Microstructural Characterization and Wear Properties of Fe-Based Amorphous-Crystalline Coating Deposited by Twin Wire Arc Spraying

Twin wire arc spraying (TWAS) was used to produce an amorphous crystalline Fe-based coating on AISI 1018 steel substrate using a commercial powder (140MXC) in order to improve microhardness and wear properties. The microstructures of coating were characterized by X-ray diffraction (XRD), scanning el...

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Main Authors: Ana Arizmendi-Morquecho, Araceli Campa-Castilla, C. Leyva-Porras, Josué Almicar Aguilar Martinez, Gregorio Vargas Gutiérrez, Karla Judith Moreno Bello, L. López López
Format: Article
Language:English
Published: Wiley 2014-01-01
Series:Advances in Materials Science and Engineering
Online Access:http://dx.doi.org/10.1155/2014/836739
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author Ana Arizmendi-Morquecho
Araceli Campa-Castilla
C. Leyva-Porras
Josué Almicar Aguilar Martinez
Gregorio Vargas Gutiérrez
Karla Judith Moreno Bello
L. López López
author_facet Ana Arizmendi-Morquecho
Araceli Campa-Castilla
C. Leyva-Porras
Josué Almicar Aguilar Martinez
Gregorio Vargas Gutiérrez
Karla Judith Moreno Bello
L. López López
author_sort Ana Arizmendi-Morquecho
collection DOAJ
description Twin wire arc spraying (TWAS) was used to produce an amorphous crystalline Fe-based coating on AISI 1018 steel substrate using a commercial powder (140MXC) in order to improve microhardness and wear properties. The microstructures of coating were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), and transmission electron microscopy (TEM) as well as the powder precursor. Analysis in the coating showed the formation of an amorphous matrix with boron and tungsten carbides randomly dispersed. At high amplifications were identified boron carbides at interface boron carbide/amorphous matrix by TEM. This kind of carbides growth can be attributed to partial crystallization by heterogeneous nucleation. These interfaces have not been reported in the literature by thermal spraying process. The measurements of average microhardness on amorphous matrix and boron carbides were 9.1 and 23.85 GPa, respectively. By contrast, the microhardness values of unmelted boron carbide in the amorphous phase were higher than in the substrate, approaching 2.14 GPa. The relative wear resistance of coating was 5.6 times that of substrate. These results indicate that the twin wire arc spraying is a promising technique to prepare amorphous crystalline coatings.
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spelling doaj-art-60b777900cc44d1d974ff1b6b2da8dcc2025-02-03T01:22:36ZengWileyAdvances in Materials Science and Engineering1687-84341687-84422014-01-01201410.1155/2014/836739836739Microstructural Characterization and Wear Properties of Fe-Based Amorphous-Crystalline Coating Deposited by Twin Wire Arc SprayingAna Arizmendi-Morquecho0Araceli Campa-Castilla1C. Leyva-Porras2Josué Almicar Aguilar Martinez3Gregorio Vargas Gutiérrez4Karla Judith Moreno Bello5L. López López6Centro de Investigación en Materiales Avanzados, S.C. Unidad Monterrey, Alianza Norte 202, 66600 Apodaca, NL, MexicoCentro de Investigación en Materiales Avanzados, S.C. Unidad Monterrey, Alianza Norte 202, 66600 Apodaca, NL, MexicoCentro de Investigación en Materiales Avanzados, S.C. Unidad Monterrey, Alianza Norte 202, 66600 Apodaca, NL, MexicoUniversidad Autónoma de Nuevo León, Facultad de Ingeniería Mecánica y Eléctrica, Centro de Investigación e Innovación en Ingeniería Aeronáutica, Carretera a Salinas Victoria km 2.3, 66600 Apodaca, NL, MexicoCentro de Investigación y de Estudios Avanzados del IPN, Unidad Saltillo, Avenida Industria Metalúrgica 1062, 25900 Ramos Arizpe, COAH, MexicoInstituto Tecnológico de Celaya, A. García Cubas S/N A.P. 57, 38010 Celaya, GTO, MexicoCorporación Mexicana de Investigación en Materiales, S.A. de C.V., Ciencia y Tecnología 790 Fracc. Saltillo 400, 25260 Saltillo, COAH, MexicoTwin wire arc spraying (TWAS) was used to produce an amorphous crystalline Fe-based coating on AISI 1018 steel substrate using a commercial powder (140MXC) in order to improve microhardness and wear properties. The microstructures of coating were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), and transmission electron microscopy (TEM) as well as the powder precursor. Analysis in the coating showed the formation of an amorphous matrix with boron and tungsten carbides randomly dispersed. At high amplifications were identified boron carbides at interface boron carbide/amorphous matrix by TEM. This kind of carbides growth can be attributed to partial crystallization by heterogeneous nucleation. These interfaces have not been reported in the literature by thermal spraying process. The measurements of average microhardness on amorphous matrix and boron carbides were 9.1 and 23.85 GPa, respectively. By contrast, the microhardness values of unmelted boron carbide in the amorphous phase were higher than in the substrate, approaching 2.14 GPa. The relative wear resistance of coating was 5.6 times that of substrate. These results indicate that the twin wire arc spraying is a promising technique to prepare amorphous crystalline coatings.http://dx.doi.org/10.1155/2014/836739
spellingShingle Ana Arizmendi-Morquecho
Araceli Campa-Castilla
C. Leyva-Porras
Josué Almicar Aguilar Martinez
Gregorio Vargas Gutiérrez
Karla Judith Moreno Bello
L. López López
Microstructural Characterization and Wear Properties of Fe-Based Amorphous-Crystalline Coating Deposited by Twin Wire Arc Spraying
Advances in Materials Science and Engineering
title Microstructural Characterization and Wear Properties of Fe-Based Amorphous-Crystalline Coating Deposited by Twin Wire Arc Spraying
title_full Microstructural Characterization and Wear Properties of Fe-Based Amorphous-Crystalline Coating Deposited by Twin Wire Arc Spraying
title_fullStr Microstructural Characterization and Wear Properties of Fe-Based Amorphous-Crystalline Coating Deposited by Twin Wire Arc Spraying
title_full_unstemmed Microstructural Characterization and Wear Properties of Fe-Based Amorphous-Crystalline Coating Deposited by Twin Wire Arc Spraying
title_short Microstructural Characterization and Wear Properties of Fe-Based Amorphous-Crystalline Coating Deposited by Twin Wire Arc Spraying
title_sort microstructural characterization and wear properties of fe based amorphous crystalline coating deposited by twin wire arc spraying
url http://dx.doi.org/10.1155/2014/836739
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