Microstructural, Mechanical, and Tribological Properties of Selective Laser Melted Inconel 718 Alloy: The Influences of Heat Treatment

The present study investigates the microstructural, mechanical, and tribological properties of Inconel 718 alloy produced by selective laser melting (SLM) in relation to heat treatment. The SLM-processed samples received a two-step heat treatment: solutionizing at 1065 °C for 1 h, followed by double...

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Main Authors: Ümit Gencay Başcı, Egemen Avcu, Mertcan Kıraç, Ahmet Sever, İdris Gökalp, Hasan İsmail Yavuz, Serkan Oktay, Eray Abakay, Yasemin Yıldıran Avcu, Rıdvan Yamanoğlu
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Language:English
Published: MDPI AG 2024-12-01
Series:Crystals
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Online Access:https://www.mdpi.com/2073-4352/15/1/18
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author Ümit Gencay Başcı
Egemen Avcu
Mertcan Kıraç
Ahmet Sever
İdris Gökalp
Hasan İsmail Yavuz
Serkan Oktay
Eray Abakay
Yasemin Yıldıran Avcu
Rıdvan Yamanoğlu
author_facet Ümit Gencay Başcı
Egemen Avcu
Mertcan Kıraç
Ahmet Sever
İdris Gökalp
Hasan İsmail Yavuz
Serkan Oktay
Eray Abakay
Yasemin Yıldıran Avcu
Rıdvan Yamanoğlu
author_sort Ümit Gencay Başcı
collection DOAJ
description The present study investigates the microstructural, mechanical, and tribological properties of Inconel 718 alloy produced by selective laser melting (SLM) in relation to heat treatment. The SLM-processed samples received a two-step heat treatment: solutionizing at 1065 °C for 1 h, followed by double aging at 720 °C for 8 h and 620 °C for 6 h. The as-built sample exhibited a grain structure mostly characterized by fine Laves phases, while the hardening phases γ′ ((Ni<sub>3</sub> (Al, Ti)) and γ″ (Ni<sub>3</sub>Nb) precipitated during the heat treatment. Following heat treatment, a transformation in crystallographic texture and dislocation density occurred, yielding a random texture and reduced dislocation density, particularly in the XZ direction, attributed to the formation of new grains via recrystallization in the microstructure. The grain size in the XY plane decreased following heat treatment, whereas the texture in the <001> direction remained unaffected. The heat-treated samples had significantly higher tensile strength (1330 MPa vs. 960 MPa) and hardness (530 HV vs. 340 HV) relative to the as-built samples. The wear resistance of heat-treated samples surpassed that of the as-built sample due to enhanced mechanical properties resulting from the fine and dispersed γ′ and γ″ precipitates in the microstructure with heat treatment.
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institution Kabale University
issn 2073-4352
language English
publishDate 2024-12-01
publisher MDPI AG
record_format Article
series Crystals
spelling doaj-art-03c870dcbd3141b69fdc3cf44790ac982025-01-24T13:28:01ZengMDPI AGCrystals2073-43522024-12-011511810.3390/cryst15010018Microstructural, Mechanical, and Tribological Properties of Selective Laser Melted Inconel 718 Alloy: The Influences of Heat TreatmentÜmit Gencay Başcı0Egemen Avcu1Mertcan Kıraç2Ahmet Sever3İdris Gökalp4Hasan İsmail Yavuz5Serkan Oktay6Eray Abakay7Yasemin Yıldıran Avcu8Rıdvan Yamanoğlu9Department of Metallurgical and Materials Engineering, Kocaeli University, Kocaeli 41001, TurkeyDepartment of Mechanical Engineering, Kocaeli University, Kocaeli 41001, TurkeyR&D Department, ERMAKSAN, Bursa 16065, TurkeyR&D Department, ERMAKSAN, Bursa 16065, TurkeyDepartment of Metallurgical and Materials Engineering, Kocaeli University, Kocaeli 41001, TurkeyDepartment of Metallurgical and Materials Engineering, Kocaeli University, Kocaeli 41001, TurkeyR&D Department, Colakoglu Metalurji, Dilovası, Kocaeli 41455, TurkeyDepartment of Metallurgy and Materials Engineering, Sakarya University, Sakarya 54050, TurkeyDepartment of Mechanical Engineering, Kocaeli University, Kocaeli 41001, TurkeyDepartment of Metallurgical and Materials Engineering, Kocaeli University, Kocaeli 41001, TurkeyThe present study investigates the microstructural, mechanical, and tribological properties of Inconel 718 alloy produced by selective laser melting (SLM) in relation to heat treatment. The SLM-processed samples received a two-step heat treatment: solutionizing at 1065 °C for 1 h, followed by double aging at 720 °C for 8 h and 620 °C for 6 h. The as-built sample exhibited a grain structure mostly characterized by fine Laves phases, while the hardening phases γ′ ((Ni<sub>3</sub> (Al, Ti)) and γ″ (Ni<sub>3</sub>Nb) precipitated during the heat treatment. Following heat treatment, a transformation in crystallographic texture and dislocation density occurred, yielding a random texture and reduced dislocation density, particularly in the XZ direction, attributed to the formation of new grains via recrystallization in the microstructure. The grain size in the XY plane decreased following heat treatment, whereas the texture in the <001> direction remained unaffected. The heat-treated samples had significantly higher tensile strength (1330 MPa vs. 960 MPa) and hardness (530 HV vs. 340 HV) relative to the as-built samples. The wear resistance of heat-treated samples surpassed that of the as-built sample due to enhanced mechanical properties resulting from the fine and dispersed γ′ and γ″ precipitates in the microstructure with heat treatment.https://www.mdpi.com/2073-4352/15/1/183D printingselective laser meltingsuper alloyheat treatmentprecipitation strengthening phasesdeformation mechanism
spellingShingle Ümit Gencay Başcı
Egemen Avcu
Mertcan Kıraç
Ahmet Sever
İdris Gökalp
Hasan İsmail Yavuz
Serkan Oktay
Eray Abakay
Yasemin Yıldıran Avcu
Rıdvan Yamanoğlu
Microstructural, Mechanical, and Tribological Properties of Selective Laser Melted Inconel 718 Alloy: The Influences of Heat Treatment
Crystals
3D printing
selective laser melting
super alloy
heat treatment
precipitation strengthening phases
deformation mechanism
title Microstructural, Mechanical, and Tribological Properties of Selective Laser Melted Inconel 718 Alloy: The Influences of Heat Treatment
title_full Microstructural, Mechanical, and Tribological Properties of Selective Laser Melted Inconel 718 Alloy: The Influences of Heat Treatment
title_fullStr Microstructural, Mechanical, and Tribological Properties of Selective Laser Melted Inconel 718 Alloy: The Influences of Heat Treatment
title_full_unstemmed Microstructural, Mechanical, and Tribological Properties of Selective Laser Melted Inconel 718 Alloy: The Influences of Heat Treatment
title_short Microstructural, Mechanical, and Tribological Properties of Selective Laser Melted Inconel 718 Alloy: The Influences of Heat Treatment
title_sort microstructural mechanical and tribological properties of selective laser melted inconel 718 alloy the influences of heat treatment
topic 3D printing
selective laser melting
super alloy
heat treatment
precipitation strengthening phases
deformation mechanism
url https://www.mdpi.com/2073-4352/15/1/18
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