Characterization of TiZrN and TaZrN Nanocomposite Multilayer Coating Deposited via RF/DC Magnetron Sputtering on AISI4140 Steel
In this present research work, TiZrN and TaZrN multilayer coating was deposited on 4140 steel by RF/DC magnetron sputtering for comparative work also prepared in single layer. The flow rate ratio of Ar/N2 was set to 15 : 3 sccm and the thin film was prepared by the PVD (physical vapor deposition) me...
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2021-01-01
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Online Access: | http://dx.doi.org/10.1155/2021/8273708 |
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author | R. Hariharan R. Raja R. J. Golden Renjith Nimal Mohamad Reda A. Refaai S Ravi Haiter Lenin Allasi |
author_facet | R. Hariharan R. Raja R. J. Golden Renjith Nimal Mohamad Reda A. Refaai S Ravi Haiter Lenin Allasi |
author_sort | R. Hariharan |
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description | In this present research work, TiZrN and TaZrN multilayer coating was deposited on 4140 steel by RF/DC magnetron sputtering for comparative work also prepared in single layer. The flow rate ratio of Ar/N2 was set to 15 : 3 sccm and the thin film was prepared by the PVD (physical vapor deposition) method by RF/DC magnetron using a Ti-Zr and Ta-Zr target with a purity of 99.99%. The crystal structure, surface morphology microstructure, and component arrangements were explored by X-ray diffraction (XRD), scanning electron microscope (SEM), and atomic force microscopy (AFM). It has been found that the crystal structure, surface morphology, microstructure, and elemental composition of the membrane are strongly dependent on deposition parameters. It is mechanically characterized by corrosion and Vickers hardness. In AFM measurements, coarse cluster particles with increasing Ti and Ta values not only increase the average roughness (Ra) by 2.341 nm (200°C) and 2.951 nm (400°C) but also have a continuous average thickness which was shown to increase by 1.504 nm and 781.75 nm. With the increase of hardness, the roughness decreases correspondingly. The TiZrN multilayer microhardness augmented to 314 GPa at 200°C and 371 GPa for TaZrN (400°C). |
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institution | Kabale University |
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language | English |
publishDate | 2021-01-01 |
publisher | Wiley |
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series | Advances in Materials Science and Engineering |
spelling | doaj-art-5cb576413f7d4593804fdb78c19d6bbe2025-02-03T06:00:50ZengWileyAdvances in Materials Science and Engineering1687-84422021-01-01202110.1155/2021/8273708Characterization of TiZrN and TaZrN Nanocomposite Multilayer Coating Deposited via RF/DC Magnetron Sputtering on AISI4140 SteelR. Hariharan0R. Raja1R. J. Golden Renjith Nimal2Mohamad Reda A. Refaai3S Ravi4Haiter Lenin Allasi5Department of Mechanical EngineeringVPMM Engineering College for WomenDepartment of Mechanical EngineeringPrince Sattam Bin Abdulaziz UniversityCentre for Materials ResearchDepartment of Mechanical EngineeringIn this present research work, TiZrN and TaZrN multilayer coating was deposited on 4140 steel by RF/DC magnetron sputtering for comparative work also prepared in single layer. The flow rate ratio of Ar/N2 was set to 15 : 3 sccm and the thin film was prepared by the PVD (physical vapor deposition) method by RF/DC magnetron using a Ti-Zr and Ta-Zr target with a purity of 99.99%. The crystal structure, surface morphology microstructure, and component arrangements were explored by X-ray diffraction (XRD), scanning electron microscope (SEM), and atomic force microscopy (AFM). It has been found that the crystal structure, surface morphology, microstructure, and elemental composition of the membrane are strongly dependent on deposition parameters. It is mechanically characterized by corrosion and Vickers hardness. In AFM measurements, coarse cluster particles with increasing Ti and Ta values not only increase the average roughness (Ra) by 2.341 nm (200°C) and 2.951 nm (400°C) but also have a continuous average thickness which was shown to increase by 1.504 nm and 781.75 nm. With the increase of hardness, the roughness decreases correspondingly. The TiZrN multilayer microhardness augmented to 314 GPa at 200°C and 371 GPa for TaZrN (400°C).http://dx.doi.org/10.1155/2021/8273708 |
spellingShingle | R. Hariharan R. Raja R. J. Golden Renjith Nimal Mohamad Reda A. Refaai S Ravi Haiter Lenin Allasi Characterization of TiZrN and TaZrN Nanocomposite Multilayer Coating Deposited via RF/DC Magnetron Sputtering on AISI4140 Steel Advances in Materials Science and Engineering |
title | Characterization of TiZrN and TaZrN Nanocomposite Multilayer Coating Deposited via RF/DC Magnetron Sputtering on AISI4140 Steel |
title_full | Characterization of TiZrN and TaZrN Nanocomposite Multilayer Coating Deposited via RF/DC Magnetron Sputtering on AISI4140 Steel |
title_fullStr | Characterization of TiZrN and TaZrN Nanocomposite Multilayer Coating Deposited via RF/DC Magnetron Sputtering on AISI4140 Steel |
title_full_unstemmed | Characterization of TiZrN and TaZrN Nanocomposite Multilayer Coating Deposited via RF/DC Magnetron Sputtering on AISI4140 Steel |
title_short | Characterization of TiZrN and TaZrN Nanocomposite Multilayer Coating Deposited via RF/DC Magnetron Sputtering on AISI4140 Steel |
title_sort | characterization of tizrn and tazrn nanocomposite multilayer coating deposited via rf dc magnetron sputtering on aisi4140 steel |
url | http://dx.doi.org/10.1155/2021/8273708 |
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