Microwave Assisted Synthesis Spectral and Antibacterial Investigations on Complexes of Mn(II) With Amide Containing Ligands

The present research work describes the synthesis, spectral and antibacterial studies on the complexes of Mn(II) with amide group containing ligands. Synthesis of complexes has been carried out by conventional method as well as by microwave method. The complexes have been characterized on the basis...

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Main Authors: N. Bhojak, D. D. Gudasaria, N. Khiwani, R. Jain
Format: Article
Language:English
Published: Wiley 2007-01-01
Series:E-Journal of Chemistry
Online Access:http://dx.doi.org/10.1155/2007/785626
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author N. Bhojak
D. D. Gudasaria
N. Khiwani
R. Jain
author_facet N. Bhojak
D. D. Gudasaria
N. Khiwani
R. Jain
author_sort N. Bhojak
collection DOAJ
description The present research work describes the synthesis, spectral and antibacterial studies on the complexes of Mn(II) with amide group containing ligands. Synthesis of complexes has been carried out by conventional method as well as by microwave method. The complexes have been characterized on the basis of elemental analysis, infrared, electronic spectra and magnetic susceptibility studies. The diffuse reflectance spectrums of the complexes show bands in the region 20,000 cm-1 to 26,000 cm-1 assignable to 6A1g → 4T2g and 6A1g → 4E1g transitions. These are also typical of tetrahedral environment around the manganese. The magnetic moment (5.80 BM) of the complex indicates high spin tetrahedral environment. The microwave method of synthesis of complexes have been found easier, convenient and ecofriendly.
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publisher Wiley
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series E-Journal of Chemistry
spelling doaj-art-56f374a9afbf454daf4ca0e490f475852025-02-03T06:42:28ZengWileyE-Journal of Chemistry0973-49452090-98102007-01-014223223710.1155/2007/785626Microwave Assisted Synthesis Spectral and Antibacterial Investigations on Complexes of Mn(II) With Amide Containing LigandsN. Bhojak0D. D. Gudasaria1N. Khiwani2R. Jain3Green Chemistry Research Centre, P.G. Department of Chemistry, Govt. Dungar College (A-Grade), University of Bikaner, Bikaner-334003, IndiaGreen Chemistry Research Centre, P.G. Department of Chemistry, Govt. Dungar College (A-Grade), University of Bikaner, Bikaner-334003, IndiaGreen Chemistry Research Centre, P.G. Department of Chemistry, Govt. Dungar College (A-Grade), University of Bikaner, Bikaner-334003, IndiaGreen Chemistry Research Centre, P.G. Department of Chemistry, Govt. Dungar College (A-Grade), University of Bikaner, Bikaner-334003, IndiaThe present research work describes the synthesis, spectral and antibacterial studies on the complexes of Mn(II) with amide group containing ligands. Synthesis of complexes has been carried out by conventional method as well as by microwave method. The complexes have been characterized on the basis of elemental analysis, infrared, electronic spectra and magnetic susceptibility studies. The diffuse reflectance spectrums of the complexes show bands in the region 20,000 cm-1 to 26,000 cm-1 assignable to 6A1g → 4T2g and 6A1g → 4E1g transitions. These are also typical of tetrahedral environment around the manganese. The magnetic moment (5.80 BM) of the complex indicates high spin tetrahedral environment. The microwave method of synthesis of complexes have been found easier, convenient and ecofriendly.http://dx.doi.org/10.1155/2007/785626
spellingShingle N. Bhojak
D. D. Gudasaria
N. Khiwani
R. Jain
Microwave Assisted Synthesis Spectral and Antibacterial Investigations on Complexes of Mn(II) With Amide Containing Ligands
E-Journal of Chemistry
title Microwave Assisted Synthesis Spectral and Antibacterial Investigations on Complexes of Mn(II) With Amide Containing Ligands
title_full Microwave Assisted Synthesis Spectral and Antibacterial Investigations on Complexes of Mn(II) With Amide Containing Ligands
title_fullStr Microwave Assisted Synthesis Spectral and Antibacterial Investigations on Complexes of Mn(II) With Amide Containing Ligands
title_full_unstemmed Microwave Assisted Synthesis Spectral and Antibacterial Investigations on Complexes of Mn(II) With Amide Containing Ligands
title_short Microwave Assisted Synthesis Spectral and Antibacterial Investigations on Complexes of Mn(II) With Amide Containing Ligands
title_sort microwave assisted synthesis spectral and antibacterial investigations on complexes of mn ii with amide containing ligands
url http://dx.doi.org/10.1155/2007/785626
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