Determination of Progestin Residues in Fish by UPLC-Q-TOF/MS Coupled with QuEChERS
A novel method was developed for simultaneous determination of 10 progestin residues in fish by ultra-performance liquid chromatography-quadrupole-time-of-flight mass spectrometry (UPLC-Q-TOF/MS) combined with a modified quick, easy, cheap, effective, rugged, and safe (QuEChERS) method. The homogeni...
Saved in:
| Main Authors: | , , , , |
|---|---|
| Format: | Article |
| Language: | English |
| Published: |
Wiley
2019-01-01
|
| Series: | Journal of Analytical Methods in Chemistry |
| Online Access: | http://dx.doi.org/10.1155/2019/6426958 |
| Tags: |
Add Tag
No Tags, Be the first to tag this record!
|
| _version_ | 1832550078353506304 |
|---|---|
| author | Chunxiu Gu Yanling Cheng Xin Zhen Xiaoxuan Chen Kaowen Zhou |
| author_facet | Chunxiu Gu Yanling Cheng Xin Zhen Xiaoxuan Chen Kaowen Zhou |
| author_sort | Chunxiu Gu |
| collection | DOAJ |
| description | A novel method was developed for simultaneous determination of 10 progestin residues in fish by ultra-performance liquid chromatography-quadrupole-time-of-flight mass spectrometry (UPLC-Q-TOF/MS) combined with a modified quick, easy, cheap, effective, rugged, and safe (QuEChERS) method. The homogenized samples were dispersed by water, extracted with acetonitrile, and then purified by QuEChERS reagent. The concentrated analytes were detected by UPLC-Q-TOF/MS. High linearities (R2 > 0.995) and recoveries (85.71–117.08%) at three spiked levels (5, 10, and 20 ng/g) and low relative standard deviation values (<8.83%, n = 7) and limits of detection (0.23–0.66 ng/g) were obtained. This method is simple, rapid, reliable, sensitive, and efficient and can be used for monitoring of progestin residues in fish. This method provides a strong guarantee to deal with food emergencies for the laboratory, provides technical support for the screening and quantitative detection of progesterone in fish, and provides technical support for the food safety of aquatic products. |
| format | Article |
| id | doaj-art-7458d5104e164ea28490518e59a033be |
| institution | Kabale University |
| issn | 2090-8865 2090-8873 |
| language | English |
| publishDate | 2019-01-01 |
| publisher | Wiley |
| record_format | Article |
| series | Journal of Analytical Methods in Chemistry |
| spelling | doaj-art-7458d5104e164ea28490518e59a033be2025-02-03T06:07:45ZengWileyJournal of Analytical Methods in Chemistry2090-88652090-88732019-01-01201910.1155/2019/64269586426958Determination of Progestin Residues in Fish by UPLC-Q-TOF/MS Coupled with QuEChERSChunxiu Gu0Yanling Cheng1Xin Zhen2Xiaoxuan Chen3Kaowen Zhou4Biochemical Engineering College, Beijing Union University, Beijing 100023, ChinaBiochemical Engineering College, Beijing Union University, Beijing 100023, ChinaBiochemical Engineering College, Beijing Union University, Beijing 100023, ChinaBiochemical Engineering College, Beijing Union University, Beijing 100023, ChinaBiochemical Engineering College, Beijing Union University, Beijing 100023, ChinaA novel method was developed for simultaneous determination of 10 progestin residues in fish by ultra-performance liquid chromatography-quadrupole-time-of-flight mass spectrometry (UPLC-Q-TOF/MS) combined with a modified quick, easy, cheap, effective, rugged, and safe (QuEChERS) method. The homogenized samples were dispersed by water, extracted with acetonitrile, and then purified by QuEChERS reagent. The concentrated analytes were detected by UPLC-Q-TOF/MS. High linearities (R2 > 0.995) and recoveries (85.71–117.08%) at three spiked levels (5, 10, and 20 ng/g) and low relative standard deviation values (<8.83%, n = 7) and limits of detection (0.23–0.66 ng/g) were obtained. This method is simple, rapid, reliable, sensitive, and efficient and can be used for monitoring of progestin residues in fish. This method provides a strong guarantee to deal with food emergencies for the laboratory, provides technical support for the screening and quantitative detection of progesterone in fish, and provides technical support for the food safety of aquatic products.http://dx.doi.org/10.1155/2019/6426958 |
| spellingShingle | Chunxiu Gu Yanling Cheng Xin Zhen Xiaoxuan Chen Kaowen Zhou Determination of Progestin Residues in Fish by UPLC-Q-TOF/MS Coupled with QuEChERS Journal of Analytical Methods in Chemistry |
| title | Determination of Progestin Residues in Fish by UPLC-Q-TOF/MS Coupled with QuEChERS |
| title_full | Determination of Progestin Residues in Fish by UPLC-Q-TOF/MS Coupled with QuEChERS |
| title_fullStr | Determination of Progestin Residues in Fish by UPLC-Q-TOF/MS Coupled with QuEChERS |
| title_full_unstemmed | Determination of Progestin Residues in Fish by UPLC-Q-TOF/MS Coupled with QuEChERS |
| title_short | Determination of Progestin Residues in Fish by UPLC-Q-TOF/MS Coupled with QuEChERS |
| title_sort | determination of progestin residues in fish by uplc q tof ms coupled with quechers |
| url | http://dx.doi.org/10.1155/2019/6426958 |
| work_keys_str_mv | AT chunxiugu determinationofprogestinresiduesinfishbyuplcqtofmscoupledwithquechers AT yanlingcheng determinationofprogestinresiduesinfishbyuplcqtofmscoupledwithquechers AT xinzhen determinationofprogestinresiduesinfishbyuplcqtofmscoupledwithquechers AT xiaoxuanchen determinationofprogestinresiduesinfishbyuplcqtofmscoupledwithquechers AT kaowenzhou determinationofprogestinresiduesinfishbyuplcqtofmscoupledwithquechers |