Characterization of TiZrN and TaZrN Nanocomposite Multilayer Coating Deposited via RF/DC Magnetron Sputtering on AISI4140 Steel

In this present research work, TiZrN and TaZrN multilayer coating was deposited on 4140 steel by RF/DC magnetron sputtering for comparative work also prepared in single layer. The flow rate ratio of Ar/N2 was set to 15 : 3 sccm and the thin film was prepared by the PVD (physical vapor deposition) me...

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Main Authors: R. Hariharan, R. Raja, R. J. Golden Renjith Nimal, Mohamad Reda A. Refaai, S Ravi, Haiter Lenin Allasi
Format: Article
Language:English
Published: Wiley 2021-01-01
Series:Advances in Materials Science and Engineering
Online Access:http://dx.doi.org/10.1155/2021/8273708
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author R. Hariharan
R. Raja
R. J. Golden Renjith Nimal
Mohamad Reda A. Refaai
S Ravi
Haiter Lenin Allasi
author_facet R. Hariharan
R. Raja
R. J. Golden Renjith Nimal
Mohamad Reda A. Refaai
S Ravi
Haiter Lenin Allasi
author_sort R. Hariharan
collection DOAJ
description In this present research work, TiZrN and TaZrN multilayer coating was deposited on 4140 steel by RF/DC magnetron sputtering for comparative work also prepared in single layer. The flow rate ratio of Ar/N2 was set to 15 : 3 sccm and the thin film was prepared by the PVD (physical vapor deposition) method by RF/DC magnetron using a Ti-Zr and Ta-Zr target with a purity of 99.99%. The crystal structure, surface morphology microstructure, and component arrangements were explored by X-ray diffraction (XRD), scanning electron microscope (SEM), and atomic force microscopy (AFM). It has been found that the crystal structure, surface morphology, microstructure, and elemental composition of the membrane are strongly dependent on deposition parameters. It is mechanically characterized by corrosion and Vickers hardness. In AFM measurements, coarse cluster particles with increasing Ti and Ta values not only increase the average roughness (Ra) by 2.341 nm (200°C) and 2.951 nm (400°C) but also have a continuous average thickness which was shown to increase by 1.504 nm and 781.75 nm. With the increase of hardness, the roughness decreases correspondingly. The TiZrN multilayer microhardness augmented to 314 GPa at 200°C and 371 GPa for TaZrN (400°C).
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spelling doaj-art-5cb576413f7d4593804fdb78c19d6bbe2025-02-03T06:00:50ZengWileyAdvances in Materials Science and Engineering1687-84422021-01-01202110.1155/2021/8273708Characterization of TiZrN and TaZrN Nanocomposite Multilayer Coating Deposited via RF/DC Magnetron Sputtering on AISI4140 SteelR. Hariharan0R. Raja1R. J. Golden Renjith Nimal2Mohamad Reda A. Refaai3S Ravi4Haiter Lenin Allasi5Department of Mechanical EngineeringVPMM Engineering College for WomenDepartment of Mechanical EngineeringPrince Sattam Bin Abdulaziz UniversityCentre for Materials ResearchDepartment of Mechanical EngineeringIn this present research work, TiZrN and TaZrN multilayer coating was deposited on 4140 steel by RF/DC magnetron sputtering for comparative work also prepared in single layer. The flow rate ratio of Ar/N2 was set to 15 : 3 sccm and the thin film was prepared by the PVD (physical vapor deposition) method by RF/DC magnetron using a Ti-Zr and Ta-Zr target with a purity of 99.99%. The crystal structure, surface morphology microstructure, and component arrangements were explored by X-ray diffraction (XRD), scanning electron microscope (SEM), and atomic force microscopy (AFM). It has been found that the crystal structure, surface morphology, microstructure, and elemental composition of the membrane are strongly dependent on deposition parameters. It is mechanically characterized by corrosion and Vickers hardness. In AFM measurements, coarse cluster particles with increasing Ti and Ta values not only increase the average roughness (Ra) by 2.341 nm (200°C) and 2.951 nm (400°C) but also have a continuous average thickness which was shown to increase by 1.504 nm and 781.75 nm. With the increase of hardness, the roughness decreases correspondingly. The TiZrN multilayer microhardness augmented to 314 GPa at 200°C and 371 GPa for TaZrN (400°C).http://dx.doi.org/10.1155/2021/8273708
spellingShingle R. Hariharan
R. Raja
R. J. Golden Renjith Nimal
Mohamad Reda A. Refaai
S Ravi
Haiter Lenin Allasi
Characterization of TiZrN and TaZrN Nanocomposite Multilayer Coating Deposited via RF/DC Magnetron Sputtering on AISI4140 Steel
Advances in Materials Science and Engineering
title Characterization of TiZrN and TaZrN Nanocomposite Multilayer Coating Deposited via RF/DC Magnetron Sputtering on AISI4140 Steel
title_full Characterization of TiZrN and TaZrN Nanocomposite Multilayer Coating Deposited via RF/DC Magnetron Sputtering on AISI4140 Steel
title_fullStr Characterization of TiZrN and TaZrN Nanocomposite Multilayer Coating Deposited via RF/DC Magnetron Sputtering on AISI4140 Steel
title_full_unstemmed Characterization of TiZrN and TaZrN Nanocomposite Multilayer Coating Deposited via RF/DC Magnetron Sputtering on AISI4140 Steel
title_short Characterization of TiZrN and TaZrN Nanocomposite Multilayer Coating Deposited via RF/DC Magnetron Sputtering on AISI4140 Steel
title_sort characterization of tizrn and tazrn nanocomposite multilayer coating deposited via rf dc magnetron sputtering on aisi4140 steel
url http://dx.doi.org/10.1155/2021/8273708
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