Synthesis, Structure, and Electrical Property of Ce1−xSr1+xGa3O7−δ
Ce1−xSr1+xGa3O7−δ powders were synthesized by a solid state reaction method under reducing atmosphere. Single melilite phase was obtained for x≤0.2. X-ray diffraction pattern displays a preferred orientation on (002) peak of the Ce0.9Sr1.1Ga3O7−δ composition. Scanning electron microscope disclosed t...
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Wiley
2015-01-01
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Series: | Advances in Materials Science and Engineering |
Online Access: | http://dx.doi.org/10.1155/2015/249348 |
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author | Xiaohui Li Jungu Xu Junshu Xiaofeng Xiaojun Kuang |
author_facet | Xiaohui Li Jungu Xu Junshu Xiaofeng Xiaojun Kuang |
author_sort | Xiaohui Li |
collection | DOAJ |
description | Ce1−xSr1+xGa3O7−δ powders were synthesized by a solid state reaction method under reducing atmosphere. Single melilite phase was obtained for x≤0.2. X-ray diffraction pattern displays a preferred orientation on (002) peak of the Ce0.9Sr1.1Ga3O7−δ composition. Scanning electron microscope disclosed the nanoscale needle-like micromorphology of this material, with an average length of ~2.5 μm and a diameter of ~500 nm. Transmission electron microscopy and selected area electron diffraction reveal the single crystal nature of these individual Ce0.9Sr1.1Ga3O7−δ needles and build up a relationship between the preferred orientation observed in X-ray diffraction pattern and the micromorphology. The phase stability of Ce1−xSr1+xGa3O7−δ in air was studied and the electrical property was investigated by impedance spectroscopy. |
format | Article |
id | doaj-art-4621bba8e09e434e8258187490984289 |
institution | Kabale University |
issn | 1687-8434 1687-8442 |
language | English |
publishDate | 2015-01-01 |
publisher | Wiley |
record_format | Article |
series | Advances in Materials Science and Engineering |
spelling | doaj-art-4621bba8e09e434e82581874909842892025-02-03T06:05:59ZengWileyAdvances in Materials Science and Engineering1687-84341687-84422015-01-01201510.1155/2015/249348249348Synthesis, Structure, and Electrical Property of Ce1−xSr1+xGa3O7−δXiaohui Li0Jungu Xu1Junshu Xiaofeng2Xiaojun Kuang3Guangxi Ministry-Province Jointly-Constructed Cultivation Base for State Key Laboratory of Processing for Non-Ferrous Metal and Featured Materials, MOE Key Laboratory of New Processing Technology for Nonferrous Metals and Materials, College of Materials Science and Engineering, Guangxi Universities Key Laboratory of Non-Ferrous Metal Oxide Electronic Functional Materials and Devices, Guilin University of Technology, Guilin 541004, ChinaGuangxi Ministry-Province Jointly-Constructed Cultivation Base for State Key Laboratory of Processing for Non-Ferrous Metal and Featured Materials, MOE Key Laboratory of New Processing Technology for Nonferrous Metals and Materials, College of Materials Science and Engineering, Guangxi Universities Key Laboratory of Non-Ferrous Metal Oxide Electronic Functional Materials and Devices, Guilin University of Technology, Guilin 541004, ChinaGuangxi Ministry-Province Jointly-Constructed Cultivation Base for State Key Laboratory of Processing for Non-Ferrous Metal and Featured Materials, MOE Key Laboratory of New Processing Technology for Nonferrous Metals and Materials, College of Materials Science and Engineering, Guangxi Universities Key Laboratory of Non-Ferrous Metal Oxide Electronic Functional Materials and Devices, Guilin University of Technology, Guilin 541004, ChinaGuangxi Ministry-Province Jointly-Constructed Cultivation Base for State Key Laboratory of Processing for Non-Ferrous Metal and Featured Materials, MOE Key Laboratory of New Processing Technology for Nonferrous Metals and Materials, College of Materials Science and Engineering, Guangxi Universities Key Laboratory of Non-Ferrous Metal Oxide Electronic Functional Materials and Devices, Guilin University of Technology, Guilin 541004, ChinaCe1−xSr1+xGa3O7−δ powders were synthesized by a solid state reaction method under reducing atmosphere. Single melilite phase was obtained for x≤0.2. X-ray diffraction pattern displays a preferred orientation on (002) peak of the Ce0.9Sr1.1Ga3O7−δ composition. Scanning electron microscope disclosed the nanoscale needle-like micromorphology of this material, with an average length of ~2.5 μm and a diameter of ~500 nm. Transmission electron microscopy and selected area electron diffraction reveal the single crystal nature of these individual Ce0.9Sr1.1Ga3O7−δ needles and build up a relationship between the preferred orientation observed in X-ray diffraction pattern and the micromorphology. The phase stability of Ce1−xSr1+xGa3O7−δ in air was studied and the electrical property was investigated by impedance spectroscopy.http://dx.doi.org/10.1155/2015/249348 |
spellingShingle | Xiaohui Li Jungu Xu Junshu Xiaofeng Xiaojun Kuang Synthesis, Structure, and Electrical Property of Ce1−xSr1+xGa3O7−δ Advances in Materials Science and Engineering |
title | Synthesis, Structure, and Electrical Property of Ce1−xSr1+xGa3O7−δ |
title_full | Synthesis, Structure, and Electrical Property of Ce1−xSr1+xGa3O7−δ |
title_fullStr | Synthesis, Structure, and Electrical Property of Ce1−xSr1+xGa3O7−δ |
title_full_unstemmed | Synthesis, Structure, and Electrical Property of Ce1−xSr1+xGa3O7−δ |
title_short | Synthesis, Structure, and Electrical Property of Ce1−xSr1+xGa3O7−δ |
title_sort | synthesis structure and electrical property of ce1 xsr1 xga3o7 δ |
url | http://dx.doi.org/10.1155/2015/249348 |
work_keys_str_mv | AT xiaohuili synthesisstructureandelectricalpropertyofce1xsr1xga3o7d AT junguxu synthesisstructureandelectricalpropertyofce1xsr1xga3o7d AT junshuxiaofeng synthesisstructureandelectricalpropertyofce1xsr1xga3o7d AT xiaojunkuang synthesisstructureandelectricalpropertyofce1xsr1xga3o7d |