Synthesis and Optimization of MWCNTs on Co-Ni/MgO by Thermal CVD
Multiwalled carbon nanotubes (MWCNTs) were prepared by the thermal chemical vapor deposition (CVD) technique. Monometallic and bimetallic Co and Ni combinations were used as a catalyst on MgO support. The mixer of H2/C2H2 was used as a carbon source. The prepared CNTs were found to possess different...
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Wiley
2008-01-01
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Series: | Advances in Condensed Matter Physics |
Online Access: | http://dx.doi.org/10.1155/2008/971457 |
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author | H. Ryu B. K. Singh K. S. Bartwal |
author_facet | H. Ryu B. K. Singh K. S. Bartwal |
author_sort | H. Ryu |
collection | DOAJ |
description | Multiwalled carbon nanotubes (MWCNTs) were prepared by the thermal chemical vapor deposition (CVD) technique. Monometallic and bimetallic Co and Ni combinations were used as a catalyst on MgO support. The mixer of H2/C2H2 was used as a carbon source. The prepared CNTs were found to possess different shapes, morphologies, and sizes. Maximum yield was found for 50% Co (MgO: 50% and Ni: 0%) catalyst at 600°C. Scanning electron microscopy (SEM) and high-resolution transmission electron microscopy (HRTEM) techniques were used for structural analysis. Raman spectra were taken to investigate the quality and crystalline perfection of the prepared CNTs. The ratio of D- and G-bands (ID/IG) was measured from these spectra. |
format | Article |
id | doaj-art-0e2fc9d526b84bc58bf305e3ae47ebb2 |
institution | Kabale University |
issn | 1687-8108 1687-8124 |
language | English |
publishDate | 2008-01-01 |
publisher | Wiley |
record_format | Article |
series | Advances in Condensed Matter Physics |
spelling | doaj-art-0e2fc9d526b84bc58bf305e3ae47ebb22025-02-03T07:26:12ZengWileyAdvances in Condensed Matter Physics1687-81081687-81242008-01-01200810.1155/2008/971457971457Synthesis and Optimization of MWCNTs on Co-Ni/MgO by Thermal CVDH. Ryu0B. K. Singh1K. S. Bartwal2Energy Materials Research Centre, Korea Research Institute of Chemical Technology, P.O. Box 107, Yuseong, Daejeon 305-600, South KoreaEnergy Materials Research Centre, Korea Research Institute of Chemical Technology, P.O. Box 107, Yuseong, Daejeon 305-600, South KoreaEnergy Materials Research Centre, Korea Research Institute of Chemical Technology, P.O. Box 107, Yuseong, Daejeon 305-600, South KoreaMultiwalled carbon nanotubes (MWCNTs) were prepared by the thermal chemical vapor deposition (CVD) technique. Monometallic and bimetallic Co and Ni combinations were used as a catalyst on MgO support. The mixer of H2/C2H2 was used as a carbon source. The prepared CNTs were found to possess different shapes, morphologies, and sizes. Maximum yield was found for 50% Co (MgO: 50% and Ni: 0%) catalyst at 600°C. Scanning electron microscopy (SEM) and high-resolution transmission electron microscopy (HRTEM) techniques were used for structural analysis. Raman spectra were taken to investigate the quality and crystalline perfection of the prepared CNTs. The ratio of D- and G-bands (ID/IG) was measured from these spectra.http://dx.doi.org/10.1155/2008/971457 |
spellingShingle | H. Ryu B. K. Singh K. S. Bartwal Synthesis and Optimization of MWCNTs on Co-Ni/MgO by Thermal CVD Advances in Condensed Matter Physics |
title | Synthesis and Optimization of MWCNTs on Co-Ni/MgO by Thermal CVD |
title_full | Synthesis and Optimization of MWCNTs on Co-Ni/MgO by Thermal CVD |
title_fullStr | Synthesis and Optimization of MWCNTs on Co-Ni/MgO by Thermal CVD |
title_full_unstemmed | Synthesis and Optimization of MWCNTs on Co-Ni/MgO by Thermal CVD |
title_short | Synthesis and Optimization of MWCNTs on Co-Ni/MgO by Thermal CVD |
title_sort | synthesis and optimization of mwcnts on co ni mgo by thermal cvd |
url | http://dx.doi.org/10.1155/2008/971457 |
work_keys_str_mv | AT hryu synthesisandoptimizationofmwcntsonconimgobythermalcvd AT bksingh synthesisandoptimizationofmwcntsonconimgobythermalcvd AT ksbartwal synthesisandoptimizationofmwcntsonconimgobythermalcvd |