Synthesis and Characterization of Imide Containing Hybrid Epoxy Resin with Improved Mechanical and Thermal Properties
Phosphorous containing amine, tripropyldiamine phosphine oxide (TPDAP), and hybrid monomer 4-(N-phthalimidophenyl) glycidylether (PPGE) were synthesized and characterized by Fourier transform infrared (FTIR) spectroscopy, nuclear magnetic resonance (NMR) spectroscopy, and elemental analysis (EDX). P...
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| Format: | Article |
| Language: | English |
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Wiley
2014-01-01
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| Series: | International Journal of Polymer Science |
| Online Access: | http://dx.doi.org/10.1155/2014/941793 |
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| author | U. G. Rane A. A. Sabnis V. V. Shertukde |
| author_facet | U. G. Rane A. A. Sabnis V. V. Shertukde |
| author_sort | U. G. Rane |
| collection | DOAJ |
| description | Phosphorous containing amine, tripropyldiamine phosphine oxide (TPDAP), and hybrid monomer 4-(N-phthalimidophenyl) glycidylether (PPGE) were synthesized and characterized by Fourier transform infrared (FTIR) spectroscopy, nuclear magnetic resonance (NMR) spectroscopy, and elemental analysis (EDX). PPGE was incorporated in bisphenol A epoxy resin (BPA) in various concentrations (5% to 20%), based on a weight percentage of BPA resin. Curing was carried out with the stoichiometric amount of TPDAP and 1,3-propanediamine (PDA) to result in cross-link network. Various mechanical, chemical, thermal, and flame retardant properties of modified and unmodified epoxy resin were studied. The coatings obtained with the addition of PPGE were found to have improved properties as compared with those of the unmodified resin. Coatings with 15% loading of PPGE showed improved flame retardant and mechanical properties with stable thermal behaviour. |
| format | Article |
| id | doaj-art-6cdda17cd28741e6a7abeabb3879a391 |
| institution | Kabale University |
| issn | 1687-9422 1687-9430 |
| language | English |
| publishDate | 2014-01-01 |
| publisher | Wiley |
| record_format | Article |
| series | International Journal of Polymer Science |
| spelling | doaj-art-6cdda17cd28741e6a7abeabb3879a3912025-02-03T06:07:48ZengWileyInternational Journal of Polymer Science1687-94221687-94302014-01-01201410.1155/2014/941793941793Synthesis and Characterization of Imide Containing Hybrid Epoxy Resin with Improved Mechanical and Thermal PropertiesU. G. Rane0A. A. Sabnis1V. V. Shertukde2Department of Polymer and Surface Engineering, Institute of Chemical Technology, Matunga, Mumbai, IndiaDepartment of Polymer and Surface Engineering, Institute of Chemical Technology, Matunga, Mumbai, IndiaDepartment of Polymer and Surface Engineering, Institute of Chemical Technology, Matunga, Mumbai, IndiaPhosphorous containing amine, tripropyldiamine phosphine oxide (TPDAP), and hybrid monomer 4-(N-phthalimidophenyl) glycidylether (PPGE) were synthesized and characterized by Fourier transform infrared (FTIR) spectroscopy, nuclear magnetic resonance (NMR) spectroscopy, and elemental analysis (EDX). PPGE was incorporated in bisphenol A epoxy resin (BPA) in various concentrations (5% to 20%), based on a weight percentage of BPA resin. Curing was carried out with the stoichiometric amount of TPDAP and 1,3-propanediamine (PDA) to result in cross-link network. Various mechanical, chemical, thermal, and flame retardant properties of modified and unmodified epoxy resin were studied. The coatings obtained with the addition of PPGE were found to have improved properties as compared with those of the unmodified resin. Coatings with 15% loading of PPGE showed improved flame retardant and mechanical properties with stable thermal behaviour.http://dx.doi.org/10.1155/2014/941793 |
| spellingShingle | U. G. Rane A. A. Sabnis V. V. Shertukde Synthesis and Characterization of Imide Containing Hybrid Epoxy Resin with Improved Mechanical and Thermal Properties International Journal of Polymer Science |
| title | Synthesis and Characterization of Imide Containing Hybrid Epoxy Resin with Improved Mechanical and Thermal Properties |
| title_full | Synthesis and Characterization of Imide Containing Hybrid Epoxy Resin with Improved Mechanical and Thermal Properties |
| title_fullStr | Synthesis and Characterization of Imide Containing Hybrid Epoxy Resin with Improved Mechanical and Thermal Properties |
| title_full_unstemmed | Synthesis and Characterization of Imide Containing Hybrid Epoxy Resin with Improved Mechanical and Thermal Properties |
| title_short | Synthesis and Characterization of Imide Containing Hybrid Epoxy Resin with Improved Mechanical and Thermal Properties |
| title_sort | synthesis and characterization of imide containing hybrid epoxy resin with improved mechanical and thermal properties |
| url | http://dx.doi.org/10.1155/2014/941793 |
| work_keys_str_mv | AT ugrane synthesisandcharacterizationofimidecontaininghybridepoxyresinwithimprovedmechanicalandthermalproperties AT aasabnis synthesisandcharacterizationofimidecontaininghybridepoxyresinwithimprovedmechanicalandthermalproperties AT vvshertukde synthesisandcharacterizationofimidecontaininghybridepoxyresinwithimprovedmechanicalandthermalproperties |