD, and XEDS to characterize for size and composition. A flame temperature field was obtained to map particle evolution within the flame. A range of conditions and parameters were studied to specifically generate targeted particles. The study augments related research towards increasing the production potential of combustion synthesis. |
| format | Article |
| id | doaj-art-76c1398ea0384d5286fd81490682b255 |
| institution | Kabale University |
| issn | 1687-8434 1687-8442 |
| language | English |
| publishDate | 2012-01-01 |
| publisher | Wiley |
| record_format | Article |
| series | Advances in Materials Science and Engineering |
| spelling | doaj-art-76c1398ea0384d5286fd81490682b2552025-02-03T06:48:38ZengWileyAdvances in Materials Science and Engineering1687-84341687-84422012-01-01201210.1155/2012/685754685754Combustion Synthesis of Fe-Incorporated SnO2 Nanoparticles Using Organometallic Precursor CombinationThomas K. Barkley0Jenna E. Vastano1James R. Applegate2Smitesh D. Bakrania3Department of Mechanical Engineering, Rowan University, 201 Mullica Hill Road, Glassboro, NJ 08028, USADepartment of Mechanical Engineering, Rowan University, 201 Mullica Hill Road, Glassboro, NJ 08028, USADepartment of Mechanical Engineering, Rowan University, 201 Mullica Hill Road, Glassboro, NJ 08028, USADepartment of Mechanical Engineering, Rowan University, 201 Mullica Hill Road, Glassboro, NJ 08028, USASynthesis of nanomaterials within flames has been demonstrated as a highly scalable and versatile approach for obtaining a variety of nanoparticles with respect to their chemistry, composition, size, morphology, and dimensionality. Its applicability can be amplified by exploring new material systems and providing further control over the particle characteristics. This study focused on iron-incorporated SnO2 nanoparticles generated using an inverse coflow diffusion flame burner that supported a near-stoichiometric methane-air combustion. A liquid organometallic precursor solution of Sn(CH3)4 and Fe(CO)5 was used to produce 11–14 nm nanocrystalline particles. Synthesized particles were analyzed using TEM, XRD, and XEDS to characterize for size and composition. A flame temperature field was obtained to map particle evolution within the flame. A range of conditions and parameters were studied to specifically generate targeted particles. The study augments related research towards increasing the production potential of combustion synthesis.http://dx.doi.org/10.1155/2012/685754 |
| spellingShingle | Thomas K. Barkley Jenna E. Vastano James R. Applegate Smitesh D. Bakrania Combustion Synthesis of Fe-Incorporated SnO2 Nanoparticles Using Organometallic Precursor Combination Advances in Materials Science and Engineering |
| title | Combustion Synthesis of Fe-Incorporated SnO2 Nanoparticles Using Organometallic Precursor Combination |
| title_full | Combustion Synthesis of Fe-Incorporated SnO2 Nanoparticles Using Organometallic Precursor Combination |
| title_fullStr | Combustion Synthesis of Fe-Incorporated SnO2 Nanoparticles Using Organometallic Precursor Combination |
| title_full_unstemmed | Combustion Synthesis of Fe-Incorporated SnO2 Nanoparticles Using Organometallic Precursor Combination |
| title_short | Combustion Synthesis of Fe-Incorporated SnO2 Nanoparticles Using Organometallic Precursor Combination |
| title_sort | combustion synthesis of fe incorporated sno2 nanoparticles using organometallic precursor combination |
| url | http://dx.doi.org/10.1155/2012/685754 |
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