Analysis of Metal Contents in Portland Type V and MTA-Based Cements

The aim of this study was to determine, by Atomic Absorption Spectrometry (AAS), the concentration levels of 11 metals in Type V gray and structural white PC, ProRoot MTA, and MTA Bio. Samples, containing one gram of each tested cement, were prepared and transferred to a 100 mL Teflon tube with a mi...

Full description

Saved in:
Bibliographic Details
Main Authors: Maura Cristiane Gonçales Orçati Dorileo, Matheus Coelho Bandeca, Fábio Luis Miranda Pedro, Luiz Evaristo Ricci Volpato, Orlando Aguirre Guedes, Ricardo Dalla Villa, Mateus Rodrigues Tonetto, Alvaro Henrique Borges
Format: Article
Language:English
Published: Wiley 2014-01-01
Series:The Scientific World Journal
Online Access:http://dx.doi.org/10.1155/2014/983728
Tags: Add Tag
No Tags, Be the first to tag this record!
_version_ 1832561213170515968
author Maura Cristiane Gonçales Orçati Dorileo
Matheus Coelho Bandeca
Fábio Luis Miranda Pedro
Luiz Evaristo Ricci Volpato
Orlando Aguirre Guedes
Ricardo Dalla Villa
Mateus Rodrigues Tonetto
Alvaro Henrique Borges
author_facet Maura Cristiane Gonçales Orçati Dorileo
Matheus Coelho Bandeca
Fábio Luis Miranda Pedro
Luiz Evaristo Ricci Volpato
Orlando Aguirre Guedes
Ricardo Dalla Villa
Mateus Rodrigues Tonetto
Alvaro Henrique Borges
author_sort Maura Cristiane Gonçales Orçati Dorileo
collection DOAJ
description The aim of this study was to determine, by Atomic Absorption Spectrometry (AAS), the concentration levels of 11 metals in Type V gray and structural white PC, ProRoot MTA, and MTA Bio. Samples, containing one gram of each tested cement, were prepared and transferred to a 100 mL Teflon tube with a mixture of 7.0 mL of nitric acid and 21 mL of hydrochloric acid. After the reaction, the mixture was filtered and then volumed to 50 mL of distilled water. For each metal, specific patterns were determined from universal standards. Arsenic quantification was performed by hydride generator. The analysis was performed five times and the data were statistically analyzed at 5% level of significance. Only the cadmium presented concentration levels of values lower than the quantification limit of the device. The AAS analysis showed increased levels of calcium, nickel, and zinc in structural white PC. Type V PC presented the greatest concentration levels of arsenic, chromium, copper, iron, lead, and manganese (P<0.05). Bismuth was found in all cements, and the lowest concentration levels were observed in Portland cements, while the highest were observed in ProRoot MTA. Both PC and MTA-based cements showed evidence of metals inclusion.
format Article
id doaj-art-42fe3484569d4b48aa900b14bd530185
institution Kabale University
issn 2356-6140
1537-744X
language English
publishDate 2014-01-01
publisher Wiley
record_format Article
series The Scientific World Journal
spelling doaj-art-42fe3484569d4b48aa900b14bd5301852025-02-03T01:25:39ZengWileyThe Scientific World Journal2356-61401537-744X2014-01-01201410.1155/2014/983728983728Analysis of Metal Contents in Portland Type V and MTA-Based CementsMaura Cristiane Gonçales Orçati Dorileo0Matheus Coelho Bandeca1Fábio Luis Miranda Pedro2Luiz Evaristo Ricci Volpato3Orlando Aguirre Guedes4Ricardo Dalla Villa5Mateus Rodrigues Tonetto6Alvaro Henrique Borges7Faculty of Dentistry, University of Cuiaba, Avenida Manoel Jose de Arruda 3.100, Jardim Europa, 78065-900 Cuiaba, MT, BrazilMaster’s Program in Dentistry, UNICEUMA, Rua Josue Montello 01, Renascenca, 65075-120 São Luıs, MA, BrazilFaculty of Dentistry, University of