Development of heat resistant Pb-free joints by TLPS process of Ag and Sn-Bi-Ag alloy powders
TLPS (Transient Liquid Phase Sintering) process is a candidate method of heat-resistant bonding, which makes use of the reaction between low-melting temperature powder of Sn-Bi base alloys and reactive powder of Ag. During heat treatment above the melting temperature of a Sn-Bi base alloy, the m...
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University of Belgrade, Technical Faculty, Bor
2012-01-01
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Series: | Journal of Mining and Metallurgy. Section B: Metallurgy |
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Online Access: | http://www.doiserbia.nb.rs/img/doi/1450-5339/2012/1450-53391200052O.pdf |
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author | Ohnuma I. Kainuma R. Ishida K. |
author_facet | Ohnuma I. Kainuma R. Ishida K. |
author_sort | Ohnuma I. |
collection | DOAJ |
description | TLPS (Transient Liquid Phase Sintering) process is a candidate method of heat-resistant bonding, which makes use of the reaction between low-melting temperature powder of Sn-Bi base alloys and reactive powder of Ag. During heat treatment above the melting temperature of a Sn-Bi base alloy, the molten Sn-Bi reacts rapidly with solid Ag particles, which results in the formation of heat-resistant intermetallic compound (IMC). In this study, the TLPS properties between Sn-17Bi-1Ag (at.%) powder with its liquidus temperature of 200°C and pure Ag powder were investigated. During differential scanning calorimetry (DSC) measurement, an exothermic reaction and an endothermic reaction occurred, which correspond to the formation of the e-Ag3Sn IMC phase and the melting of the Sn-17Bi-1Ag alloy, respectively. After the overall measurement, the obtained reactant consists of the Ag3Sn-IMC and Bi-rich phases, both of which start melting above 250°C, with a small amount of the residual Sn-Bi eutectic phase. These results suggest that the TLPS process can be applied for Pb-free heatresistant bonding. |
format | Article |
id | doaj-art-00ffa2d253794849a33d91159f8bda95 |
institution | Kabale University |
issn | 1450-5339 |
language | English |
publishDate | 2012-01-01 |
publisher | University of Belgrade, Technical Faculty, Bor |
record_format | Article |
series | Journal of Mining and Metallurgy. Section B: Metallurgy |
spelling | doaj-art-00ffa2d253794849a33d91159f8bda952025-02-02T07:03:45ZengUniversity of Belgrade, Technical Faculty, BorJournal of Mining and Metallurgy. Section B: Metallurgy1450-53392012-01-0148341341810.2298/JMMB121123052ODevelopment of heat resistant Pb-free joints by TLPS process of Ag and Sn-Bi-Ag alloy powdersOhnuma I.Kainuma R.Ishida K.TLPS (Transient Liquid Phase Sintering) process is a candidate method of heat-resistant bonding, which makes use of the reaction between low-melting temperature powder of Sn-Bi base alloys and reactive powder of Ag. During heat treatment above the melting temperature of a Sn-Bi base alloy, the molten Sn-Bi reacts rapidly with solid Ag particles, which results in the formation of heat-resistant intermetallic compound (IMC). In this study, the TLPS properties between Sn-17Bi-1Ag (at.%) powder with its liquidus temperature of 200°C and pure Ag powder were investigated. During differential scanning calorimetry (DSC) measurement, an exothermic reaction and an endothermic reaction occurred, which correspond to the formation of the e-Ag3Sn IMC phase and the melting of the Sn-17Bi-1Ag alloy, respectively. After the overall measurement, the obtained reactant consists of the Ag3Sn-IMC and Bi-rich phases, both of which start melting above 250°C, with a small amount of the residual Sn-Bi eutectic phase. These results suggest that the TLPS process can be applied for Pb-free heatresistant bonding.http://www.doiserbia.nb.rs/img/doi/1450-5339/2012/1450-53391200052O.pdfTransient Liquid Phase Sintering (TLPS)CALPHADhigh-tepmerature Pb-free solder |
spellingShingle | Ohnuma I. Kainuma R. Ishida K. Development of heat resistant Pb-free joints by TLPS process of Ag and Sn-Bi-Ag alloy powders Journal of Mining and Metallurgy. Section B: Metallurgy Transient Liquid Phase Sintering (TLPS) CALPHAD high-tepmerature Pb-free solder |
title | Development of heat resistant Pb-free joints by TLPS process of Ag and Sn-Bi-Ag alloy powders |
title_full | Development of heat resistant Pb-free joints by TLPS process of Ag and Sn-Bi-Ag alloy powders |
title_fullStr | Development of heat resistant Pb-free joints by TLPS process of Ag and Sn-Bi-Ag alloy powders |
title_full_unstemmed | Development of heat resistant Pb-free joints by TLPS process of Ag and Sn-Bi-Ag alloy powders |
title_short | Development of heat resistant Pb-free joints by TLPS process of Ag and Sn-Bi-Ag alloy powders |
title_sort | development of heat resistant pb free joints by tlps process of ag and sn bi ag alloy powders |
topic | Transient Liquid Phase Sintering (TLPS) CALPHAD high-tepmerature Pb-free solder |
url | http://www.doiserbia.nb.rs/img/doi/1450-5339/2012/1450-53391200052O.pdf |
work_keys_str_mv | AT ohnumai developmentofheatresistantpbfreejointsbytlpsprocessofagandsnbiagalloypowders AT kainumar developmentofheatresistantpbfreejointsbytlpsprocessofagandsnbiagalloypowders AT ishidak developmentofheatresistantpbfreejointsbytlpsprocessofagandsnbiagalloypowders |