Electrophoretic Deposition of Aluminum Nitride from Its Suspension in Acetylacetone Using Iodine as an Additive
We have studied electrophoretic deposition of AlN from its suspension in acetylacetone with I2 as an additive. AlN powder with particle size <10 μm is dispersed to produce a positive charge and deposited on the cathode by applying fields greater than 10 V/cm between the electrodes. X-ray diffrac...
Saved in:
Main Authors: | , , |
---|---|
Format: | Article |
Language: | English |
Published: |
Wiley
2013-01-01
|
Series: | Journal of Chemistry |
Online Access: | http://dx.doi.org/10.1155/2013/489734 |
Tags: |
Add Tag
No Tags, Be the first to tag this record!
|
_version_ | 1832560027821408256 |
---|---|
author | Bizuneh Workie Brian E. McCandless Zewdu Gebeyehu |
author_facet | Bizuneh Workie Brian E. McCandless Zewdu Gebeyehu |
author_sort | Bizuneh Workie |
collection | DOAJ |
description | We have studied electrophoretic deposition of AlN from its suspension in acetylacetone with I2 as an additive. AlN powder with particle size <10 μm is dispersed to produce a positive charge and deposited on the cathode by applying fields greater than 10 V/cm between the electrodes. X-ray diffraction and FTIR studies indicate that the AlN before and after deposition has the same composition and structure. An increase in the amount of AlN in the suspension, the deposition potential, and the deposition time results in a linear increase in the weight of the AlN deposited. Electrophoretic deposition from 10 g/L AlN suspension shows an initial increase in the weight of AlN deposited with the concentration of I2, and the weight of AlN decreases after reaching a maximum at 0.20 g/L I2. |
format | Article |
id | doaj-art-410810d1927440b5905da5e308ebf7fe |
institution | Kabale University |
issn | 2090-9063 2090-9071 |
language | English |
publishDate | 2013-01-01 |
publisher | Wiley |
record_format | Article |
series | Journal of Chemistry |
spelling | doaj-art-410810d1927440b5905da5e308ebf7fe2025-02-03T01:28:37ZengWileyJournal of Chemistry2090-90632090-90712013-01-01201310.1155/2013/489734489734Electrophoretic Deposition of Aluminum Nitride from Its Suspension in Acetylacetone Using Iodine as an AdditiveBizuneh Workie0Brian E. McCandless1Zewdu Gebeyehu2Department of Chemistry, Delaware State University, 1200 N. DuPont Highway, Dover, DE 19901, USAInstitute of Energy Conversion, University of Delaware, Newark, DE 19716, USADepartment of Chemistry, Columbus State University, Columbus, GA 31907, USAWe have studied electrophoretic deposition of AlN from its suspension in acetylacetone with I2 as an additive. AlN powder with particle size <10 μm is dispersed to produce a positive charge and deposited on the cathode by applying fields greater than 10 V/cm between the electrodes. X-ray diffraction and FTIR studies indicate that the AlN before and after deposition has the same composition and structure. An increase in the amount of AlN in the suspension, the deposition potential, and the deposition time results in a linear increase in the weight of the AlN deposited. Electrophoretic deposition from 10 g/L AlN suspension shows an initial increase in the weight of AlN deposited with the concentration of I2, and the weight of AlN decreases after reaching a maximum at 0.20 g/L I2.http://dx.doi.org/10.1155/2013/489734 |
spellingShingle | Bizuneh Workie Brian E. McCandless Zewdu Gebeyehu Electrophoretic Deposition of Aluminum Nitride from Its Suspension in Acetylacetone Using Iodine as an Additive Journal of Chemistry |
title | Electrophoretic Deposition of Aluminum Nitride from Its Suspension in Acetylacetone Using Iodine as an Additive |
title_full | Electrophoretic Deposition of Aluminum Nitride from Its Suspension in Acetylacetone Using Iodine as an Additive |
title_fullStr | Electrophoretic Deposition of Aluminum Nitride from Its Suspension in Acetylacetone Using Iodine as an Additive |
title_full_unstemmed | Electrophoretic Deposition of Aluminum Nitride from Its Suspension in Acetylacetone Using Iodine as an Additive |
title_short | Electrophoretic Deposition of Aluminum Nitride from Its Suspension in Acetylacetone Using Iodine as an Additive |
title_sort | electrophoretic deposition of aluminum nitride from its suspension in acetylacetone using iodine as an additive |
url | http://dx.doi.org/10.1155/2013/489734 |
work_keys_str_mv | AT bizunehworkie electrophoreticdepositionofaluminumnitridefromitssuspensioninacetylacetoneusingiodineasanadditive AT brianemccandless electrophoreticdepositionofaluminumnitridefromitssuspensioninacetylacetoneusingiodineasanadditive AT zewdugebeyehu electrophoreticdepositionofaluminumnitridefromitssuspensioninacetylacetoneusingiodineasanadditive |