Cuiaba, Avenida Manoel Jose de Arruda 3.100, Jardim Europa, 78065-900 Cuiaba, MT, BrazilFaculty of Dentistry, University of Cuiaba, Avenida Manoel Jose de Arruda 3.100, Jardim Europa, 78065-900 Cuiaba, MT, BrazilFaculty of Dentistry, University of Cuiaba, Avenida Manoel Jose de Arruda 3.100, Jardim Europa, 78065-900 Cuiaba, MT, BrazilMaster’s Program in Chemistry, Mato Grosso Federal University, Avenida Fernando Correa da Costa 2367, Boa Esperanca, 78060-900 Cuiaba, MT, BrazilFaculty of Dentistry, University of Cuiaba, Avenida Manoel Jose de Arruda 3.100, Jardim Europa, 78065-900 Cuiaba, MT, BrazilMaster’s Program in Integrated Dentistry Science, Faculty of Dentistry, University of Cuiaba, Avenida Manoel Jose de Arruda 3.100, Jardim Europa, 78065-900 Cuiaba, MT, BrazilThe aim of this study was to determine, by Atomic Absorption Spectrometry (AAS), the concentration levels of 11 metals in Type V gray and structural white PC, ProRoot MTA, and MTA Bio. Samples, containing one gram of each tested cement, were prepared and transferred to a 100 mL Teflon tube with a mixture of 7.0 mL of nitric acid and 21 mL of hydrochloric acid. After the reaction, the mixture was filtered and then volumed to 50 mL of distilled water. For each metal, specific patterns were determined from universal standards. Arsenic quantification was performed by hydride generator. The analysis was performed five times and the data were statistically analyzed at 5% level of significance. Only the cadmium presented concentration levels of values lower than the quantification limit of the device. The AAS analysis showed increased levels of calcium, nickel, and zinc in structural white PC. Type V PC presented the greatest concentration levels of arsenic, chromium, copper, iron, lead, and manganese (P<0.05). Bismuth was found in all cements, and the lowest concentration levels were observed in Portland cements, while the highest were observed in ProRoot MTA. Both PC and MTA-based cements showed evidence of metals inclusion.http://dx.doi.org/10.1155/2014/983728
spellingShingle Maura Cristiane Gonçales Orçati Dorileo
Matheus Coelho Bandeca
Fábio Luis Miranda Pedro
Luiz Evaristo Ricci Volpato
Orlando Aguirre Guedes
Ricardo Dalla Villa
Mateus Rodrigues Tonetto
Alvaro Henrique Borges
Analysis of Metal Contents in Portland Type V and MTA-Based Cements
The Scientific World Journal
title Analysis of Metal Contents in Portland Type V and MTA-Based Cements
title_full Analysis of Metal Contents in Portland Type V and MTA-Based Cements
title_fullStr Analysis of Metal Contents in Portland Type V and MTA-Based Cements
title_full_unstemmed Analysis of Metal Contents in Portland Type V and MTA-Based Cements
title_short Analysis of Metal Contents in Portland Type V and MTA-Based Cements
title_sort analysis of metal contents in portland type v and mta based cements
url http://dx.doi.org/10.1155/2014/983728
work_keys_str_mv AT mauracristianegoncalesorcatidorileo analysisofmetalcontentsinportlandtypevandmtabasedcements
AT matheuscoelhobandeca analysisofmetalcontentsinportlandtypevandmtabasedcements
AT fabioluismirandapedro analysisofmetalcontentsinportlandtypevandmtabasedcements
AT luizevaristoriccivolpato analysisofmetalcontentsinportlandtypevandmtabasedcements
AT orlandoaguirreguedes analysisofmetalcontentsinportlandtypevandmtabasedcements
AT ricardodallavilla analysisofmetalcontentsinportlandtypevandmtabasedcements
AT mateusrodriguestonetto analysisofmetalcontentsinportlandtypevandmtabasedcements
AT alvarohenriqueborges analysisofmetalcontentsinportlandtypevandmtabasedcements