Synthesis of 1,5-Diaryl-1,4-pentadien-3-one Amidinohydrazone Hydrochloride Under Ultrasound Irradiation
Synthesis of 1,5-diaryl-1,4-pentadien-3-one amidinohydrazone hydrochloride via the condensation of 1,5-diaryl-1,4-pentadien-3-one and aminoguanidine hydrochloride catalyzed by hydrochloric acid was carried out in 80-94% yield at 35-37°C within 1.5 h under ultrasound irradiation. Compared to the clas...
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Format: | Article |
Language: | English |
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Wiley
2012-01-01
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Series: | E-Journal of Chemistry |
Online Access: | http://dx.doi.org/10.1155/2012/802408 |
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author | Chao Du Ji Tai Li |
author_facet | Chao Du Ji Tai Li |
author_sort | Chao Du |
collection | DOAJ |
description | Synthesis of 1,5-diaryl-1,4-pentadien-3-one amidinohydrazone hydrochloride via the condensation of 1,5-diaryl-1,4-pentadien-3-one and aminoguanidine hydrochloride catalyzed by hydrochloric acid was carried out in 80-94% yield at 35-37°C within 1.5 h under ultrasound irradiation. Compared to the classical method, the advantages of this method are milder conditions, shorter reaction time and higher yield. |
format | Article |
id | doaj-art-5e9688fc95dd4fc8bec7ba6532b938f4 |
institution | Kabale University |
issn | 0973-4945 2090-9810 |
language | English |
publishDate | 2012-01-01 |
publisher | Wiley |
record_format | Article |
series | E-Journal of Chemistry |
spelling | doaj-art-5e9688fc95dd4fc8bec7ba6532b938f42025-02-03T05:53:48ZengWileyE-Journal of Chemistry0973-49452090-98102012-01-01942108211310.1155/2012/802408Synthesis of 1,5-Diaryl-1,4-pentadien-3-one Amidinohydrazone Hydrochloride Under Ultrasound IrradiationChao Du0Ji Tai Li1Key Laboratory Analytical Science and Technology Hebei Province, Key Laboratory of Medical Chemistry and Molecular Diagnosis, Ministry of Education, College Chemistry and Environmental Science, Hebei University, Baoding 071002, ChinaKey Laboratory Analytical Science and Technology Hebei Province, Key Laboratory of Medical Chemistry and Molecular Diagnosis, Ministry of Education, College Chemistry and Environmental Science, Hebei University, Baoding 071002, ChinaSynthesis of 1,5-diaryl-1,4-pentadien-3-one amidinohydrazone hydrochloride via the condensation of 1,5-diaryl-1,4-pentadien-3-one and aminoguanidine hydrochloride catalyzed by hydrochloric acid was carried out in 80-94% yield at 35-37°C within 1.5 h under ultrasound irradiation. Compared to the classical method, the advantages of this method are milder conditions, shorter reaction time and higher yield.http://dx.doi.org/10.1155/2012/802408 |
spellingShingle | Chao Du Ji Tai Li Synthesis of 1,5-Diaryl-1,4-pentadien-3-one Amidinohydrazone Hydrochloride Under Ultrasound Irradiation E-Journal of Chemistry |
title | Synthesis of 1,5-Diaryl-1,4-pentadien-3-one Amidinohydrazone Hydrochloride Under Ultrasound Irradiation |
title_full | Synthesis of 1,5-Diaryl-1,4-pentadien-3-one Amidinohydrazone Hydrochloride Under Ultrasound Irradiation |
title_fullStr | Synthesis of 1,5-Diaryl-1,4-pentadien-3-one Amidinohydrazone Hydrochloride Under Ultrasound Irradiation |
title_full_unstemmed | Synthesis of 1,5-Diaryl-1,4-pentadien-3-one Amidinohydrazone Hydrochloride Under Ultrasound Irradiation |
title_short | Synthesis of 1,5-Diaryl-1,4-pentadien-3-one Amidinohydrazone Hydrochloride Under Ultrasound Irradiation |
title_sort | synthesis of 1 5 diaryl 1 4 pentadien 3 one amidinohydrazone hydrochloride under ultrasound irradiation |
url | http://dx.doi.org/10.1155/2012/802408 |
work_keys_str_mv | AT chaodu synthesisof15diaryl14pentadien3oneamidinohydrazonehydrochlorideunderultrasoundirradiation AT jitaili synthesisof15diaryl14pentadien3oneamidinohydrazonehydrochlorideunderultrasoundirradiation |