Cytotoxic Activity of Essential Oils from Middle Eastern Medicinal Plants on Malignant Keratinocytes

Skin cancer, including melanoma and non-melanoma cancers (basal and squamous cell carcinomas), is the most common type of cancer. UV radiation, family history, and genetic predisposition are the main risk factors. Although surgical excision is the standard treatment, essential oils are attracting gr...

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Main Authors: Rima Othman, Vanessa Moarbes, Muriel Tahtouh Zaatar, Diane Antonios, Rabih Roufayel, Marc Beyrouthy, Ziad Fajloun, Jean-Marc Sabatier, Marc Karam
Format: Article
Language:English
Published: MDPI AG 2025-07-01
Series:Molecules
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Online Access:https://www.mdpi.com/1420-3049/30/13/2844
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author Rima Othman
Vanessa Moarbes
Muriel Tahtouh Zaatar
Diane Antonios
Rabih Roufayel
Marc Beyrouthy
Ziad Fajloun
Jean-Marc Sabatier
Marc Karam
author_facet Rima Othman
Vanessa Moarbes
Muriel Tahtouh Zaatar
Diane Antonios
Rabih Roufayel
Marc Beyrouthy
Ziad Fajloun
Jean-Marc Sabatier
Marc Karam
author_sort Rima Othman
collection DOAJ
description Skin cancer, including melanoma and non-melanoma cancers (basal and squamous cell carcinomas), is the most common type of cancer. UV radiation, family history, and genetic predisposition are the main risk factors. Although surgical excision is the standard treatment, essential oils are attracting growing interest for their anti-cancer effects. This study tested the effects of <i>Juniperus excelsa</i> M. Bieb. (Cupressaceae), <i>Lavandula vera</i> DC. (Lamiaceae), and <i>Salvia fruticosa (Mill)</i>. (Lamiaceae) essential oils extracted from Middle Eastern medicinal plants on HaCaT (normal), A5 (benign), and II4 (low-grade malignant) keratinocytes. Essential oils were extracted from <i>Juniperus excelsa</i>, <i>Lavandula vera</i>, and <i>Salvia libanotica</i> using steam distillation and then were chemically analyzed. The oils were sterilized, dissolved in DMSO, and prepared at concentrations of 0.75, 0.5, and 0.25 mg/mL. Human keratinocyte (HaCaT), benign (A5), and malignant (II4) cell lines were cultured in DMEM and treated with the essential oils for 24 or 48 h. Cell viability was assessed using the Trypan Blue Exclusion Test, while cell proliferation was evaluated using the MTT assay. Statistical analysis was performed using ANOVA with appropriate post hoc tests, considering <i>p</i> < 0.05 as significant. The results show that <i>J. excelsa</i> is cytotoxic but lacks selectivity, limiting its efficacy. In contrast, <i>L. vera</i> and <i>S. fruticosa</i> preferentially target malignant cells, particularly at low concentrations, while sparing normal cells. These oils have dose-dependent anticancer effects, with <i>L. vera</i> efficacy increasing as the concentration increases. In conclusion, <i>L. vera</i> and <i>S. fruticosa</i> are promising candidates for the treatment of skin cancer, although further in vivo studies are required.
