柱切换二维色谱法测定鱼肝油制剂中维生素D<sub>3</sub>含量

柱切换二维色谱法测定鱼肝油制剂中维生素D<sub>3</sub>含量

<sec><title>目的</title>建立鱼肝油制剂中维生素D<sub>3</sub>含量测定的柱切换二维液相色谱方法。</sec><sec><title>方法</title>通过皂化萃取制备样品，采用双泵单阀切换双检测器的二维液相色谱法，对色谱柱、捕获装置和检测波长进行优化，对方法的线性、系统适用性、回收率、重复性和样品稳定性进行考察，并在实际样品测定中进一步验证。</sec><sec><title>结果</title>建立了柱切换...

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Bibliographic Details
Main Authors:	戚绿叶, 张丽媛, 程巧鸳, 颜琳琦, 周明昊
Format:	Article
Language:	zho
Published:	Zhejiang University Press 2025-01-01
Series:	浙江大学学报. 医学版
Subjects:	鱼肝油维生素D<sub>3</sub> 含量测定二维液相色谱法
Online Access:	https://www.sciengine.com/doi/10.3724/zdxbyxb-2024-0045
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