The Influence of Lead Concentration on Photocatalytic Reduction of Pb(II) Ions Assisted by Cu-TiO2 Nanotubes
Cu2+ ions were successfully loaded into TiO2 nanotubes using wet impregnation technique in 0.6 M Cu(NO3)2·3H2O solution. The effect of reaction temperatures on the nanotube’s morphology, crystal structure, and their photocatalytic reduction of Pb(II) ions were investigated. The high reaction tempera...
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2014-01-01
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Series: | International Journal of Photoenergy |
Online Access: | http://dx.doi.org/10.1155/2014/839106 |
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author | Srimala Sreekantan Chin Wei Lai Syazwani Mohd Zaki |
author_facet | Srimala Sreekantan Chin Wei Lai Syazwani Mohd Zaki |
author_sort | Srimala Sreekantan |
collection | DOAJ |
description | Cu2+ ions were successfully loaded into TiO2 nanotubes using wet impregnation technique in 0.6 M Cu(NO3)2·3H2O solution. The effect of reaction temperatures on the nanotube’s morphology, crystal structure, and their photocatalytic reduction of Pb(II) ions were investigated. The high reaction temperature could improve the crystallinity of anatase phase. However, irregular and corrugated nanotubular surface covered with Cu precipitates was observed. In the present study, incorporation of an optimum content of Cu element (1.3 at%) into TiO2 nanotubes at room temperature has an important function in enhancing the photocatalytic reduction of Pb(II) ions in alkaline condition (pH 11) due to the higher synergistic effects of photocatalytic reaction under UV illumination. The optimum concentration of Pb(II) ions for effective Pb(II) ions removal performance was found in between 20 and 60 ppm. |
format | Article |
id | doaj-art-6814584c7967460e86419946e3352fae |
institution | Kabale University |
issn | 1110-662X 1687-529X |
language | English |
publishDate | 2014-01-01 |
publisher | Wiley |
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series | International Journal of Photoenergy |
spelling | doaj-art-6814584c7967460e86419946e3352fae2025-02-03T01:21:36ZengWileyInternational Journal of Photoenergy1110-662X1687-529X2014-01-01201410.1155/2014/839106839106The Influence of Lead Concentration on Photocatalytic Reduction of Pb(II) Ions Assisted by Cu-TiO2 NanotubesSrimala Sreekantan0Chin Wei Lai1Syazwani Mohd Zaki2School of Materials and Mineral Resources Engineering, Universiti Sains Malaysia, Engineering Campus, Seberang Perai Selatan, 14300 Nibong Tebal, Pulau Pinang, MalaysiaNanotechnology & Catalysis Research Centre (NANOCAT), 3rd Floor, Block A, Institute of Postgraduate Studies (IPS), University of Malaya, 50603 Kuala Lumpur, MalaysiaSchool of Materials and Mineral Resources Engineering, Universiti Sains Malaysia, Engineering Campus, Seberang Perai Selatan, 14300 Nibong Tebal, Pulau Pinang, MalaysiaCu2+ ions were successfully loaded into TiO2 nanotubes using wet impregnation technique in 0.6 M Cu(NO3)2·3H2O solution. The effect of reaction temperatures on the nanotube’s morphology, crystal structure, and their photocatalytic reduction of Pb(II) ions were investigated. The high reaction temperature could improve the crystallinity of anatase phase. However, irregular and corrugated nanotubular surface covered with Cu precipitates was observed. In the present study, incorporation of an optimum content of Cu element (1.3 at%) into TiO2 nanotubes at room temperature has an important function in enhancing the photocatalytic reduction of Pb(II) ions in alkaline condition (pH 11) due to the higher synergistic effects of photocatalytic reaction under UV illumination. The optimum concentration of Pb(II) ions for effective Pb(II) ions removal performance was found in between 20 and 60 ppm.http://dx.doi.org/10.1155/2014/839106 |
spellingShingle | Srimala Sreekantan Chin Wei Lai Syazwani Mohd Zaki The Influence of Lead Concentration on Photocatalytic Reduction of Pb(II) Ions Assisted by Cu-TiO2 Nanotubes International Journal of Photoenergy |
title | The Influence of Lead Concentration on Photocatalytic Reduction of Pb(II) Ions Assisted by Cu-TiO2 Nanotubes |
title_full | The Influence of Lead Concentration on Photocatalytic Reduction of Pb(II) Ions Assisted by Cu-TiO2 Nanotubes |
title_fullStr | The Influence of Lead Concentration on Photocatalytic Reduction of Pb(II) Ions Assisted by Cu-TiO2 Nanotubes |
title_full_unstemmed | The Influence of Lead Concentration on Photocatalytic Reduction of Pb(II) Ions Assisted by Cu-TiO2 Nanotubes |
title_short | The Influence of Lead Concentration on Photocatalytic Reduction of Pb(II) Ions Assisted by Cu-TiO2 Nanotubes |
title_sort | influence of lead concentration on photocatalytic reduction of pb ii ions assisted by cu tio2 nanotubes |
url | http://dx.doi.org/10.1155/2014/839106 |
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