Rapid Synthesis of Bradykinin in Solution

Two variants of the two-phase-purification method are examined, using the preparation of bradykinin as a model. In one synthesis, intermediate purification by liquid-liquid extraction was carried out after each completed elongation, in the other, new variant, the extractions were performed after th...

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Main Authors: Hanspeter Rolli, Conrad H. Schneider
Format: Article
Language:deu
Published: Swiss Chemical Society 1981-10-01
Series:CHIMIA
Online Access:https://www.chimia.ch/chimia/article/view/9537
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author Hanspeter Rolli
Conrad H. Schneider
author_facet Hanspeter Rolli
Conrad H. Schneider
author_sort Hanspeter Rolli
collection DOAJ
description Two variants of the two-phase-purification method are examined, using the preparation of bradykinin as a model. In one synthesis, intermediate purification by liquid-liquid extraction was carried out after each completed elongation, in the other, new variant, the extractions were performed after the deprotection steps. If not hampered by technical difficulties the second variant is more efficient.
format Article
id doaj-art-01a622abdf734e19b5e2c90d81b25f2c
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2673-2424
language deu
publishDate 1981-10-01
publisher Swiss Chemical Society
record_format Article
series CHIMIA
spelling doaj-art-01a622abdf734e19b5e2c90d81b25f2c2025-08-20T02:29:54ZdeuSwiss Chemical SocietyCHIMIA0009-42932673-24241981-10-01351010.2533/chimia.1981.403Rapid Synthesis of Bradykinin in SolutionHanspeter Rolli0Conrad H. Schneider1Institute for Clinical Immunology, Inselspital, 3010 Bern; Institute for Organic Chemistry, Freiestrasse 3, 3012 BernInstitute for Clinical Immunology, Inselspital, 3010 Bern; Institute for Organic Chemistry, Freiestrasse 3, 3012 Bern Two variants of the two-phase-purification method are examined, using the preparation of bradykinin as a model. In one synthesis, intermediate purification by liquid-liquid extraction was carried out after each completed elongation, in the other, new variant, the extractions were performed after the deprotection steps. If not hampered by technical difficulties the second variant is more efficient. https://www.chimia.ch/chimia/article/view/9537
spellingShingle Hanspeter Rolli
Conrad H. Schneider
Rapid Synthesis of Bradykinin in Solution
CHIMIA
title Rapid Synthesis of Bradykinin in Solution
title_full Rapid Synthesis of Bradykinin in Solution
title_fullStr Rapid Synthesis of Bradykinin in Solution
title_full_unstemmed Rapid Synthesis of Bradykinin in Solution
title_short Rapid Synthesis of Bradykinin in Solution
title_sort rapid synthesis of bradykinin in solution
url https://www.chimia.ch/chimia/article/view/9537
work_keys_str_mv AT hanspeterrolli rapidsynthesisofbradykinininsolution
AT conradhschneider rapidsynthesisofbradykinininsolution