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spelling doaj-art-023d5575e1f04ace88cf489d0588549b2025-08-20T03:28:33ZengMDPI AGMolecules1420-30492025-07-013013284410.3390/molecules30132844Cytotoxic Activity of Essential Oils from Middle Eastern Medicinal Plants on Malignant KeratinocytesRima Othman0Vanessa Moarbes1Muriel Tahtouh Zaatar2Diane Antonios3Rabih Roufayel4Marc Beyrouthy5Ziad Fajloun6Jean-Marc Sabatier7Marc Karam8Department of Pulmonary Medicine and Critical Care, Johns Hopkins University, Baltimore, MD 21205, USADepartment of Biology, Faculty of Sciences, University of Balamand, Al-Kourah, Tripoli P.O. Box 100, LebanonDepartment of Biological and Physical Sciences, American University in Dubai, Dubai P.O. Box 28282, United Arab EmiratesLaboratory of Toxicology, Faculty of Pharmacy, Saint Joseph University of Beirut, Damascus Road, Beirut P.O. Box 11-5076, LebanonCollege of Engineering and Technology, American University of the Middle East, Egaila 54200, KuwaitDepartment of Agriculture and Food Engineering, School of Engineering, Holy Spirit University of Kaslik, Jounieh P.O. Box 446, LebanonDepartment of Cell Culture, Laboratory of Applied Biotechnology (LBA3B), Azm Center for Research in Biotechnology and Its Applications, EDST, Lebanese University, Tripoli 1300, LebanonInst Neurophysiopathol (INP), CNRS, Aix-Marseille Université, 13385 Marseille, FranceDepartment of Biology, Faculty of Sciences, University of Balamand, Al-Kourah, Tripoli P.O. Box 100, LebanonSkin cancer, including melanoma and non-melanoma cancers (basal and squamous cell carcinomas), is the most common type of cancer. UV radiation, family history, and genetic predisposition are the main risk factors. Although surgical excision is the standard treatment, essential oils are attracting growing interest for their anti-cancer effects. This study tested the effects of <i>Juniperus excelsa</i> M. Bieb. (Cupressaceae), <i>Lavandula vera</i> DC. (Lamiaceae), and <i>Salvia fruticosa (Mill)</i>. (Lamiaceae) essential oils extracted from Middle Eastern medicinal plants on HaCaT (normal), A5 (benign), and II4 (low-grade malignant) keratinocytes. Essential oils were extracted from <i>Juniperus excelsa</i>, <i>Lavandula vera</i>, and <i>Salvia libanotica</i> using steam distillation and then were chemically analyzed. The oils were sterilized, dissolved in DMSO, and prepared at concentrations of 0.75, 0.5, and 0.25 mg/mL. Human keratinocyte (HaCaT), benign (A5), and malignant (II4) cell lines were cultured in DMEM and treated with the essential oils for 24 or 48 h. Cell viability was assessed using the Trypan Blue Exclusion Test, while cell proliferation was evaluated using the MTT assay. Statistical analysis was performed using ANOVA with appropriate post hoc tests, considering <i>p</i> < 0.05 as significant. The results show that <i>J. excelsa</i> is cytotoxic but lacks selectivity, limiting its efficacy. In contrast, <i>L. vera</i> and <i>S. fruticosa</i> preferentially target malignant cells, particularly at low concentrations, while sparing normal cells. These oils have dose-dependent anticancer effects, with <i>L. vera</i> efficacy increasing as the concentration increases. In conclusion, <i>L. vera</i> and <i>S. fruticosa</i> are promising candidates for the treatment of skin cancer, although further in vivo studies are required.https://www.mdpi.com/1420-3049/30/13/2844anti-cancer effectMTT assayessential oilHaCatA5 cell linesII4 cell lines
spellingShingle Rima Othman
Vanessa Moarbes
Muriel Tahtouh Zaatar
Diane Antonios
Rabih Roufayel
Marc Beyrouthy
Ziad Fajloun
Jean-Marc Sabatier
Marc Karam
Cytotoxic Activity of Essential Oils from Middle Eastern Medicinal Plants on Malignant Keratinocytes
Molecules
anti-cancer effect
MTT assay
essential oil
HaCat
A5 cell lines
II4 cell lines
title Cytotoxic Activity of Essential Oils from Middle Eastern Medicinal Plants on Malignant Keratinocytes
title_full Cytotoxic Activity of Essential Oils from Middle Eastern Medicinal Plants on Malignant Keratinocytes
title_fullStr Cytotoxic Activity of Essential Oils from Middle Eastern Medicinal Plants on Malignant Keratinocytes
title_full_unstemmed Cytotoxic Activity of Essential Oils from Middle Eastern Medicinal Plants on Malignant Keratinocytes
title_short Cytotoxic Activity of Essential Oils from Middle Eastern Medicinal Plants on Malignant Keratinocytes
title_sort cytotoxic activity of essential oils from middle eastern medicinal plants on malignant keratinocytes
topic anti-cancer effect
MTT assay
essential oil
HaCat
A5 cell lines
II4 cell lines
url https://www.mdpi.com/1420-3049/30/13/2844
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