Innovative dispersion techniques of graphene nanoplatelets (GNPs) through mechanical stirring and ultrasonication: Impact on morphological, mechanical, and thermal properties of epoxy nanocomposites
Graphene nanoplatelets (GNPs) have attracted tremendous interest due to their unique properties and bonding capabilities. This study focuses on the effect of GNP dispersion on the mechanical, thermal, and morphological behavior of GNP/epoxy nanocomposites. This study aims to understand how the dispe...
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KeAi Communications Co., Ltd.
2025-01-01
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| Series: | Defence Technology |
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| Online Access: | http://www.sciencedirect.com/science/article/pii/S2214914724001041 |
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| author | Vasi Uddin Siddiqui S.M. Sapuan Mohd Roshdi Hassan |
| author_facet | Vasi Uddin Siddiqui S.M. Sapuan Mohd Roshdi Hassan |
| author_sort | Vasi Uddin Siddiqui |
| collection | DOAJ |
| description | Graphene nanoplatelets (GNPs) have attracted tremendous interest due to their unique properties and bonding capabilities. This study focuses on the effect of GNP dispersion on the mechanical, thermal, and morphological behavior of GNP/epoxy nanocomposites. This study aims to understand how the dispersion of GNPs affects the properties of epoxy nanocomposite and to identify the best dispersion approach for improving mechanical performance. A solvent mixing technique that includes mechanical stirring and ultrasonication was used for producing the nanocomposites. Fourier transform infrared spectroscopy was used to investigate the interaction between GNPs and the epoxy matrix. The measurements of density and moisture content were used to confirm that GNPs were successfully incorporated into the nanocomposite. The findings showed that GNPs are successfully dispersed in the epoxy matrix by combining mechanical stirring and ultrasonication in a single step, producing well-dispersed nanocomposites with improved mechanical properties. Particularly, the nanocomposites at a low GNP loading of 0.1 wt%, demonstrate superior mechanical strength, as shown by increased tensile properties, including improved Young's modulus (1.86 GPa), strength (57.31 MPa), and elongation at break (4.98). The nanocomposite with 0.25 wt% GNP loading performs better, according to the viscoelastic analysis and flexural properties (113.18 MPa). Except for the nanocomposite with a 0.5 wt% GNP loading, which has a higher thermal breakdown temperature, the thermal characteristics do not significantly alter. The effective dispersion of GNPs in the epoxy matrix and low agglomeration is confirmed by the morphological characterization. The findings help with filler selection and identifying the best dispersion approach, which improves mechanical performance. The effective integration of GNPs and their interaction with the epoxy matrix provides the doorway for additional investigation and the development of sophisticated nanocomposites. In fields like aerospace, automotive, and electronics where higher mechanical performance and functionality are required, GNPs' improved mechanical properties and successful dispersion present exciting potential. |
| format | Article |
| id | doaj-art-0e638731b38348f4b0d37e08ca4038c8 |
| institution | Kabale University |
| issn | 2214-9147 |
| language | English |
| publishDate | 2025-01-01 |
| publisher | KeAi Communications Co., Ltd. |
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| series | Defence Technology |
| spelling | doaj-art-0e638731b38348f4b0d37e08ca4038c82025-01-23T05:26:46ZengKeAi Communications Co., Ltd.Defence Technology2214-91472025-01-01431325Innovative dispersion techniques of graphene nanoplatelets (GNPs) through mechanical stirring and ultrasonication: Impact on morphological, mechanical, and thermal properties of epoxy nanocompositesVasi Uddin Siddiqui0S.M. Sapuan1Mohd Roshdi Hassan2Advanced Engineering Materials and Composites Research Centre (AEMC), Department of Mechanical and Manufacturing Engineering, Universiti Putra Malaysia, UPM Serdang, Selangor 43400, MalaysiaAdvanced Engineering Materials and Composites Research Centre (AEMC), Department of Mechanical and Manufacturing Engineering, Universiti Putra Malaysia, UPM Serdang, Selangor 43400, Malaysia; Corresponding author.Department