Synthesis of 1,5-Diaryl-1,4-pentadien-3-one Amidinohydrazone Hydrochloride Under Ultrasound Irradiation

Synthesis of 1,5-diaryl-1,4-pentadien-3-one amidinohydrazone hydrochloride via the condensation of 1,5-diaryl-1,4-pentadien-3-one and aminoguanidine hydrochloride catalyzed by hydrochloric acid was carried out in 80-94% yield at 35-37°C within 1.5 h under ultrasound irradiation. Compared to the clas...

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Main Authors: Chao Du, Ji Tai Li
Format: Article
Language:English
Published: Wiley 2012-01-01
Series:E-Journal of Chemistry
Online Access:http://dx.doi.org/10.1155/2012/802408
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author Chao Du
Ji Tai Li
author_facet Chao Du
Ji Tai Li
author_sort Chao Du
collection DOAJ
description Synthesis of 1,5-diaryl-1,4-pentadien-3-one amidinohydrazone hydrochloride via the condensation of 1,5-diaryl-1,4-pentadien-3-one and aminoguanidine hydrochloride catalyzed by hydrochloric acid was carried out in 80-94% yield at 35-37°C within 1.5 h under ultrasound irradiation. Compared to the classical method, the advantages of this method are milder conditions, shorter reaction time and higher yield.
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institution Kabale University
issn 0973-4945
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language English
publishDate 2012-01-01
publisher Wiley
record_format Article
series E-Journal of Chemistry
spelling doaj-art-5e9688fc95dd4fc8bec7ba6532b938f42025-02-03T05:53:48ZengWileyE-Journal of Chemistry0973-49452090-98102012-01-01942108211310.1155/2012/802408Synthesis of 1,5-Diaryl-1,4-pentadien-3-one Amidinohydrazone Hydrochloride Under Ultrasound IrradiationChao Du0Ji Tai Li1Key Laboratory Analytical Science and Technology Hebei Province, Key Laboratory of Medical Chemistry and Molecular Diagnosis, Ministry of Education, College Chemistry and Environmental Science, Hebei University, Baoding 071002, ChinaKey Laboratory Analytical Science and Technology Hebei Province, Key Laboratory of Medical Chemistry and Molecular Diagnosis, Ministry of Education, College Chemistry and Environmental Science, Hebei University, Baoding 071002, ChinaSynthesis of 1,5-diaryl-1,4-pentadien-3-one amidinohydrazone hydrochloride via the condensation of 1,5-diaryl-1,4-pentadien-3-one and aminoguanidine hydrochloride catalyzed by hydrochloric acid was carried out in 80-94% yield at 35-37°C within 1.5 h under ultrasound irradiation. Compared to the classical method, the advantages of this method are milder conditions, shorter reaction time and higher yield.http://dx.doi.org/10.1155/2012/802408
spellingShingle Chao Du
Ji Tai Li
Synthesis of 1,5-Diaryl-1,4-pentadien-3-one Amidinohydrazone Hydrochloride Under Ultrasound Irradiation
E-Journal of Chemistry
title Synthesis of 1,5-Diaryl-1,4-pentadien-3-one Amidinohydrazone Hydrochloride Under Ultrasound Irradiation
title_full Synthesis of 1,5-Diaryl-1,4-pentadien-3-one Amidinohydrazone Hydrochloride Under Ultrasound Irradiation
title_fullStr Synthesis of 1,5-Diaryl-1,4-pentadien-3-one Amidinohydrazone Hydrochloride Under Ultrasound Irradiation
title_full_unstemmed Synthesis of 1,5-Diaryl-1,4-pentadien-3-one Amidinohydrazone Hydrochloride Under Ultrasound Irradiation
title_short Synthesis of 1,5-Diaryl-1,4-pentadien-3-one Amidinohydrazone Hydrochloride Under Ultrasound Irradiation
title_sort synthesis of 1 5 diaryl 1 4 pentadien 3 one amidinohydrazone hydrochloride under ultrasound irradiation
url http://dx.doi.org/10.1155/2012/802408
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AT jitaili synthesisof15diaryl14pentadien3oneamidinohydrazonehydrochlorideunderultrasoundirradiation