Effects of ultrasonication on electrical and self-sensing properties for fiber-reinforced cementitious composites containing MWCNTs

The uniform dispersion of carbon nanotubes (CNTs) is essential for enhancing the mechanical and electrical properties of cement composites. This improvement significantly increases their potential for use in embedded self-sensing applications within structural health monitoring (SHM) systems, which...

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Main Authors: Jin-Seok Woo, Ai-Hua Jin, Hyun-Do Yun, Junhee Yu, Je Hyun Bae, Sun-Woo Kim, Soo-Yeon Seo, Gun-Cheol Lee, Seongwon Hong, Kang-Soo Kim, Sangyoung Han
Format: Article
Language:English
Published: Elsevier 2025-01-01
Series:Journal of Materials Research and Technology
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Online Access:http://www.sciencedirect.com/science/article/pii/S2238785424029612
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author Jin-Seok Woo
Ai-Hua Jin
Hyun-Do Yun
Junhee Yu
Je Hyun Bae
Sun-Woo Kim
Soo-Yeon Seo
Gun-Cheol Lee
Seongwon Hong
Kang-Soo Kim
Sangyoung Han
author_facet Jin-Seok Woo
Ai-Hua Jin
Hyun-Do Yun
Junhee Yu
Je Hyun Bae
Sun-Woo Kim
Soo-Yeon Seo
Gun-Cheol Lee
Seongwon Hong
Kang-Soo Kim
Sangyoung Han
author_sort Jin-Seok Woo
collection DOAJ
description The uniform dispersion of carbon nanotubes (CNTs) is essential for enhancing the mechanical and electrical properties of cement composites. This improvement significantly increases their potential for use in embedded self-sensing applications within structural health monitoring (SHM) systems, which are defined as systems for monitoring, assessing, and evaluating structural conditions. To take advantage of this benefit, multi-walled carbon nanotubes (MWCNTs) were incorporated into fiber-reinforced cementitious composites, and the optimal method for achieving uniform dispersion was investigated by applying a specific ultrasonic dispersion energy level. The results revealed that the E500-CFRC specimen, treated with an ultrasonic energy of 500 J, achieved proper dispersion of MWCNTs, as evidenced by SEM images. This uniform dispersion significantly improved its mechanical strengths compared to other specimens. Additionally, this optimal dispersion within the cementitious composite enhanced self-sensing capability, accuracy to strain changes, and repeatability, indicating strong self-sensing capabilities. These results were validated by the strongest linear correlation observed between fractional change in resistance and compressive strain, with an R2 value of 0.935, outperforming other specimens. Furthermore, the proposed method enables well-dispersed MWCNTs to be integrated into a pre-mixed cementitious composite using the standardized mixing method, making it adaptable to a variety of cementitious mixtures. Given the limited research on the self-SHM performance of MWCNTs-filled cementitious composites under varying ultrasonic dispersion energy levels, this study contributes significantly to advancing the self-monitoring capabilities of reinforced concrete structures.
