Synthesis and Optimization of MWCNTs on Co-Ni/MgO by Thermal CVD

Multiwalled carbon nanotubes (MWCNTs) were prepared by the thermal chemical vapor deposition (CVD) technique. Monometallic and bimetallic Co and Ni combinations were used as a catalyst on MgO support. The mixer of H2/C2H2 was used as a carbon source. The prepared CNTs were found to possess different...

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Main Authors: H. Ryu, B. K. Singh, K. S. Bartwal
Format: Article
Language:English
Published: Wiley 2008-01-01
Series:Advances in Condensed Matter Physics
Online Access:http://dx.doi.org/10.1155/2008/971457
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author H. Ryu
B. K. Singh
K. S. Bartwal
author_facet H. Ryu
B. K. Singh
K. S. Bartwal
author_sort H. Ryu
collection DOAJ
description Multiwalled carbon nanotubes (MWCNTs) were prepared by the thermal chemical vapor deposition (CVD) technique. Monometallic and bimetallic Co and Ni combinations were used as a catalyst on MgO support. The mixer of H2/C2H2 was used as a carbon source. The prepared CNTs were found to possess different shapes, morphologies, and sizes. Maximum yield was found for 50% Co (MgO: 50% and Ni: 0%) catalyst at 600°C. Scanning electron microscopy (SEM) and high-resolution transmission electron microscopy (HRTEM) techniques were used for structural analysis. Raman spectra were taken to investigate the quality and crystalline perfection of the prepared CNTs. The ratio of D- and G-bands (ID/IG) was measured from these spectra.
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series Advances in Condensed Matter Physics
spelling doaj-art-0e2fc9d526b84bc58bf305e3ae47ebb22025-02-03T07:26:12ZengWileyAdvances in Condensed Matter Physics1687-81081687-81242008-01-01200810.1155/2008/971457971457Synthesis and Optimization of MWCNTs on Co-Ni/MgO by Thermal CVDH. Ryu0B. K. Singh1K. S. Bartwal2Energy Materials Research Centre, Korea Research Institute of Chemical Technology, P.O. Box 107, Yuseong, Daejeon 305-600, South KoreaEnergy Materials Research Centre, Korea Research Institute of Chemical Technology, P.O. Box 107, Yuseong, Daejeon 305-600, South KoreaEnergy Materials Research Centre, Korea Research Institute of Chemical Technology, P.O. Box 107, Yuseong, Daejeon 305-600, South KoreaMultiwalled carbon nanotubes (MWCNTs) were prepared by the thermal chemical vapor deposition (CVD) technique. Monometallic and bimetallic Co and Ni combinations were used as a catalyst on MgO support. The mixer of H2/C2H2 was used as a carbon source. The prepared CNTs were found to possess different shapes, morphologies, and sizes. Maximum yield was found for 50% Co (MgO: 50% and Ni: 0%) catalyst at 600°C. Scanning electron microscopy (SEM) and high-resolution transmission electron microscopy (HRTEM) techniques were used for structural analysis. Raman spectra were taken to investigate the quality and crystalline perfection of the prepared CNTs. The ratio of D- and G-bands (ID/IG) was measured from these spectra.http://dx.doi.org/10.1155/2008/971457
spellingShingle H. Ryu
B. K. Singh
K. S. Bartwal
Synthesis and Optimization of MWCNTs on Co-Ni/MgO by Thermal CVD
Advances in Condensed Matter Physics
title Synthesis and Optimization of MWCNTs on Co-Ni/MgO by Thermal CVD
title_full Synthesis and Optimization of MWCNTs on Co-Ni/MgO by Thermal CVD
title_fullStr Synthesis and Optimization of MWCNTs on Co-Ni/MgO by Thermal CVD
title_full_unstemmed Synthesis and Optimization of MWCNTs on Co-Ni/MgO by Thermal CVD
title_short Synthesis and Optimization of MWCNTs on Co-Ni/MgO by Thermal CVD
title_sort synthesis and optimization of mwcnts on co ni mgo by thermal cvd
url http://dx.doi.org/10.1155/2008/971457
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