Volatile Components of Haplophyllum canaliculatum Boiss. by Different Extraction Procedures
Volatile components of Haplophyllum canaliculatum Boiss. grown in Iran were extracted by hydrodistillation (HD), solvent-free microwave extraction (SFME), and headspace solid-phase microextraction (HS-SPME). The components were analyzed by means of GC and GC-MS. The extraction time and temperature f...
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| Format: | Article |
| Language: | English |
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Wiley
2020-01-01
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| Series: | Journal of Analytical Methods in Chemistry |
| Online Access: | http://dx.doi.org/10.1155/2020/4202871 |
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| author | Nastaran Ahadi Marzieh Torabbeigi Zahra Aghaiee Meibodei Fatemeh Safatian |
| author_facet | Nastaran Ahadi Marzieh Torabbeigi Zahra Aghaiee Meibodei Fatemeh Safatian |
| author_sort | Nastaran Ahadi |
| collection | DOAJ |
| description | Volatile components of Haplophyllum canaliculatum Boiss. grown in Iran were extracted by hydrodistillation (HD), solvent-free microwave extraction (SFME), and headspace solid-phase microextraction (HS-SPME). The components were analyzed by means of GC and GC-MS. The extraction time and temperature for HS-SPME, microwave, power, and exposure time of extraction for SFME were optimized. Twenty-five compounds that represent 99.88% of total compounds in the oil were obtained by the HD method, and the major components for this method were identified as β-pinene (18.90%), 1,8-cineole (13.94%), and piperitone (12.22%). However, piperitone (34.50%), caryophyllene oxide (9.94%), and a-eudesmol were the main compounds among twenty-one constituents, representing 99.89% of the total composition that were characterized in volatiles extracted by the SFME method. Moreover, thirteen compounds, representing 99.95% of the total constituents, were characterized in volatile fraction extracted by the HS-SPME method, which were dominated by β-pinene (21.13%), a-pinene (13.07%), limonene (11.65%), and δ-2-carene (10.23%) as major constituents. |
| format | Article |
| id | doaj-art-41cbe458e9fd40abb691cc4ea4f699e0 |
| institution | Kabale University |
| issn | 2090-8865 2090-8873 |
| language | English |
| publishDate | 2020-01-01 |
| publisher | Wiley |
| record_format | Article |
| series | Journal of Analytical Methods in Chemistry |
| spelling | doaj-art-41cbe458e9fd40abb691cc4ea4f699e02025-02-03T01:04:23ZengWileyJournal of Analytical Methods in Chemistry2090-88652090-88732020-01-01202010.1155/2020/42028714202871Volatile Components of Haplophyllum canaliculatum Boiss. by Different Extraction ProceduresNastaran Ahadi0Marzieh Torabbeigi1Zahra Aghaiee Meibodei2Fatemeh Safatian3Pharmaceutical Science Branch, Islamic Azad University, Tehran, IranSchool of Public Health and Safety, Shahid Beheshti University of Medical Sciences, P.O. Box 16858-116, Tehran, IranDepartment of Chemistry, East Branch of Tehran (Ghiam Dasht), Islamic Azad University, Tehran, IranRamsar International Branch, Mazandaran University of Medical Sciences, Ramsar, IranVolatile components of Haplophyllum canaliculatum Boiss. grown in Iran were extracted by hydrodistillation (HD), solvent-free microwave extraction (SFME), and headspace solid-phase microextraction (HS-SPME). The components were analyzed by means of GC and GC-MS. The extraction time and temperature for HS-SPME, microwave, power, and exposure time of extraction for SFME were optimized. Twenty-five compounds that represent 99.88% of total compounds in the oil were obtained by the HD method, and the major components for this method were identified as β-pinene (18.90%), 1,8-cineole (13.94%), and piperitone (12.22%). However, piperitone (34.50%), caryophyllene oxide (9.94%), and a-eudesmol were the main compounds among twenty-one constituents, representing 99.89% of the total composition that were characterized in volatiles extracted by the SFME method. Moreover, thirteen compounds, representing 99.95% of the total constituents, were characterized in volatile fraction extracted by the HS-SPME method, which were dominated by β-pinene (21.13%), a-pinene (13.07%), limonene (11.65%), and δ-2-carene (10.23%) as major constituents.http://dx.doi.org/10.1155/2020/4202871 |
| spellingShingle | Nastaran Ahadi Marzieh Torabbeigi Zahra Aghaiee Meibodei Fatemeh Safatian Volatile Components of Haplophyllum canaliculatum Boiss. by Different Extraction Procedures Journal of Analytical Methods in Chemistry |
| title | Volatile Components of Haplophyllum canaliculatum Boiss. by Different Extraction Procedures |
| title_full | Volatile Components of Haplophyllum canaliculatum Boiss. by Different Extraction Procedures |
| title_fullStr | Volatile Components of Haplophyllum canaliculatum Boiss. by Different Extraction Procedures |
| title_full_unstemmed | Volatile Components of Haplophyllum canaliculatum Boiss. by Different Extraction Procedures |
| title_short | Volatile Components of Haplophyllum canaliculatum Boiss. by Different Extraction Procedures |
| title_sort | volatile components of haplophyllum canaliculatum boiss by different extraction procedures |
| url | http://dx.doi.org/10.1155/2020/4202871 |
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