Analysis of Metal Contents in Portland Type V and MTA-Based Cements
The aim of this study was to determine, by Atomic Absorption Spectrometry (AAS), the concentration levels of 11 metals in Type V gray and structural white PC, ProRoot MTA, and MTA Bio. Samples, containing one gram of each tested cement, were prepared and transferred to a 100 mL Teflon tube with a mi...
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2014-01-01
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Series: | The Scientific World Journal |
Online Access: | http://dx.doi.org/10.1155/2014/983728 |
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author | Maura Cristiane Gonçales Orçati Dorileo Matheus Coelho Bandeca Fábio Luis Miranda Pedro Luiz Evaristo Ricci Volpato Orlando Aguirre Guedes Ricardo Dalla Villa Mateus Rodrigues Tonetto Alvaro Henrique Borges |
author_facet | Maura Cristiane Gonçales Orçati Dorileo Matheus Coelho Bandeca Fábio Luis Miranda Pedro Luiz Evaristo Ricci Volpato Orlando Aguirre Guedes Ricardo Dalla Villa Mateus Rodrigues Tonetto Alvaro Henrique Borges |
author_sort | Maura Cristiane Gonçales Orçati Dorileo |
collection | DOAJ |
description | The aim of this study was to determine, by Atomic Absorption Spectrometry (AAS), the concentration levels of 11 metals in Type V gray and structural white PC, ProRoot MTA, and MTA Bio. Samples, containing one gram of each tested cement, were prepared and transferred to a 100 mL Teflon tube with a mixture of 7.0 mL of nitric acid and 21 mL of hydrochloric acid. After the reaction, the mixture was filtered and then volumed to 50 mL of distilled water. For each metal, specific patterns were determined from universal standards. Arsenic quantification was performed by hydride generator. The analysis was performed five times and the data were statistically analyzed at 5% level of significance. Only the cadmium presented concentration levels of values lower than the quantification limit of the device. The AAS analysis showed increased levels of calcium, nickel, and zinc in structural white PC. Type V PC presented the greatest concentration levels of arsenic, chromium, copper, iron, lead, and manganese (P<0.05). Bismuth was found in all cements, and the lowest concentration levels were observed in Portland cements, while the highest were observed in ProRoot MTA. Both PC and MTA-based cements showed evidence of metals inclusion. |
format | Article |
id | doaj-art-42fe3484569d4b48aa900b14bd530185 |
institution | Kabale University |
issn | 2356-6140 1537-744X |
language | English |
publishDate | 2014-01-01 |
publisher | Wiley |
record_format | Article |
series | The Scientific World Journal |
spelling | doaj-art-42fe3484569d4b48aa900b14bd5301852025-02-03T01:25:39ZengWileyThe Scientific World Journal2356-61401537-744X2014-01-01201410.1155/2014/983728983728Analysis of Metal Contents in Portland Type V and MTA-Based CementsMaura Cristiane Gonçales Orçati Dorileo0Matheus Coelho Bandeca1Fábio Luis Miranda Pedro2Luiz Evaristo Ricci Volpato3Orlando Aguirre Guedes4Ricardo Dalla Villa5Mateus Rodrigues Tonetto6Alvaro Henrique Borges7Faculty of Dentistry, University of Cuiaba, Avenida Manoel Jose de Arruda 3.100, Jardim Europa, 78065-900 Cuiaba, MT, BrazilMaster’s Program in Dentistry, UNICEUMA, Rua Josue Montello 01, Renascenca, 65075-120 São Luıs, MA, BrazilFaculty of Dentistry, University of Cuiaba, Avenida Manoel Jose de Arruda 3.100, Jardim Europa, 78065-900 Cuiaba, MT, BrazilFaculty of Dentistry, University of Cuiaba, Avenida Manoel Jose de Arruda 3.100, Jardim Europa, 78065-900 Cuiaba, MT, BrazilFaculty of Dentistry, University of Cuiaba, Avenida Manoel Jose de Arruda 3.100, Jardim Europa, 78065-900 Cuiaba, MT, BrazilMaster’s Program in Chemistry, Mato Grosso Federal University, Avenida Fernando Correa da Costa 2367, Boa Esperanca, 78060-900 Cuiaba, MT, BrazilFaculty of Dentistry, University of Cuiaba, Avenida Manoel Jose de Arruda 3.100, Jardim Europa, 78065-900 Cuiaba, MT, BrazilMaster’s Program in Integrated Dentistry Science, Faculty of Dentistry, University of Cuiaba, Avenida Manoel Jose de Arruda 3.100, Jardim Europa, 78065-900 Cuiaba, MT, BrazilThe aim of this study was to determine, by Atomic Absorption Spectrometry (AAS), the concentration levels of 11 metals in Type V gray and structural white PC, ProRoot MTA, and MTA Bio. Samples, containing one gram of each tested cement, were prepared and transferred to a 100 mL Teflon tube with a mixture of 7.0 mL of nitric acid and 21 mL of hydrochloric acid. After the reaction, the mixture was filtered and then volumed to 50 mL of distilled water. For each metal, specific patterns were determined from universal standards. Arsenic quantification was performed by hydride generator. The analysis was performed five times and the data were statistically analyzed at 5% level of significance. Only the cadmium presented concentration levels of values lower than the quantification limit of the device. The AAS analysis showed increased levels of calcium, nickel, and zinc in structural white PC. Type V PC presented the greatest concentration levels of arsenic, chromium, copper, iron, lead, and manganese (P<0.05). Bismuth was found in all cements, and the lowest concentration levels were observed in Portland cements, while the highest were observed in ProRoot MTA. Both PC and MTA-based cements showed evidence of metals inclusion.http://dx.doi.org/10.1155/2014/983728 |
spellingShingle | Maura Cristiane Gonçales Orçati Dorileo Matheus Coelho Bandeca Fábio Luis Miranda Pedro Luiz Evaristo Ricci Volpato Orlando Aguirre Guedes Ricardo Dalla Villa Mateus Rodrigues Tonetto Alvaro Henrique Borges Analysis of Metal Contents in Portland Type V and MTA-Based Cements The Scientific World Journal |
title | Analysis of Metal Contents in Portland Type V and MTA-Based Cements |
title_full | Analysis of Metal Contents in Portland Type V and MTA-Based Cements |
title_fullStr | Analysis of Metal Contents in Portland Type V and MTA-Based Cements |
title_full_unstemmed | Analysis of Metal Contents in Portland Type V and MTA-Based Cements |
title_short | Analysis of Metal Contents in Portland Type V and MTA-Based Cements |
title_sort | analysis of metal contents in portland type v and mta based cements |
url | http://dx.doi.org/10.1155/2014/983728 |
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