Elaboration of the Al-Al3Ni Alloy Eutectic by a Carbothermal Process

The present study develops an elaborate method of materials Al-Al3Ni by carbothermic reduction of nickel oxide from the decomposition of Ni(NO3)2.4H2O mixed with aluminum powder. This nitrate salt represents the source of nickel for an elaboration of these materials. The thermodynamic parameters ado...

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Main Authors: Imane Bahaj, Mohammed Kaddami, Mohamed Essahli
Format: Article
Language:English
Published: Wiley 2022-01-01
Series:The Scientific World Journal
Online Access:http://dx.doi.org/10.1155/2022/7764487
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author Imane Bahaj
Mohammed Kaddami
Mohamed Essahli
author_facet Imane Bahaj
Mohammed Kaddami
Mohamed Essahli
author_sort Imane Bahaj
collection DOAJ
description The present study develops an elaborate method of materials Al-Al3Ni by carbothermic reduction of nickel oxide from the decomposition of Ni(NO3)2.4H2O mixed with aluminum powder. This nitrate salt represents the source of nickel for an elaboration of these materials. The thermodynamic parameters adopted in the experimental study were defined based on the liquid-solid phase equilibrium diagram of the binary system Al-Ni and the Ellingham approach. Throughout this study, the metal Ni is elaborated by carbothermic reduction of nickel oxide resulting from nitrate salt decomposition at 900°C under a nitrogen atmosphere. The heat treatment at 900 °C of a mixture of nitrate salt with aluminum powder under an inert gas atmosphere leads to the formation of phases Al2O3, Al4C3, Al, and Ni. The annealing of these obtained phases during 1 h and under a nitrogen flow atmosphere at the temperature of 600°C allowed us to obtain the Al-Al3Ni alloy devoid of oxides. The characterization of these obtained solid phases was carried out by the XRD analysis, the SEM-EDS, the DTA, and the DSC.
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issn 1537-744X
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publishDate 2022-01-01
publisher Wiley
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spelling doaj-art-2ff53aacb4a24ec38dc59e69ad40bae42025-02-03T06:08:38ZengWileyThe Scientific World Journal1537-744X2022-01-01202210.1155/2022/7764487Elaboration of the Al-Al3Ni Alloy Eutectic by a Carbothermal ProcessImane Bahaj0Mohammed Kaddami1Mohamed Essahli2Hassan First University of SettatHassan First University of SettatHassan First University of SettatThe present study develops an elaborate method of materials Al-Al3Ni by carbothermic reduction of nickel oxide from the decomposition of Ni(NO3)2.4H2O mixed with aluminum powder. This nitrate salt represents the source of nickel for an elaboration of these materials. The thermodynamic parameters adopted in the experimental study were defined based on the liquid-solid phase equilibrium diagram of the binary system Al-Ni and the Ellingham approach. Throughout this study, the metal Ni is elaborated by carbothermic reduction of nickel oxide resulting from nitrate salt decomposition at 900°C under a nitrogen atmosphere. The heat treatment at 900 °C of a mixture of nitrate salt with aluminum powder under an inert gas atmosphere leads to the formation of phases Al2O3, Al4C3, Al, and Ni. The annealing of these obtained phases during 1 h and under a nitrogen flow atmosphere at the temperature of 600°C allowed us to obtain the Al-Al3Ni alloy devoid of oxides. The characterization of these obtained solid phases was carried out by the XRD analysis, the SEM-EDS, the DTA, and the DSC.http://dx.doi.org/10.1155/2022/7764487
spellingShingle Imane Bahaj
Mohammed Kaddami
Mohamed Essahli
Elaboration of the Al-Al3Ni Alloy Eutectic by a Carbothermal Process
The Scientific World Journal
title Elaboration of the Al-Al3Ni Alloy Eutectic by a Carbothermal Process
title_full Elaboration of the Al-Al3Ni Alloy Eutectic by a Carbothermal Process
title_fullStr Elaboration of the Al-Al3Ni Alloy Eutectic by a Carbothermal Process
title_full_unstemmed Elaboration of the Al-Al3Ni Alloy Eutectic by a Carbothermal Process
title_short Elaboration of the Al-Al3Ni Alloy Eutectic by a Carbothermal Process
title_sort elaboration of the al al3ni alloy eutectic by a carbothermal process
url http://dx.doi.org/10.1155/2022/7764487
work_keys_str_mv AT imanebahaj elaborationofthealal3nialloyeutecticbyacarbothermalprocess
AT mohammedkaddami elaborationofthealal3nialloyeutecticbyacarbothermalprocess
AT mohamedessahli elaborationofthealal3nialloyeutecticbyacarbothermalprocess