Formation of alumina-aluminide coatings on ferritic-martensitic T91 steel

In this work, alumina-aluminide coatings were formed on ferritic-martensitic T91 steel substrate. First, coatings of aluminum were deposited electrochemically on T91 steel in a room temperature AlCl3-1-ethyl-3-methyl imidazolium chloride ionic liquid, then the obtained coating was subjected...

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Bibliographic Details
Main Authors: Choudhary R.K., Kain V., Hubli R.C.
Format: Article
Language:English
Published: University of Belgrade, Technical Faculty, Bor 2014-01-01
Series:Journal of Mining and Metallurgy. Section B: Metallurgy
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Online Access:http://www.doiserbia.nb.rs/img/doi/1450-5339/2014/1450-53391400022C.pdf
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Summary:In this work, alumina-aluminide coatings were formed on ferritic-martensitic T91 steel substrate. First, coatings of aluminum were deposited electrochemically on T91 steel in a room temperature AlCl3-1-ethyl-3-methyl imidazolium chloride ionic liquid, then the obtained coating was subjected to a two stage heat treatment procedure consisting of prolonged heat treatment of the sample in vacuum at 300 ○C followed by oxidative heat treatment in air at 650 ○C for 16 hours. X-ray diffraction measurement of the oxidatively heat treated samples indicated formation of Fe-Al and Cr-Al intermetallics and presence of amorphous alumina. Energy dispersive X-ray spectroscopy measurement confirmed 50 wt- % O in the oxidized coating. Microscratch adhesion test conducted on alumina-aluminide coating formed on T91 steel substrate showed no major adhesive detachment up to 20 N loads. However, adhesive failure was observed at a few discrete points on the coating along the scratch track.
ISSN:1450-5339