The Preparation and Performances of Self-Dispersed Nanomicron Emulsified Wax Solid Lubricant Ewax for Drilling Fluids

An oil-in-water nanomicron wax emulsion with oil phase content 45 wt% was prepared by using the emulsifying method of surfactant-in-oil. The optimum prepared condition is 85°C, 20 min, and 5 wt% complex emulsifiers. Then the abovementioned nanomicron emulsifying wax was immersed into a special water...

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Main Authors: Feng-shan Zhou, Ting-ting Wang, Zheng-qiang Xiong, Wen-yue Guo, Xi Xiang, Huan-na Wang, Xia-lei Zhu, Fang Liu, Bao-lin Cui
Format: Article
Language:English
Published: Wiley 2014-01-01
Series:Journal of Spectroscopy
Online Access:http://dx.doi.org/10.1155/2014/530284
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author Feng-shan Zhou
Ting-ting Wang
Zheng-qiang Xiong
Wen-yue Guo
Xi Xiang
Huan-na Wang
Xia-lei Zhu
Fang Liu
Bao-lin Cui
author_facet Feng-shan Zhou
Ting-ting Wang
Zheng-qiang Xiong
Wen-yue Guo
Xi Xiang
Huan-na Wang
Xia-lei Zhu
Fang Liu
Bao-lin Cui
author_sort Feng-shan Zhou
collection DOAJ
description An oil-in-water nanomicron wax emulsion with oil phase content 45 wt% was prepared by using the emulsifying method of surfactant-in-oil. The optimum prepared condition is 85°C, 20 min, and 5 wt% complex emulsifiers. Then the abovementioned nanomicron emulsifying wax was immersed into a special water-soluble polymer in a certain percentage by the semidry technology. At last, a solidified self-dispersed nanomicron emulsified wax named as Ewax, a kind of solid lubricant for water based drilling fluid, was obtained after dried in the special soluble polymer containing emulsifying wax in low temperature. It is shown that the adhesion coefficient reduced rate (ΔKf) is 73.5% and the extreme pressure (E-P) friction coefficient reduced rate (Δf) is 77.6% when the produced Ewax sample was added to fresh water based drilling fluid at dosage 1.0 wt%. In comparison with other normal similar liquid products, Ewax not only has better performances of lubrication, filtration loss control property, heat resistance, and tolerance to salt and is environmentally friendly, but also can solve the problems of freezing in the winter and poor storage stability of liquid wax emulsion in oilfield applications.
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publishDate 2014-01-01
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spelling doaj-art-1e38c6abdc7b4e5b84d8c4189e53a97a2025-02-03T01:11:48ZengWileyJournal of Spectroscopy2314-49202314-49392014-01-01201410.1155/2014/530284530284The Preparation and Performances of Self-Dispersed Nanomicron Emulsified Wax Solid Lubricant Ewax for Drilling FluidsFeng-shan Zhou0Ting-ting Wang1Zheng-qiang Xiong2Wen-yue Guo3Xi Xiang4Huan-na Wang5Xia-lei Zhu6Fang Liu7Bao-lin Cui8School of Materials Science and Technology, China University of Geosciences, Beijing 100083, ChinaSchool of Materials Science and Technology, China University of Geosciences, Beijing 100083, ChinaBeijing Institute of Exploration Engineering, Beijing 100083, ChinaSchool of Materials Science and Technology, China University of Geosciences, Beijing 100083, ChinaSchool of Materials Science and Technology, China University of Geosciences, Beijing 100083, ChinaSchool of Materials Science and Technology, China University of Geosciences, Beijing 100083, ChinaSchool of Materials Science and Technology, China University of Geosciences, Beijing 100083, ChinaSchool of Materials Science and Technology, China University of Geosciences, Beijing 100083, ChinaSchool of Materials Science and Technology, China University of Geosciences, Beijing 100083, ChinaAn oil-in-water nanomicron wax emulsion with oil phase content 45 wt% was prepared by using the emulsifying method of surfactant-in-oil. The optimum prepared condition is 85°C, 20 min, and 5 wt% complex emulsifiers. Then the abovementioned nanomicron emulsifying wax was immersed into a special water-soluble polymer in a certain percentage by the semidry technology. At last, a solidified self-dispersed nanomicron emulsified wax named as Ewax, a kind of solid lubricant for water based drilling fluid, was obtained after dried in the special soluble polymer containing emulsifying wax in low temperature. It is shown that the adhesion coefficient reduced rate (ΔKf) is 73.5% and the extreme pressure (E-P) friction coefficient reduced rate (Δf) is 77.6% when the produced Ewax sample was added to fresh water based drilling fluid at dosage 1.0 wt%. In comparison with other normal similar liquid products, Ewax not only has better performances of lubrication, filtration loss control property, heat resistance, and tolerance to salt and is environmentally friendly, but also can solve the problems of freezing in the winter and poor storage stability of liquid wax emulsion in oilfield applications.http://dx.doi.org/10.1155/2014/530284
spellingShingle Feng-shan Zhou
Ting-ting Wang
Zheng-qiang Xiong
Wen-yue Guo
Xi Xiang
Huan-na Wang
Xia-lei Zhu
Fang Liu
Bao-lin Cui
The Preparation and Performances of Self-Dispersed Nanomicron Emulsified Wax Solid Lubricant Ewax for Drilling Fluids
Journal of Spectroscopy
title The Preparation and Performances of Self-Dispersed Nanomicron Emulsified Wax Solid Lubricant Ewax for Drilling Fluids
title_full The Preparation and Performances of Self-Dispersed Nanomicron Emulsified Wax Solid Lubricant Ewax for Drilling Fluids
title_fullStr The Preparation and Performances of Self-Dispersed Nanomicron Emulsified Wax Solid Lubricant Ewax for Drilling Fluids
title_full_unstemmed The Preparation and Performances of Self-Dispersed Nanomicron Emulsified Wax Solid Lubricant Ewax for Drilling Fluids
title_short The Preparation and Performances of Self-Dispersed Nanomicron Emulsified Wax Solid Lubricant Ewax for Drilling Fluids
title_sort preparation and performances of self dispersed nanomicron emulsified wax solid lubricant ewax for drilling fluids
url http://dx.doi.org/10.1155/2014/530284
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