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publishDate 2025-01-01
publisher Elsevier
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spelling doaj-art-443035bc9ccc4e90a6b3d742e4d8d6432025-01-19T06:25:39ZengElsevierJournal of Materials Research and Technology2238-78542025-01-013415091528Effects of ultrasonication on electrical and self-sensing properties for fiber-reinforced cementitious composites containing MWCNTsJin-Seok Woo0Ai-Hua Jin1Hyun-Do Yun2Junhee Yu3Je Hyun Bae4Sun-Woo Kim5Soo-Yeon Seo6Gun-Cheol Lee7Seongwon Hong8Kang-Soo Kim9Sangyoung Han10Department of Architectural Engineering, Chungnam National University, Daejeon, 34134, Republic of KoreaDepartment of Architectural Engineering, Chungnam National University, Daejeon, 34134, Republic of KoreaDepartment of Architectural Engineering, Chungnam National University, Daejeon, 34134, Republic of Korea; Corresponding author.Graduate School of Analytical Science and Technology (GRAST), Chungnam National University, Daejeon, 34134, Republic of KoreaGraduate School of Analytical Science and Technology (GRAST), Chungnam National University, Daejeon, 34134, Republic of KoreaDepartment of Construction Engineering Education, Chungnam National University, Daejeon, 34134, Republic of Korea; Corresponding author.Department of Architectural Engineering, Korea National University of Transportation, Chungju, 27469, Republic of KoreaDepartment of Architectural Engineering, Korea National University of Transportation, Chungju, 27469, Republic of KoreaDepartment of Safety Engineering, Korea National University of Transportation, Chungju, 27469, Republic of KoreaDepartment of Architectural Engineering, University of Seoul, Seoul, 02504, Republic of KoreaDepartment of ICT Integrated Ocean Smart City Engineering, Dong-A University, Busan, 49315, Republic of Korea; Corresponding author.The uniform dispersion of carbon nanotubes (CNTs) is essential for enhancing the mechanical and electrical properties of cement composites. This improvement significantly increases their potential for use in embedded self-sensing applications within structural health monitoring (SHM) systems, which are defined as systems for monitoring, assessing, and evaluating structural conditions. To take advantage of this benefit, multi-walled carbon nanotubes (MWCNTs) were incorporated into fiber-reinforced cementitious composites, and the optimal method for achieving uniform dispersion was investigated by applying a specific ultrasonic dispersion energy level. The results revealed that the E500-CFRC specimen, treated with an ultrasonic energy of 500 J, achieved proper dispersion of MWCNTs, as evidenced by SEM images. This uniform dispersion significantly improved its mechanical strengths compared to other specimens. Additionally, this optimal dispersion within the cementitious composite enhanced self-sensing capability, accuracy to strain changes, and repeatability, indicating strong self-sensing capabilities. These results were validated by the strongest linear correlation observed between fractional change in resistance and compressive strain, with an R2 value of 0.935, outperforming other specimens. Furthermore, the proposed method enables well-dispersed MWCNTs to be integrated into a pre-mixed cementitious composite using the standardized mixing method, making it adaptable to a variety of cementitious mixtures. Given the limited research on the self-SHM performance of MWCNTs-filled cementitious composites under varying ultrasonic dispersion energy levels, this study contributes significantly to advancing the self-monitoring capabilities of reinforced concrete structures.http://www.sciencedirect.com/science/article/pii/S2238785424029612Structural health monitoringSelf-sensing capabilityMulti-walled carbon nanotubesMWCNTs-filled cementitious compositePolyethylene fiberSteel fiber
spellingShingle Jin-Seok Woo
Ai-Hua Jin
Hyun-Do Yun
Junhee Yu
Je Hyun Bae
Sun-Woo Kim
Soo-Yeon Seo
Gun-Cheol Lee
Seongwon Hong
Kang-Soo Kim
Sangyoung Han
Effects of ultrasonication on electrical and self-sensing properties for fiber-reinforced cementitious composites containing MWCNTs
Journal of Materials Research and Technology
Structural health monitoring
Self-sensing capability
Multi-walled carbon nanotubes
MWCNTs-filled cementitious composite
Polyethylene fiber
Steel fiber
title Effects of ultrasonication on electrical and self-sensing properties for fiber-reinforced cementitious composites containing MWCNTs
title_full Effects of ultrasonication on electrical and self-sensing properties for fiber-reinforced cementitious composites containing MWCNTs
title_fullStr Effects of ultrasonication on electrical and self-sensing properties for fiber-reinforced cementitious composites containing MWCNTs
title_full_unstemmed Effects of ultrasonication on electrical and self-sensing properties for fiber-reinforced cementitious composites containing MWCNTs
title_short Effects of ultrasonication on electrical and self-sensing properties for fiber-reinforced cementitious composites containing MWCNTs
title_sort effects of ultrasonication on electrical and self sensing properties for fiber reinforced cementitious composites containing mwcnts
topic Structural health monitoring
Self-sensing capability
Multi-walled carbon nanotubes
MWCNTs-filled cementitious composite
Polyethylene fiber
Steel fiber
url http://www.sciencedirect.com/science/article/pii/S2238785424029612
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