H4SiW12O40 Catalyzed One-Pot Synthesis of 12-Aryl-8,9,10,12-tetrahydrobenzo[a] Xanthen-11-ones Under Solvent-Free Conditions
An efficient and environmentally benign protocol for the one-pot, three-component synthesis of 12-aryl-8,9,10,12-tetrahydro-benzo[a]xanthen-11-one derivatives by condensation of aryl aldehydes, 2-naphthol and dimedone using H4SiW12O40 (SiWA) as a reusable catalyst with high catalytic activity was re...
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Language: | English |
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Wiley
2012-01-01
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Series: | E-Journal of Chemistry |
Online Access: | http://dx.doi.org/10.1155/2012/930251 |
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author | A. Hassankhani E. Mosaddegh S. Y. Ebrahimipour |
author_facet | A. Hassankhani E. Mosaddegh S. Y. Ebrahimipour |
author_sort | A. Hassankhani |
collection | DOAJ |
description | An efficient and environmentally benign protocol for the one-pot, three-component synthesis of 12-aryl-8,9,10,12-tetrahydro-benzo[a]xanthen-11-one derivatives by condensation of aryl aldehydes, 2-naphthol and dimedone using H4SiW12O40 (SiWA) as a reusable catalyst with high catalytic activity was reported. The reaction was carried out at 100 ºC under solvent-free conditions within 15-40 min in 82-91% yield. |
format | Article |
id | doaj-art-52bf2b9deb124364a005106e7815114f |
institution | Kabale University |
issn | 0973-4945 2090-9810 |
language | English |
publishDate | 2012-01-01 |
publisher | Wiley |
record_format | Article |
series | E-Journal of Chemistry |
spelling | doaj-art-52bf2b9deb124364a005106e7815114f2025-02-03T06:07:21ZengWileyE-Journal of Chemistry0973-49452090-98102012-01-019278679010.1155/2012/930251H4SiW12O40 Catalyzed One-Pot Synthesis of 12-Aryl-8,9,10,12-tetrahydrobenzo[a] Xanthen-11-ones Under Solvent-Free ConditionsA. Hassankhani0E. Mosaddegh1S. Y. Ebrahimipour2Department of Materials Science, International Center for Science, High Technology & Environmental Sciences, P. O. Box 76315-117, Kerman, IranDepartment of Materials Science, International Center for Science, High Technology & Environmental Sciences, P. O. Box 76315-117, Kerman, IranDepartment of Chemistry, Payame Noor University (PNU), Mashhad, IranAn efficient and environmentally benign protocol for the one-pot, three-component synthesis of 12-aryl-8,9,10,12-tetrahydro-benzo[a]xanthen-11-one derivatives by condensation of aryl aldehydes, 2-naphthol and dimedone using H4SiW12O40 (SiWA) as a reusable catalyst with high catalytic activity was reported. The reaction was carried out at 100 ºC under solvent-free conditions within 15-40 min in 82-91% yield.http://dx.doi.org/10.1155/2012/930251 |
spellingShingle | A. Hassankhani E. Mosaddegh S. Y. Ebrahimipour H4SiW12O40 Catalyzed One-Pot Synthesis of 12-Aryl-8,9,10,12-tetrahydrobenzo[a] Xanthen-11-ones Under Solvent-Free Conditions E-Journal of Chemistry |
title | H4SiW12O40 Catalyzed One-Pot Synthesis of 12-Aryl-8,9,10,12-tetrahydrobenzo[a] Xanthen-11-ones Under Solvent-Free Conditions |
title_full | H4SiW12O40 Catalyzed One-Pot Synthesis of 12-Aryl-8,9,10,12-tetrahydrobenzo[a] Xanthen-11-ones Under Solvent-Free Conditions |
title_fullStr | H4SiW12O40 Catalyzed One-Pot Synthesis of 12-Aryl-8,9,10,12-tetrahydrobenzo[a] Xanthen-11-ones Under Solvent-Free Conditions |
title_full_unstemmed | H4SiW12O40 Catalyzed One-Pot Synthesis of 12-Aryl-8,9,10,12-tetrahydrobenzo[a] Xanthen-11-ones Under Solvent-Free Conditions |
title_short | H4SiW12O40 Catalyzed One-Pot Synthesis of 12-Aryl-8,9,10,12-tetrahydrobenzo[a] Xanthen-11-ones Under Solvent-Free Conditions |
title_sort | h4siw12o40 catalyzed one pot synthesis of 12 aryl 8 9 10 12 tetrahydrobenzo a xanthen 11 ones under solvent free conditions |
url | http://dx.doi.org/10.1155/2012/930251 |
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