Microstructure evolution and recrystallization behavior of two nickel-based single crystal superalloys

This study focuses on the single crystal (SC) superalloys CMSX-4 and DD5, designing and fabricating a SC test plate casting with five distinct stages. Castings with the same crystal orientation are selected to investigate their recrystallization (RX) behavior after solution heat treatment at 1300 ℃...

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Main Authors: XU Fuze, LIN Yongcheng, MA Dexin, HE Daoguang, ZHAO Yunxing, LI Lyu, CHENG Bowen, DENG Yangpi
Format: Article
Language:zho
Published: Journal of Materials Engineering 2025-01-01
Series:Cailiao gongcheng
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Online Access:https://jme.biam.ac.cn/CN/10.11868/j.issn.1001-4381.2024.000381
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author XU Fuze
LIN Yongcheng
MA Dexin
HE Daoguang
ZHAO Yunxing
LI Lyu
CHENG Bowen
DENG Yangpi
author_facet XU Fuze
LIN Yongcheng
MA Dexin
HE Daoguang
ZHAO Yunxing
LI Lyu
CHENG Bowen
DENG Yangpi
author_sort XU Fuze
collection DOAJ
description This study focuses on the single crystal (SC) superalloys CMSX-4 and DD5, designing and fabricating a SC test plate casting with five distinct stages. Castings with the same crystal orientation are selected to investigate their recrystallization (RX) behavior after solution heat treatment at 1300 ℃ for 2 h and 1310 ℃ for 4 h. The results indicate that CMSX-4 exhibits a stronger tendency for RX compared to DD5. Following a solution heat treatment at 1300 ℃, the CMSX-4 SC test plate displayed RX at the lower corners of 2-5 stage platforms, with the extent of RX expanding as the solution heat treatment temperature rose. Conversely, no RX was detected in the DD5 SC test plate post-treatment at 1300 ℃. Elevating the solution temperature to 1310 ℃ results in only a minor area of RX on the outer platform of the fourth stage in the DD5 SC test plate. The micro-shrinkage porosity and eutectic content of the as-cast and solution heat treated CMSX-4 alloy are both higher than those of the DD5 alloy. The higher content of eutectic and micro-shrinkage porosity provides more nucleation sites and quantities for RX in the CMSX-4 alloy, while the solution heat treatment temperatures above the γ' phase dissolution temperature weakens the pinning effect of coarse γ' phase on RX growth, and high melting point carbides and residual eutectic become important factors hindering RX growth. In addition, the high content of Co element reduces the stacking fault energy of the CMSX-4 alloy, making it with a high recrystallization tendency.
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institution Kabale University
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publishDate 2025-01-01
publisher Journal of Materials Engineering
record_format Article
series Cailiao gongcheng
spelling doaj-art-16d38d16ce8544d4a86134f67410dcc12025-01-21T09:44:41ZzhoJournal of Materials EngineeringCailiao gongcheng1001-43812025-01-0153111012010.11868/j.issn.1001-4381.2024.0003811001-4381(2025)01-0110-11Microstructure evolution and recrystallization behavior of two nickel-based single crystal superalloysXU Fuze0LIN Yongcheng1MA Dexin2HE Daoguang3ZHAO Yunxing4LI Lyu5CHENG Bowen6DENG Yangpi7School of Mechanical and Electrical Engineering,Central South University,Changsha 410083,ChinaSchool of Mechanical and Electrical Engineering,Central South University,Changsha 410083,ChinaShenzhen Wedge Central South Research Institute Co.,Ltd.,Shenzhen 518045,Guangdong, ChinaSchool of Mechanical and Electrical Engineering,Central South University,Changsha 410083,ChinaShenzhen Wedge Central South Research Institute Co.,Ltd.,Shenzhen 518045,Guangdong, ChinaShenzhen Wedge Central South Research Institute Co.,Ltd.,Shenzhen 518045,Guangdong, ChinaShenzhen Wedge Central South Research Institute Co.,Ltd.,Shenzhen 518045,Guangdong, ChinaShenzhen Wedge Central South Research Institute Co.,Ltd.,Shenzhen 518045,Guangdong, ChinaThis study focuses on the single crystal (SC) superalloys CMSX-4 and DD5, designing and fabricating a SC test plate casting with five distinct stages. Castings with the same crystal orientation are selected to investigate their recrystallization (RX) behavior after solution heat treatment at 1300 ℃ for 2 h and 1310 ℃ for 4 h. The results indicate that CMSX-4 exhibits a stronger tendency for RX compared to DD5. Following a solution heat treatment at 1300 ℃, the CMSX-4 SC test plate displayed RX at the lower corners of 2-5 stage platforms, with the extent of RX expanding as the solution heat treatment temperature rose. Conversely, no RX was detected in the DD5 SC test plate post-treatment at 1300 ℃. Elevating the solution temperature to 1310 ℃ results in only a minor area of RX on the outer platform of the fourth stage in the DD5 SC test plate. The micro-shrinkage porosity and eutectic content of the as-cast and solution heat treated CMSX-4 alloy are both higher than those of the DD5 alloy. The higher content of eutectic and micro-shrinkage porosity provides more nucleation sites and quantities for RX in the CMSX-4 alloy, while the solution heat treatment temperatures above the γ' phase dissolution temperature weakens the pinning effect of coarse γ' phase on RX growth, and high melting point carbides and residual eutectic become important factors hindering RX growth. In addition, the high content of Co element reduces the stacking fault energy of the CMSX-4 alloy, making it with a high recrystallization tendency.https://jme.biam.ac.cn/CN/10.11868/j.issn.1001-4381.2024.000381single crystal superalloycmsx-4dd5recrystallizationplastic strain
spellingShingle XU Fuze
LIN Yongcheng
MA Dexin
HE Daoguang
ZHAO Yunxing
LI Lyu
CHENG Bowen
DENG Yangpi
Microstructure evolution and recrystallization behavior of two nickel-based single crystal superalloys
Cailiao gongcheng
single crystal superalloy
cmsx-4
dd5
recrystallization
plastic strain
title Microstructure evolution and recrystallization behavior of two nickel-based single crystal superalloys
title_full Microstructure evolution and recrystallization behavior of two nickel-based single crystal superalloys
title_fullStr Microstructure evolution and recrystallization behavior of two nickel-based single crystal superalloys
title_full_unstemmed Microstructure evolution and recrystallization behavior of two nickel-based single crystal superalloys
title_short Microstructure evolution and recrystallization behavior of two nickel-based single crystal superalloys
title_sort microstructure evolution and recrystallization behavior of two nickel based single crystal superalloys
topic single crystal superalloy
cmsx-4
dd5
recrystallization
plastic strain
url https://jme.biam.ac.cn/CN/10.11868/j.issn.1001-4381.2024.000381
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AT linyongcheng microstructureevolutionandrecrystallizationbehavioroftwonickelbasedsinglecrystalsuperalloys
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AT hedaoguang microstructureevolutionandrecrystallizationbehavioroftwonickelbasedsinglecrystalsuperalloys
AT zhaoyunxing microstructureevolutionandrecrystallizationbehavioroftwonickelbasedsinglecrystalsuperalloys
AT lilyu microstructureevolutionandrecrystallizationbehavioroftwonickelbasedsinglecrystalsuperalloys
AT chengbowen microstructureevolutionandrecrystallizationbehavioroftwonickelbasedsinglecrystalsuperalloys
AT dengyangpi microstructureevolutionandrecrystallizationbehavioroftwonickelbasedsinglecrystalsuperalloys