Microstructure characterization of porous microalloyed aluminium-silicate ceramics

Kaolinite and bentonite clay powders mixed with active additives, based on Mg(NO3)2 and Al(NO3)2, sintered at high temperatures produce very porous ceramics with microcrystalline and amorphous regions and highly developed metalized surfaces (mainly with magnesium surplus). Microstructure investi...

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Main Authors: Purenović Jelena, Mitić V.V., Paunović V., Purenović M.
Format: Article
Language:English
Published: University of Belgrade, Technical Faculty, Bor 2011-01-01
Series:Journal of Mining and Metallurgy. Section B: Metallurgy
Subjects:
Online Access:http://www.doiserbia.nb.rs/img/doi/1450-5339/2011/1450-53391100011P.pdf
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author Purenović Jelena
Mitić V.V.
Paunović V.
Purenović M.
author_facet Purenović Jelena
Mitić V.V.
Paunović V.
Purenović M.
author_sort Purenović Jelena
collection DOAJ
description Kaolinite and bentonite clay powders mixed with active additives, based on Mg(NO3)2 and Al(NO3)2, sintered at high temperatures produce very porous ceramics with microcrystalline and amorphous regions and highly developed metalized surfaces (mainly with magnesium surplus). Microstructure investigations have revealed non-uniform and highly porous structure with broad distribution of grain size, specifically shaped grains and high degree of agglomeration. The ceramics samples were characterized by scanning electron microscopy (SEM), energy dispersive spectrometer (EDS), X-ray diffraction analysis (XRD) and IR spectroscopy analysis, prior and after treatment in “synthetic water”, i.e. in aqueous solution of arsenic-salt. Grain size distribution for untreated and treated samples was done with software SemAfore 4. It has shown great variety in size distribution of grains from clay powders to sintered samples.
format Article
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institution Kabale University
issn 1450-5339
language English
publishDate 2011-01-01
publisher University of Belgrade, Technical Faculty, Bor
record_format Article
series Journal of Mining and Metallurgy. Section B: Metallurgy
spelling doaj-art-270008d5f12d4ab9b5aae91df8a3ea912025-02-02T20:39:31ZengUniversity of Belgrade, Technical Faculty, BorJournal of Mining and Metallurgy. Section B: Metallurgy1450-53392011-01-0147215716910.2298/JMMB110331011PMicrostructure characterization of porous microalloyed aluminium-silicate ceramicsPurenović JelenaMitić V.V.Paunović V.Purenović M.Kaolinite and bentonite clay powders mixed with active additives, based on Mg(NO3)2 and Al(NO3)2, sintered at high temperatures produce very porous ceramics with microcrystalline and amorphous regions and highly developed metalized surfaces (mainly with magnesium surplus). Microstructure investigations have revealed non-uniform and highly porous structure with broad distribution of grain size, specifically shaped grains and high degree of agglomeration. The ceramics samples were characterized by scanning electron microscopy (SEM), energy dispersive spectrometer (EDS), X-ray diffraction analysis (XRD) and IR spectroscopy analysis, prior and after treatment in “synthetic water”, i.e. in aqueous solution of arsenic-salt. Grain size distribution for untreated and treated samples was done with software SemAfore 4. It has shown great variety in size distribution of grains from clay powders to sintered samples.http://www.doiserbia.nb.rs/img/doi/1450-5339/2011/1450-53391100011P.pdfaluminium-silicate ceramicsactive additivesmicrostructuremicro alloyinggrain size distribution
spellingShingle Purenović Jelena
Mitić V.V.
Paunović V.
Purenović M.
Microstructure characterization of porous microalloyed aluminium-silicate ceramics
Journal of Mining and Metallurgy. Section B: Metallurgy
aluminium-silicate ceramics
active additives
microstructure
micro alloying
grain size distribution
title Microstructure characterization of porous microalloyed aluminium-silicate ceramics
title_full Microstructure characterization of porous microalloyed aluminium-silicate ceramics
title_fullStr Microstructure characterization of porous microalloyed aluminium-silicate ceramics
title_full_unstemmed Microstructure characterization of porous microalloyed aluminium-silicate ceramics
title_short Microstructure characterization of porous microalloyed aluminium-silicate ceramics
title_sort microstructure characterization of porous microalloyed aluminium silicate ceramics
topic aluminium-silicate ceramics
active additives
microstructure
micro alloying
grain size distribution
url http://www.doiserbia.nb.rs/img/doi/1450-5339/2011/1450-53391100011P.pdf
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AT miticvv microstructurecharacterizationofporousmicroalloyedaluminiumsilicateceramics
AT paunovicv microstructurecharacterizationofporousmicroalloyedaluminiumsilicateceramics
AT purenovicm microstructurecharacterizationofporousmicroalloyedaluminiumsilicateceramics