Synthesis of silver leaves and their potential application for analysis and degradation of phenolic pollutants
Abstract A one‐pot bottom‐up synthesis method was used to synthesise multi‐level leaf‐like nano‐silver (silver leaf) by simply mixing AgNO3, L‐ascorbic acid, Sodium sodium citrate, and polyvinylpyrrolidone (PVP) in the ethanol‐water mixed solvents. Scanning electron microscopy (SEM) characterisation...
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| Format: | Article |
| Language: | English |
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Wiley
2022-05-01
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| Series: | IET Nanobiotechnology |
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| Online Access: | https://doi.org/10.1049/nbt2.12077 |
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| author | Jianan Sun Xianhui Gao Wei Wei |
| author_facet | Jianan Sun Xianhui Gao Wei Wei |
| author_sort | Jianan Sun |
| collection | DOAJ |
| description | Abstract A one‐pot bottom‐up synthesis method was used to synthesise multi‐level leaf‐like nano‐silver (silver leaf) by simply mixing AgNO3, L‐ascorbic acid, Sodium sodium citrate, and polyvinylpyrrolidone (PVP) in the ethanol‐water mixed solvents. Scanning electron microscopy (SEM) characterisations show that the silver leaves have tertiary structures and their sizes are controllable. In addition, silver leaves exhibit excellent Raman enhancement effect (SERS) and chemical catalytic activities for phenolic molecules. Interestingly, the SERS and catalytic activities increase as the size of the silver leaves decrease within a certain range, but when the size is too small, both of these performances weaken. The nanometre size and interstitial structure have a common amplification effect and influence on these activities. The present work not only showed a new method for the synthesis of silver leaves but also could be generalised to find other metallic leaves that could be used as promising heterogeneous catalysts for various reactions. The production of such small‐sized silver leaves will facilitate the analysis of phenolic pollutants through Raman enhancement and treat these pollutants through catalytic degradation. |
| format | Article |
| id | doaj-art-4998045e1f5842d2891cd8d8b9ea2736 |
| institution | Kabale University |
| issn | 1751-8741 1751-875X |
| language | English |
| publishDate | 2022-05-01 |
| publisher | Wiley |
| record_format | Article |
| series | IET Nanobiotechnology |
| spelling | doaj-art-4998045e1f5842d2891cd8d8b9ea27362025-02-03T01:29:25ZengWileyIET Nanobiotechnology1751-87411751-875X2022-05-01163788410.1049/nbt2.12077Synthesis of silver leaves and their potential application for analysis and degradation of phenolic pollutantsJianan Sun0Xianhui Gao1Wei Wei2Department of Basic Medicine Jinzhou Medical University Jinzhou ChinaDepartment of Basic Medicine Jinzhou Medical University Jinzhou ChinaDepartment of Basic Medicine Jinzhou Medical University Jinzhou ChinaAbstract A one‐pot bottom‐up synthesis method was used to synthesise multi‐level leaf‐like nano‐silver (silver leaf) by simply mixing AgNO3, L‐ascorbic acid, Sodium sodium citrate, and polyvinylpyrrolidone (PVP) in the ethanol‐water mixed solvents. Scanning electron microscopy (SEM) characterisations show that the silver leaves have tertiary structures and their sizes are controllable. In addition, silver leaves exhibit excellent Raman enhancement effect (SERS) and chemical catalytic activities for phenolic molecules. Interestingly, the SERS and catalytic activities increase as the size of the silver leaves decrease within a certain range, but when the size is too small, both of these performances weaken. The nanometre size and interstitial structure have a common amplification effect and influence on these activities. The present work not only showed a new method for the synthesis of silver leaves but also could be generalised to find other metallic leaves that could be used as promising heterogeneous catalysts for various reactions. The production of such small‐sized silver leaves will facilitate the analysis of phenolic pollutants through Raman enhancement and treat these pollutants through catalytic degradation.https://doi.org/10.1049/nbt2.12077catalysiselectrocatalysisleafSERSsilver leaves |
| spellingShingle | Jianan Sun Xianhui Gao Wei Wei Synthesis of silver leaves and their potential application for analysis and degradation of phenolic pollutants IET Nanobiotechnology catalysis electrocatalysis leaf SERS silver leaves |
| title | Synthesis of silver leaves and their potential application for analysis and degradation of phenolic pollutants |
| title_full | Synthesis of silver leaves and their potential application for analysis and degradation of phenolic pollutants |
| title_fullStr | Synthesis of silver leaves and their potential application for analysis and degradation of phenolic pollutants |
| title_full_unstemmed | Synthesis of silver leaves and their potential application for analysis and degradation of phenolic pollutants |
| title_short | Synthesis of silver leaves and their potential application for analysis and degradation of phenolic pollutants |
| title_sort | synthesis of silver leaves and their potential application for analysis and degradation of phenolic pollutants |
| topic | catalysis electrocatalysis leaf SERS silver leaves |
| url | https://doi.org/10.1049/nbt2.12077 |
| work_keys_str_mv | AT jianansun synthesisofsilverleavesandtheirpotentialapplicationforanalysisanddegradationofphenolicpollutants AT xianhuigao synthesisofsilverleavesandtheirpotentialapplicationforanalysisanddegradationofphenolicpollutants AT weiwei synthesisofsilverleavesandtheirpotentialapplicationforanalysisanddegradationofphenolicpollutants |