Rod-Shaped Magnetite Nano/Microparticles Synthesis at Ambient Temperature
Here, we reported room temperature synthesis of Fe3O4 rod-shaped nano/microparticles by chemical reduction method from FeCl3 precursor and NaBH4 as the reducing agent in the presence of the pyrrole as a capping agent. The magnetic Fe3O4 particles were characterized by several methods, such as SEM, X...
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| Format: | Article |
| Language: | English |
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Wiley
2013-01-01
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| Series: | Journal of Chemistry |
| Online Access: | http://dx.doi.org/10.1155/2013/537976 |
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| author | Balaprasad Ankamwar Ashwini Thorat |
| author_facet | Balaprasad Ankamwar Ashwini Thorat |
| author_sort | Balaprasad Ankamwar |
| collection | DOAJ |
| description | Here, we reported room temperature synthesis of Fe3O4 rod-shaped nano/microparticles by chemical reduction method from FeCl3 precursor and NaBH4 as the reducing agent in the presence of the pyrrole as a capping agent. The magnetic Fe3O4 particles were characterized by several methods, such as SEM, XRD, FTIR, and TGA. The average aspect ratio of Fe3O4 rod-shaped particles was ~2.8. These particles were redispersed in deionised water to form a colloidal solution and showed magnetic properties. This economical synthesis route is scalable, and Fe3O4 particles can be exploited for various applications such as MRI contrast enhancement, biodiseperations, Ni-Fe batteries, and as a catalyst. |
| format | Article |
| id | doaj-art-1f0edc2bc8cd453589e8113cf9334dec |
| institution | Kabale University |
| issn | 2090-9063 2090-9071 |
| language | English |
| publishDate | 2013-01-01 |
| publisher | Wiley |
| record_format | Article |
| series | Journal of Chemistry |
| spelling | doaj-art-1f0edc2bc8cd453589e8113cf9334dec2025-02-03T01:27:09ZengWileyJournal of Chemistry2090-90632090-90712013-01-01201310.1155/2013/537976537976Rod-Shaped Magnetite Nano/Microparticles Synthesis at Ambient TemperatureBalaprasad Ankamwar0Ashwini Thorat1Department of Chemistry, University of Pune, Ganeshkhind, Pune 411007, IndiaDepartment of Chemistry, University of Pune, Ganeshkhind, Pune 411007, IndiaHere, we reported room temperature synthesis of Fe3O4 rod-shaped nano/microparticles by chemical reduction method from FeCl3 precursor and NaBH4 as the reducing agent in the presence of the pyrrole as a capping agent. The magnetic Fe3O4 particles were characterized by several methods, such as SEM, XRD, FTIR, and TGA. The average aspect ratio of Fe3O4 rod-shaped particles was ~2.8. These particles were redispersed in deionised water to form a colloidal solution and showed magnetic properties. This economical synthesis route is scalable, and Fe3O4 particles can be exploited for various applications such as MRI contrast enhancement, biodiseperations, Ni-Fe batteries, and as a catalyst.http://dx.doi.org/10.1155/2013/537976 |
| spellingShingle | Balaprasad Ankamwar Ashwini Thorat Rod-Shaped Magnetite Nano/Microparticles Synthesis at Ambient Temperature Journal of Chemistry |
| title | Rod-Shaped Magnetite Nano/Microparticles Synthesis at Ambient Temperature |
| title_full | Rod-Shaped Magnetite Nano/Microparticles Synthesis at Ambient Temperature |
| title_fullStr | Rod-Shaped Magnetite Nano/Microparticles Synthesis at Ambient Temperature |
| title_full_unstemmed | Rod-Shaped Magnetite Nano/Microparticles Synthesis at Ambient Temperature |
| title_short | Rod-Shaped Magnetite Nano/Microparticles Synthesis at Ambient Temperature |
| title_sort | rod shaped magnetite nano microparticles synthesis at ambient temperature |
| url | http://dx.doi.org/10.1155/2013/537976 |
| work_keys_str_mv | AT balaprasadankamwar rodshapedmagnetitenanomicroparticlessynthesisatambienttemperature AT ashwinithorat rodshapedmagnetitenanomicroparticlessynthesisatambienttemperature |