Microstructural Analysis and Constitutive Modeling of Superplastic Deformation Behavior of Al-Mg-Zn-Cu-Zr-xNi Alloys with Different Ni Contents

Superplastic forming is a process that enables the production of complex-shaped parts using metallic alloys. To design the optimal forming regimes and ensure the success of forming operations, it is essential to use mathematical models that accurately represent the superplastic deformation behavior....

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Main Authors: Zarnigor S. Turaeva, Ahmed O. Mosleh, Olga A. Yakovtseva, Anton D. Kotov, Anastasia V. Mikhaylovskaya
Format: Article
Language:English
Published: MDPI AG 2025-01-01
Series:Metals
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Online Access:https://www.mdpi.com/2075-4701/15/1/45
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author Zarnigor S. Turaeva
Ahmed O. Mosleh
Olga A. Yakovtseva
Anton D. Kotov
Anastasia V. Mikhaylovskaya
author_facet Zarnigor S. Turaeva
Ahmed O. Mosleh
Olga A. Yakovtseva
Anton D. Kotov
Anastasia V. Mikhaylovskaya
author_sort Zarnigor S. Turaeva
collection DOAJ
description Superplastic forming is a process that enables the production of complex-shaped parts using metallic alloys. To design the optimal forming regimes and ensure the success of forming operations, it is essential to use mathematical models that accurately represent the superplastic deformation behavior. This paper is concerned with the study of the microstructure and superplastic deformation behavior, with the construction of a constitutive model, of Al-Mg-Zn-Cu-Zr aluminum alloys with varying Ni contents. The aluminum solid solution and coarse precipitates of the T(Mg<sub>32</sub>(Al,Zn)<sub>49</sub> and Al<sub>3</sub>Ni second phases were formed in the studied alloy and Cu dissolved in both second phases. The deformation behavior was investigated in the temperature range of 400–480 °C and the strain rate range of 10<sup>−3</sup>–10<sup>−1</sup> s<sup>−1</sup>. Due to the fine Al<sub>3</sub>Zr precipitates, the alloys exhibit a partially recrystallized grain structure before the onset of superplastic deformation. Coarse precipitates of the second phases facilitate dynamic recrystallization and enhance superplasticity at the strain rates and temperatures studied. The alloys with ~6–9% particles exhibit high-strain-rate superplasticity at temperatures of 440–480 °C and strain rates of 10<sup>−2</sup>–10<sup>−1</sup> s<sup>−1</sup>. The presence of high fractions of ~9% Al<sub>3</sub>(Ni,Cu) and ~3% T-phase precipitates provided high-strain-rate superplasticity with elongations of 700–800% at a low temperature of 400 °C. An Arrhenius-type constitutive model with good agreement between the predicted and experimental flow stresses was developed for the alloys with different Ni contents.
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spelling doaj-art-64ec418db62043aa98efb59a351f708f2025-01-24T13:41:30ZengMDPI AGMetals2075-47012025-01-011514510.3390/met15010045Microstructural Analysis and Constitutive Modeling of Superplastic Deformation Behavior of Al-Mg-Zn-Cu-Zr-xNi Alloys with Different Ni ContentsZarnigor S. Turaeva0Ahmed O. Mosleh1Olga A. Yakovtseva2Anton D. Kotov3Anastasia V. Mikhaylovskaya4Department of Physical Metallurgy of Non-Ferrous Metals, National University of Science and Technology “MISIS”, Moscow 119049, RussiaDepartment of Mechanical Engineering, Faculty of Engineering at Shoubra, Benha University, Cairo 11629, EgyptDepartment of Physical Metallurgy of Non-Ferrous Metals, National University of Science and Technology “MISIS”, Moscow 119049, RussiaDepartment of Physical Metallurgy of Non-Ferrous Metals, National University of Science and Technology “MISIS”, Moscow 119049, RussiaDepartment of Physical Metallurgy of Non-Ferrous Metals, National University of Science and Technology “MISIS”, Moscow 119049, RussiaSuperplastic forming is a process that enables the production of complex-shaped parts using metallic alloys. To design the optimal forming regimes and ensure the success of forming operations, it is essential to use mathematical models that accurately represent the superplastic deformation behavior. This paper is concerned with the study of the microstructure and superplastic deformation behavior, with the construction of a constitutive model, of Al-Mg-Zn-Cu-Zr aluminum alloys with varying Ni contents. The aluminum solid solution and coarse precipitates of the T(Mg<sub>32</sub>(Al,Zn)<sub>49</sub> and Al<sub>3</sub>Ni second phases were formed in the studied alloy and Cu dissolved in both second phases. The deformation behavior was investigated in the temperature range of 400–480 °C and the strain rate range of 10<sup>−3</sup>–10<sup>−1</sup> s<sup>−1</sup>. Due to the fine Al<sub>3</sub>Zr precipitates, the alloys exhibit a partially recrystallized grain structure before the onset of superplastic deformation. Coarse precipitates of the second phases facilitate dynamic recrystallization and enhance superplasticity at the strain rates and temperatures studied. The alloys with ~6–9% particles exhibit high-strain-rate superplasticity at temperatures of 440–480 °C and strain rates of 10<sup>−2</sup>–10<sup>−1</sup> s<sup>−1</sup>. The presence of high fractions of ~9% Al<sub>3</sub>(Ni,Cu) and ~3% T-phase precipitates provided high-strain-rate superplasticity with elongations of 700–800% at a low temperature of 400 °C. An Arrhenius-type constitutive model with good agreement between the predicted and experimental flow stresses was developed for the alloys with different Ni contents.https://www.mdpi.com/2075-4701/15/1/45superplasticityaluminum alloysmicrostructureconstitutive modelingactivation energy
spellingShingle Zarnigor S. Turaeva
Ahmed O. Mosleh
Olga A. Yakovtseva
Anton D. Kotov
Anastasia V. Mikhaylovskaya
Microstructural Analysis and Constitutive Modeling of Superplastic Deformation Behavior of Al-Mg-Zn-Cu-Zr-xNi Alloys with Different Ni Contents
Metals
superplasticity
aluminum alloys
microstructure
constitutive modeling
activation energy
title Microstructural Analysis and Constitutive Modeling of Superplastic Deformation Behavior of Al-Mg-Zn-Cu-Zr-xNi Alloys with Different Ni Contents
title_full Microstructural Analysis and Constitutive Modeling of Superplastic Deformation Behavior of Al-Mg-Zn-Cu-Zr-xNi Alloys with Different Ni Contents
title_fullStr Microstructural Analysis and Constitutive Modeling of Superplastic Deformation Behavior of Al-Mg-Zn-Cu-Zr-xNi Alloys with Different Ni Contents
title_full_unstemmed Microstructural Analysis and Constitutive Modeling of Superplastic Deformation Behavior of Al-Mg-Zn-Cu-Zr-xNi Alloys with Different Ni Contents
title_short Microstructural Analysis and Constitutive Modeling of Superplastic Deformation Behavior of Al-Mg-Zn-Cu-Zr-xNi Alloys with Different Ni Contents
title_sort microstructural analysis and constitutive modeling of superplastic deformation behavior of al mg zn cu zr xni alloys with different ni contents
topic superplasticity
aluminum alloys
microstructure
constitutive modeling
activation energy
url https://www.mdpi.com/2075-4701/15/1/45
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