of Mechanical and Manufacturing Engineering, Universiti Putra Malaysia, UPM Serdang, Selangor 43400, MalaysiaGraphene nanoplatelets (GNPs) have attracted tremendous interest due to their unique properties and bonding capabilities. This study focuses on the effect of GNP dispersion on the mechanical, thermal, and morphological behavior of GNP/epoxy nanocomposites. This study aims to understand how the dispersion of GNPs affects the properties of epoxy nanocomposite and to identify the best dispersion approach for improving mechanical performance. A solvent mixing technique that includes mechanical stirring and ultrasonication was used for producing the nanocomposites. Fourier transform infrared spectroscopy was used to investigate the interaction between GNPs and the epoxy matrix. The measurements of density and moisture content were used to confirm that GNPs were successfully incorporated into the nanocomposite. The findings showed that GNPs are successfully dispersed in the epoxy matrix by combining mechanical stirring and ultrasonication in a single step, producing well-dispersed nanocomposites with improved mechanical properties. Particularly, the nanocomposites at a low GNP loading of 0.1 wt%, demonstrate superior mechanical strength, as shown by increased tensile properties, including improved Young's modulus (1.86 GPa), strength (57.31 MPa), and elongation at break (4.98). The nanocomposite with 0.25 wt% GNP loading performs better, according to the viscoelastic analysis and flexural properties (113.18 MPa). Except for the nanocomposite with a 0.5 wt% GNP loading, which has a higher thermal breakdown temperature, the thermal characteristics do not significantly alter. The effective dispersion of GNPs in the epoxy matrix and low agglomeration is confirmed by the morphological characterization. The findings help with filler selection and identifying the best dispersion approach, which improves mechanical performance. The effective integration of GNPs and their interaction with the epoxy matrix provides the doorway for additional investigation and the development of sophisticated nanocomposites. In fields like aerospace, automotive, and electronics where higher mechanical performance and functionality are required, GNPs' improved mechanical properties and successful dispersion present exciting potential.http://www.sciencedirect.com/science/article/pii/S2214914724001041Graphene nanoplateletsEpoxyNanocompositesMechanical propertiesThermal propertiesMechanical stirrer |
| spellingShingle | Vasi Uddin Siddiqui S.M. Sapuan Mohd Roshdi Hassan Innovative dispersion techniques of graphene nanoplatelets (GNPs) through mechanical stirring and ultrasonication: Impact on morphological, mechanical, and thermal properties of epoxy nanocomposites Defence Technology Graphene nanoplatelets Epoxy Nanocomposites Mechanical properties Thermal properties Mechanical stirrer |
| title | Innovative dispersion techniques of graphene nanoplatelets (GNPs) through mechanical stirring and ultrasonication: Impact on morphological, mechanical, and thermal properties of epoxy nanocomposites |
| title_full | Innovative dispersion techniques of graphene nanoplatelets (GNPs) through mechanical stirring and ultrasonication: Impact on morphological, mechanical, and thermal properties of epoxy nanocomposites |
| title_fullStr | Innovative dispersion techniques of graphene nanoplatelets (GNPs) through mechanical stirring and ultrasonication: Impact on morphological, mechanical, and thermal properties of epoxy nanocomposites |
| title_full_unstemmed | Innovative dispersion techniques of graphene nanoplatelets (GNPs) through mechanical stirring and ultrasonication: Impact on morphological, mechanical, and thermal properties of epoxy nanocomposites |
| title_short | Innovative dispersion techniques of graphene nanoplatelets (GNPs) through mechanical stirring and ultrasonication: Impact on morphological, mechanical, and thermal properties of epoxy nanocomposites |
| title_sort | innovative dispersion techniques of graphene nanoplatelets gnps through mechanical stirring and ultrasonication impact on morphological mechanical and thermal properties of epoxy nanocomposites |
| topic | Graphene nanoplatelets Epoxy Nanocomposites Mechanical properties Thermal properties Mechanical stirrer |
| url | http://www.sciencedirect.com/science/article/pii/S2214914724001041 |
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