Investigation of Characteristics Whey Protein Isolate/Chitosan with Silica Addition in Biocomposite Film

Biocomposites made from whey protein isolate (WPI), chitosan, and silica (SiO2) have the potential as an environmentally friendly biopolymer material. In this research, the WPI biocomposite film has been developed by casting method with the addition of chitosan and SiO2. The loading of SiO2 (1, 3, a...

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Main Authors: Ika Zuwanna, Medyan Riza, Sri Aprilia, Yanna Syamsuddin, Syahiddin Said, Rozanna Dewi
Format: Article
Language:English
Published: Universitas Indonesia 2025-01-01
Series:International Journal of Technology
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Online Access:https://ijtech.eng.ui.ac.id/article/view/6335
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author Ika Zuwanna
Medyan Riza
Sri Aprilia
Yanna Syamsuddin
Syahiddin Said
Rozanna Dewi
author_facet Ika Zuwanna
Medyan Riza
Sri Aprilia
Yanna Syamsuddin
Syahiddin Said
Rozanna Dewi
author_sort Ika Zuwanna
collection DOAJ
description Biocomposites made from whey protein isolate (WPI), chitosan, and silica (SiO2) have the potential as an environmentally friendly biopolymer material. In this research, the WPI biocomposite film has been developed by casting method with the addition of chitosan and SiO2. The loading of SiO2 (1, 3, and 5 %w/w) and chitosan (1.5 %w/w) affects the characteristics of the biocomposite film. The functional groups, morphology, structure, mechanical, thermal, and transparency of the biocomposite films were evaluated by Fourier transform infrared (FTIR) spectroscopy, Scanning electron microscope (SEM), X-ray diffraction (XRD), tensile strength, thermogravimetric (TGA), differential scanning calorimetry (DSC), thickness, swelling, and UV-Vis. The results showed that the swelling value of WPI/chitosan 78.23% decreased to 69.35% with the use of 5% SiO2. Film transparency decreased with higher SiO2, while the film tensile strength increased with the addition of 5% SiO2 with a value of 28.83 MPa. The incorporation of SiO2 improves the thermal properties of biocomposite films. According to the results, increasing the amount of SiO2 in biocomposite films boosts their performance, suggesting that they could eventually replace synthetic polymers in packaging applications.
format Article
id doaj-art-6a9a5a980c7748528b50ee606d5f9a0d
institution Kabale University
issn 2086-9614
2087-2100
language English
publishDate 2025-01-01
publisher Universitas Indonesia
record_format Article
series International Journal of Technology
spelling doaj-art-6a9a5a980c7748528b50ee606d5f9a0d2025-01-31T14:13:03ZengUniversitas IndonesiaInternational Journal of Technology2086-96142087-21002025-01-0116135936910.14716/ijtech.v16i1.63356335Investigation of Characteristics Whey Protein Isolate/Chitosan with Silica Addition in Biocomposite FilmIka Zuwanna0Medyan Riza1Sri Aprilia2Yanna Syamsuddin3Syahiddin Said4Rozanna Dewi51. Doctoral Program, School of Engineering, Post Graduate Program, Universitas Syiah Kuala, Banda Aceh 23111, Indonesia, 2. Department of Chemical Engineering, Faculty of Engineering, Universitas SyiaDepartment of Chemical Engineering, Faculty of Engineering, Universitas Syiah Kuala, Banda Aceh 23111, IndonesiaDepartment of Chemical Engineering, Faculty of Engineering, Universitas Syiah Kuala, Banda Aceh 23111, IndonesiaDepartment of Chemical Engineering, Faculty of Engineering, Universitas Syiah Kuala, Banda Aceh 23111, IndonesiaDepartment of Chemical Engineering, Faculty of Engineering, Universitas Syiah Kuala, Banda Aceh 23111, IndonesiaDepartment of Chemical Engineering, Faculty of Engineering, Universitas Malikussaleh, Aceh Utara 24351, IndonesiaBiocomposites made from whey protein isolate (WPI), chitosan, and silica (SiO2) have the potential as an environmentally friendly biopolymer material. In this research, the WPI biocomposite film has been developed by casting method with the addition of chitosan and SiO2. The loading of SiO2 (1, 3, and 5 %w/w) and chitosan (1.5 %w/w) affects the characteristics of the biocomposite film. The functional groups, morphology, structure, mechanical, thermal, and transparency of the biocomposite films were evaluated by Fourier transform infrared (FTIR) spectroscopy, Scanning electron microscope (SEM), X-ray diffraction (XRD), tensile strength, thermogravimetric (TGA), differential scanning calorimetry (DSC), thickness, swelling, and UV-Vis. The results showed that the swelling value of WPI/chitosan 78.23% decreased to 69.35% with the use of 5% SiO2. Film transparency decreased with higher SiO2, while the film tensile strength increased with the addition of 5% SiO2 with a value of 28.83 MPa. The incorporation of SiO2 improves the thermal properties of biocomposite films. According to the results, increasing the amount of SiO2 in biocomposite films boosts their performance, suggesting that they could eventually replace synthetic polymers in packaging applications.https://ijtech.eng.ui.ac.id/article/view/6335biocomposite filmchitosanfilm propertiessilicawhey protein isolate
spellingShingle Ika Zuwanna
Medyan Riza
Sri Aprilia
Yanna Syamsuddin
Syahiddin Said
Rozanna Dewi
Investigation of Characteristics Whey Protein Isolate/Chitosan with Silica Addition in Biocomposite Film
International Journal of Technology
biocomposite film
chitosan
film properties
silica
whey protein isolate
title Investigation of Characteristics Whey Protein Isolate/Chitosan with Silica Addition in Biocomposite Film
title_full Investigation of Characteristics Whey Protein Isolate/Chitosan with Silica Addition in Biocomposite Film
title_fullStr Investigation of Characteristics Whey Protein Isolate/Chitosan with Silica Addition in Biocomposite Film
title_full_unstemmed Investigation of Characteristics Whey Protein Isolate/Chitosan with Silica Addition in Biocomposite Film
title_short Investigation of Characteristics Whey Protein Isolate/Chitosan with Silica Addition in Biocomposite Film
title_sort investigation of characteristics whey protein isolate chitosan with silica addition in biocomposite film
topic biocomposite film
chitosan
film properties
silica
whey protein isolate
url https://ijtech.eng.ui.ac.id/article/view/6335
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AT medyanriza investigationofcharacteristicswheyproteinisolatechitosanwithsilicaadditioninbiocompositefilm
AT sriaprilia investigationofcharacteristicswheyproteinisolatechitosanwithsilicaadditioninbiocompositefilm
AT yannasyamsuddin investigationofcharacteristicswheyproteinisolatechitosanwithsilicaadditioninbiocompositefilm
AT syahiddinsaid investigationofcharacteristicswheyproteinisolatechitosanwithsilicaadditioninbiocompositefilm
AT rozannadewi investigationofcharacteristicswheyproteinisolatechitosanwithsilicaadditioninbiocompositefilm