Physical, Mechanical, and Thermal Analysis of Polylactic Acid/Fumed Silica/Clay (1.28E) Nanocomposites
Polylactic acid/fumed silica/clay (PLA/FS/clay) (1.28E) nanocomposites have been successfully prepared by solution-intercalation film-casting technique. The resultant nanocomposites were characterized by Fourier Transform Infrared Spectroscopy (FT-IR), Scanning Electron Microscopy (SEM), tensile tes...
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Format: | Article |
Language: | English |
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Wiley
2015-01-01
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Series: | International Journal of Polymer Science |
Online Access: | http://dx.doi.org/10.1155/2015/698738 |
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author | Josephine Chang Hui Lai Md. Rezaur Rahman Sinin Hamdan |
author_facet | Josephine Chang Hui Lai Md. Rezaur Rahman Sinin Hamdan |
author_sort | Josephine Chang Hui Lai |
collection | DOAJ |
description | Polylactic acid/fumed silica/clay (PLA/FS/clay) (1.28E) nanocomposites have been successfully prepared by solution-intercalation film-casting technique. The resultant nanocomposites were characterized by Fourier Transform Infrared Spectroscopy (FT-IR), Scanning Electron Microscopy (SEM), tensile test, thermogravimetric analysis (TGA), and moisture absorption test. The FT-IR spectrum indicated that PLA/FS/clay with 2 wt% had much broader peak compared to 5 wt%, 10 wt%, and 15 wt% nanocomposites. Incorporation of clay (1.28E) with 2 wt% showed the best compatibility with PLA/FS matrix. PLA/FS/clay (1.28E) nanocomposite with 2 wt% of clay loading had higher tensile strength and modulus compared to other nanocomposites. The thermal stability and activation energy of 2 wt% of PLA/FS/clay (1.28E) nanocomposite are the highest among all the nanocomposites. The moisture absorbed into PLA/FS/clay (1.28E) nanocomposite was significantly reduced with clay loading of 2 wt%. |
format | Article |
id | doaj-art-3ab25aaf13a74e3b9361c70075fb590c |
institution | Kabale University |
issn | 1687-9422 1687-9430 |
language | English |
publishDate | 2015-01-01 |
publisher | Wiley |
record_format | Article |
series | International Journal of Polymer Science |
spelling | doaj-art-3ab25aaf13a74e3b9361c70075fb590c2025-02-03T01:23:02ZengWileyInternational Journal of Polymer Science1687-94221687-94302015-01-01201510.1155/2015/698738698738Physical, Mechanical, and Thermal Analysis of Polylactic Acid/Fumed Silica/Clay (1.28E) NanocompositesJosephine Chang Hui Lai0Md. Rezaur Rahman1Sinin Hamdan2Department of Chemical Engineering and Energy Sustainability, Faculty of Engineering, Universiti Malaysia Sarawak (UNIMAS), 94300 Kota Samarahan, Sarawak, MalaysiaDepartment of Chemical Engineering and Energy Sustainability, Faculty of Engineering, Universiti Malaysia Sarawak (UNIMAS), 94300 Kota Samarahan, Sarawak, MalaysiaDepartment of Mechanical and Manufacturing Engineering, Faculty of Engineering, Universiti Malaysia Sarawak (UNIMAS), 94300 Kota Samarahan, Sarawak, MalaysiaPolylactic acid/fumed silica/clay (PLA/FS/clay) (1.28E) nanocomposites have been successfully prepared by solution-intercalation film-casting technique. The resultant nanocomposites were characterized by Fourier Transform Infrared Spectroscopy (FT-IR), Scanning Electron Microscopy (SEM), tensile test, thermogravimetric analysis (TGA), and moisture absorption test. The FT-IR spectrum indicated that PLA/FS/clay with 2 wt% had much broader peak compared to 5 wt%, 10 wt%, and 15 wt% nanocomposites. Incorporation of clay (1.28E) with 2 wt% showed the best compatibility with PLA/FS matrix. PLA/FS/clay (1.28E) nanocomposite with 2 wt% of clay loading had higher tensile strength and modulus compared to other nanocomposites. The thermal stability and activation energy of 2 wt% of PLA/FS/clay (1.28E) nanocomposite are the highest among all the nanocomposites. The moisture absorbed into PLA/FS/clay (1.28E) nanocomposite was significantly reduced with clay loading of 2 wt%.http://dx.doi.org/10.1155/2015/698738 |
spellingShingle | Josephine Chang Hui Lai Md. Rezaur Rahman Sinin Hamdan Physical, Mechanical, and Thermal Analysis of Polylactic Acid/Fumed Silica/Clay (1.28E) Nanocomposites International Journal of Polymer Science |
title | Physical, Mechanical, and Thermal Analysis of Polylactic Acid/Fumed Silica/Clay (1.28E) Nanocomposites |
title_full | Physical, Mechanical, and Thermal Analysis of Polylactic Acid/Fumed Silica/Clay (1.28E) Nanocomposites |
title_fullStr | Physical, Mechanical, and Thermal Analysis of Polylactic Acid/Fumed Silica/Clay (1.28E) Nanocomposites |
title_full_unstemmed | Physical, Mechanical, and Thermal Analysis of Polylactic Acid/Fumed Silica/Clay (1.28E) Nanocomposites |
title_short | Physical, Mechanical, and Thermal Analysis of Polylactic Acid/Fumed Silica/Clay (1.28E) Nanocomposites |
title_sort | physical mechanical and thermal analysis of polylactic acid fumed silica clay 1 28e nanocomposites |
url | http://dx.doi.org/10.1155/2015/698738 |
work_keys_str_mv | AT josephinechanghuilai physicalmechanicalandthermalanalysisofpolylacticacidfumedsilicaclay128enanocomposites AT mdrezaurrahman physicalmechanicalandthermalanalysisofpolylacticacidfumedsilicaclay128enanocomposites AT sininhamdan physicalmechanicalandthermalanalysisofpolylacticacidfumedsilicaclay128enanocomposites |